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GB/T 30089-2013: Determination chlorpropamide, carbutamide and tolbutamide in cosmetics by LC-MS/MS method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 30089-2013 | English | 189 |
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Determination chlorpropamide, carbutamide and tolbutamide in cosmetics by LC-MS/MS method
| Valid |
GB/T 30089-2013
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Basic data | Standard ID | GB/T 30089-2013 (GB/T30089-2013) | | Description (Translated English) | Determination chlorporpamide, carbutamide and tolbutamide in cosmetics by LC-MS/MS method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 8,887 | | Quoted Standard | GB/T 6682 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the cosmetics chlorpropamide, carbutamide, tolbutamide liquid chromatography/tandem mass spectrometry. This standard applies to agent class, Cream, urea, carbutamide measured tolbutamide of gels, powder and lipstick Cosmetics chlor | GB/T 30089-2013: Determination chlorpropamide, carbutamide and tolbutamide in cosmetics by LC-MS/MS method
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Determination chlorporpamide, carbutamide and tolbutamide in cosmetics by LC-MS/MS method
ICS 71.100.70
Y42
National Standards of People's Republic of China
Cosmetics chlorpropamide, carbutamide, tolbutamide
Determination of liquid chromatography/tandem mass spectrometry
Determinationofchlorporpamide, carbutamideandtolbutamidein
Issued on. 2013-12-17
2014-03-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard was drafted in accordance with the rules of GB/T 1.1-2009 and GB/T 20001.4-2001 given.
This standard by the National Quality Supervision key product testing method Standardization Technical Committee (SAC/TC374) centralized.
This standard was drafted. Country cosmetics Quality Supervision and Inspection Center (Beijing), Beijing Haidian District, product quality supervision, inspection, inspection
Alliance (Beijing) Technology Research Institute of Quality.
The main drafters of this standard. Guoqi Lei, Yang Hongmei, Shihai Liang, Li Zhao, Liu Yanqin, Tian Yanling.
Cosmetics chlorpropamide, carbutamide, tolbutamide
Determination of liquid chromatography/tandem mass spectrometry
1 Scope
This standard specifies the cosmetics chlorpropamide, carbutamide, tolbutamide liquid chromatography/tandem mass spectrometry.
This standard applies to agent class, cream category, gels, powder and lipstick cosmetics category chlorpropamide, carbutamide, tolbutamide of
Determination.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Agent class, cream category, gels, powder cosmetics extracted with methanol; lipstick cosmetics dispersed by tetrahydrofuran, methanol extraction, solid phase extraction
Take a small column purification, using high performance liquid chromatography/tandem mass spectrometer, external standard.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade water as a water GB/T 6682 regulations.
4.1 acetonitrile. chromatography.
4.2 Methanol. chromatographically pure.
4.3 formic acid. Chromatographic pure.
4.4 tetrahydrofuran.
4.5 ammonia.
4.6 sodium chloride.
4.7 0.1% formic acid aqueous solution. accurate Pipette 1mL acid (4.3) to 1000mL volumetric flask, water volume.
4.8 2% methanol solution of formic acid. accurate Pipette 10mL formic acid (4.3) to 500mL volumetric flask with methanol (4.2) volume.
4.9 5% methanol aqueous ammonia solution. accurate Pipette 25mL ammonia (4.5) to 500mL volumetric flask with methanol (4.2) volume.
4.10 standard sample. chlorpropamide, carbutamide, tolbutamide standard sample specific information shown in Table 1.
Table 1 Standard sample information
Chinese name English name CAS Registry Number Formula Molecular Weight
Chlorpropamide Chlorpropamide 94-20-2 C10H13ClN2O3S 276.74
Carbutamide Carbutamide 339-43-5 C11H17N3O3S 271.34
Tolbutamide Tolbutamide 64-77-7 C12H18N2O3S 270.35
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