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Determination of six kinds of phthalates in PVC toys and childcare articles. GC/MS method
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SN/T 2078-2008
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Basic data | Standard ID | SN/T 2078-2008 (SN/T2078-2008) | | Description (Translated English) | Determination of six kinds of phthalates in PVC toys and childcare articles. GC/MS method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | Y57 | | Word Count Estimation | 10,172 | | Date of Issue | 2008-04-29 | | Date of Implementation | 2008-11-01 | | Regulation (derived from) | Industry standard filing Notice 2008 No. 7 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the PVC toys and childcare articles in the six kinds of phthalate esters by gas chromatography mass spectrometry. This standard applies to PVC toys and childcare articles in six kinds of phthalates measured. | SN/T 2078-2008: Determination of six kinds of phthalates in PVC toys and childcare articles. GC/MS method
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Determination of six kinds of phthalates in PVC toys and childcare articles.GC/MS method
Exit inspection and quarantine industry standard book People's Republic of China
P Vp C toys and childcare articles of 6 phthalic
Dicarboxylate measured by gas chromatography - mass spectrometry
Posted 2008-04-29
2008-11-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
Appendix A of this standard is a normative appendix, Appendix B and Appendix C are informative appendix.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China, Shenzhen CIQ.
The main drafters. Zhang Ya, Liu Li, Wang Chengyun.
This standard is the first release of the entry-exit inspection and quarantine industry standards.
P Vp C toys and childcare articles of 6 phthalic
Dicarboxylate measured by gas chromatography - mass spectrometry
1 Scope
This standard specifies the gas chromatographic PVC toys and childcare articles in six kinds of phthalates - mass spectrometry methods.
This standard applies to the determination of PVC toys and childcare articles in six kinds of phthalates.
2 Terms and definitions
The following terms and definitions apply to this standard.
2.1
Containing PVC (polyvinyl chloride) toys and children's products.
Principle 3
Sample using ethyl acetate as the extraction solvent, the extraction, after extraction fluid volume by gas chromatography - mass spectrometry determination, internal standard method
Quantified. English name six kinds of phthalates, CAS number, and the formula given in Appendix A.
4 Reagents and materials
Unless otherwise specified, the reagents used were of analytical grade should be.
4.1 ethyl acetate.
4.2-n-butyl phthalate (DBP) standard. Purity ≥97%.
4.3 phthalate, butyl benzyl phthalate (BBP) Standard. Purity ≥97%.
4.4 bis (2-ethylhexyl) phthalate (DEHP) standard. Purity ≥97%.
4.5 phthalate, di-n-octyl phthalate (DNOP) Standard. Purity ≥97%.
4.6 diisononyl phthalate (DINP) Standard. Purity ≥97%.
4.7 phthalate, diisodecyl phthalate (DIDP) Standard. Purity ≥97%.
Phthalate 4.8 standard stock solution. Weigh accurately respectively dibutyl phthalate (DBP) standard (4.2), dibutyl phthalate
Benzyl ester (the BBP) standard (4.3), bis (2-ethylhexyl) phthalate (DEHP) standard (4.4) and di-n-octyl phthalate
(DNOP) standard (4.5) each 10.0mg, diisononyl phthalate (DINP) standard (4.6) and diisodecyl phthalate
(DIDP) standard (4.7) each 100.0mg, were placed in 100mL flask, diluted with ethyl acetate (4.1) to the mark and mix. Mark
Quasi stock solution was stored at 0 ℃ ~ 4 ℃ refrigerator valid for 12 months.
4.9 Internal standard. di-n-hexyl phthalate (DHP was). purity ≥97%.
4.10 standard internal standard stock solution. accurately weighed amount of di-n-hexyl phthalate (DHP) standard (4.9), with ethyl
(4.1) formulated at a concentration of 100mg/mL standard stock solution. Validity of standard stock solution was stored at 0 ℃ ~ 4 ℃ refrigerator
12 months.
4.11 mixed standard working solution. Apply the standard internal standard stock solution (4.10), phthalates standard stock solution (4.8), according to
We need to be diluted into a mixed standard working solution with suitable concentration of ethyl acetate (4.1). Validity of the working solution was kept at 0 ℃ ~ 4 ℃ refrigerator
6 months.
4.12 Internal standard solution. take appropriate internal standard stock solution (4.10), diluted to the appropriate concentration was necessary with ethyl acetate (4.1).
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