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GB/T 30088-2013: Determination of methyl eugenol in cosmetics by gas chromatography/mass spectrometry method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 30088-2013 | English | 189 |
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Determination of methyl eugenol in cosmetics by gas chromatography/mass spectrometry method
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GB/T 30088-2013
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Basic data | Standard ID | GB/T 30088-2013 (GB/T30088-2013) | | Description (Translated English) | Determination of methyl eugenol in cosmetics by gas chromatography/mass spectrometry method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 8,834 | | Regulation (derived from) | National Standards Bulletin No. 25 of 2013 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the cosmetics methyl eugenol gas chromatography/mass spectrometry. This standard applies to the determination of methyl eugenol agent class, cream lotion, lipstick and other cosmetics category. | GB/T 30088-2013: Determination of methyl eugenol in cosmetics by gas chromatography/mass spectrometry method
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Determination of methyl eugenol in cosmetics by gas chromatography/mass spectrometry method
ICS 71.100.70
Y42
National Standards of People's Republic of China
Determination of cosmetics methyl eugenol
Gas Chromatography/Mass Spectrometry
Issued on. 2013-12-17
2014-03-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard was drafted in accordance with the rules of GB/T 1.1-2009 and GB/T 20001.4-2001 given.
This standard by the National Quality Supervision key product testing method Standardization Technical Committee (SAC/TC374) centralized.
This standard was drafted. Country cosmetics Quality Supervision and Inspection Center (Beijing), Beijing Haidian District, product quality supervision, inspection, inspection
Alliance (Beijing) Technology Research Institute of Quality.
The main drafters of this standard. periphery Juan, Zhao Yuqi, Xu Hua, Liu Yanqin, Wuyan Tao, Cao Hong.
Determination of cosmetics methyl eugenol
Gas Chromatography/Mass Spectrometry
1 Scope
This standard specifies the methyl eugenol in cosmetics by gas chromatography/mass spectrometry.
This standard applies to the determination of methyl eugenol agent class, cream lotion, lipstick and other cosmetics.
Principle 2
Samples were solvent extracted, centrifuged, the supernatant microporous membrane filtration, and the filtrate was determined by gas chromatography/mass spectrometry, select from
Son and retention time qualitative, external standard.
3 Reagents and materials
Unless otherwise noted, all reagents were of analytical grade.
3.1 ethanol.
3.2 over anhydrous sodium sulfate.
3.3 sodium chloride.
3.4 hexane. chromatographically pure.
3.5 methyl eugenol standard sample specific information shown in Table 1.
Table 1-methyl-eugenol standard sample information
Chinese name INCI name CAS Registry Number Formula Molecular Weight Purity
Methyl eugenol MethylEugenol 93-15-2 C11H14O2 178.23 ≥98%
3.6 methyl eugenol standard stock solution. Weigh accurately standard sample 0.1000g, with anhydrous ethanol (3.1) dubbed 1000μg/mL standard
Stock solution, 4 ℃ refrigerator.
3.7 standard solution. take the right amount of methyl eugenol standard stock solution (3.6), with anhydrous ethanol (3.1) were formulated as a concentration
0.01μg/mL, 0.05μg/mL, 0.1μg/mL, 0.2μg/mL, 0.5μg/mL, 1μg/mL, 2μg/mL series of standard working solution
liquid. This series of standard working solution should now use the existing.
3.8 microporous membrane. 0.22μm, organic phase.
4 instruments and equipment
4.1 Gas chromatography/mass spectrometry (GC-MS). Hotels with electron impact ionization (EI).
4.2 Analysis of balance. a sense of the amount of 0.0001g.
4.3 centrifuges. centrifugal force of not less than 6000g.
4.4 ultrasonic cleaner.
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