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GB 6675.14-2014 English PDF

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GB 6675.14-2014: Safety of toys -- Part 14: Requirements and test methods of finger paints
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Basic data

Standard ID GB 6675.14-2014 (GB6675.14-2014)
Description (Translated English) Safety of toys -- Part 14: Requirements and test methods of finger paints
Sector / Industry National Standard
Classification of Chinese Standard Y57
Classification of International Standard 97.200.50
Word Count Estimation 23,254
Date of Issue 12/5/2014
Date of Implementation 1/1/2016
Quoted Standard GB/T 1717; GB 5296.5; GB 6675.4; GB/T 6682; GB/T 23344; cosmetics hygiene norms (People's Republic of China Ministry of Health)
Regulation (derived from) Announcement of Newly Approved National Standards 2014 No. 27
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the technical requirements and test methods for use by children under 14 years of age for the finger paints. This standard applies to finger paints for children under 14 to use the substances and materials, finger paints and other

GB 6675.14-2014: Safety of toys -- Part 14: Requirements and test methods of finger paints

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Safety of toys - Part 14. Requirements and test methods of finger paints ICS 97.200.50 Y57 National Standards of People's Republic of China Safety of toys - Part 14. Finger paints technical requirements and test methods Safetyoftoys-Part 14. Issued on. 2014-12-05 2016-01-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Table of Contents

Preface Ⅰ 1 Scope 1 2 Normative references 1 3 Terms and definitions 4 requires 2 4.1 General requirements 2 4.2 colorant 2 4.3 Preservatives 2 4.4 adhesives, fillers, humectants and surfactants 3 4.5 pH value 3 4.6 Migration can limit specific elements 3 4.7 free primary aromatic amines Limited 3 Taste and smell 4 4.8 5 Test Method 5 5.1 colorant 5 Preservatives 5.2 5 5.3 pH value of 5 Migration of certain elements 5 5.4 5.5 free primary aromatic amines 5 6 logo and instructions 5 Appendix A (informative) Finger paints allowed colorant 6 Appendix B (normative) Finger paints preservatives allowed 11 Annex C (informative) Finger paints used in the production of components 13 Confirm method for determining Annex D (informative) specific azo dyes and primary aromatic amines 15

Foreword

GB 6675 according to Section 4.6 are mandatory, others are recommended. GB 6675 toy safety series of standards, including the following sections. --- Basic specification (GB 6675.1); --- General requirements, including but not limited to, move the mechanical and physical properties (GB 6675.2), flammability (GB 6675.3), a particular element Move (GB 6675.4); --- Specific requirements, requirements for specific products. This is Part 14 GB 6675's. This part is a series of toy safety standards Finger paints specific requirements (GB 6675.14), and GB 6675.1, GB 6675.2, GB 6675.3, GB 6675.4, GB 19865 (applicable to electric toys) combination. This section drafted in accordance with GB/T 1.1-2009 given rules. Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents. This part is proposed by the China National Light Industry Council. This part of the National Toy Standardization Technical Committee (SAC/TC253) centralized. This section drafted by. China Shanghai Import and Export Toy Inspection Center, Shenzhen City, measuring Detection Co., Ltd., Beijing Certification Center of Light, SZCIQ Toy Testing Center, Shenzhen Academy of Metrology and Quality Inspection, Inspection and Quarantine Bureau of Guangdong Entry-Exit Phytophthora Toys Lab Technology Center, Zhejiang Institute of Quality and Technical Supervision and Inspection. The main drafters of this section. Bi Wei Wen, Yu Wen Jia, Zhu Ping, Li Xuan, Zhao Yan, Xiao-hong, Chenxiao Zhen, Miujun Wen. Safety of toys - Part 14. Finger paints technical requirements and test methods

1 Scope

GB 6675 This section specifies the technical requirements and test methods used by children under 14 for the finger paints. This section applies to finger paints for children under 14 to use the substances and materials, products, in addition to finger paints Finger paints outside Other components and materials used in this section does not apply.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. Determination of GB/T 1717 aqueous pigment suspension pH value GB 5296.5 consumer use - Part 5. Toys GB 6675.4 Safety of toys - Part 4. Migration of certain elements Laboratory use specifications and test methods GB/T 6682 Analysis Determination of GB/T 23344 Textiles 4-amino azobenzene "Hygienic Standard for Cosmetics" (People's Republic of China Ministry of Health)

3 Terms and Definitions

The following terms and definitions apply to this document. 3.1 Finger paints fingerpaints Designed for children with a finger or hand applied directly to the surface of clay or gel-like coloring material. NOTE. Finger pigment component other than water, including colorants, fillers, adhesives, humectants, preservatives, surfactants and the like bitterness. 3.2 Colorant colourant Compound for coloring (dyes and pigments). 3.3 Fillers extender Insoluble substance by the particles to increase the volume of the product, or to optimize the use of the effect of beauty products. 3.4 Humectant humectant Can delay product dry substance. 3.5 Adhesives bindingagent Less volatile, soluble or water-soluble compound, the product can adhere to the surface of his painting. 3.6 Preservative preservative Prevent microbial growth substances. 3.7 Surfactant surfactant Improve product surface active substances. 3.8 Bitters embitteringagent So that products with a bitter substance.

4 Requirements

4.1 General requirements Finger paints must not contain dangerous substances or preparations, in order to avoid the use of children's finger paints pose a health risk. Appendix A and Appendix B listed coloring agents and preservatives shall comply with the requirements of 4.1. 4.2 colorant 4.2.1 Finger paints disable the following materials. Acute toxicity --- (1) --- Skin corrosion/irritation (2) --- Serious eye damage/eye irritation (3) --- Respiratory or skin sensitization (4) --- Germ cell mutagenicity (5) --- Carcinogenic (6) --- Reproductive toxicity (7) --- Specific target organ toxicity single exposure (8) --- Specific target organ toxicity, repeated exposure (9) --- Inhalation Hazard (10) Note 1. (1) See GB 30000.18-2013 "classification and labeling of chemicals - Part 18. Acute toxicity"; (2) See GB 30000.19-2013 "Chemistry Product classification and labeling specifications - Part 19. Skin corrosion/irritation "; (3) See GB 30000.20-2013" chemical classification and labeling regulations Fan - Part 20. Serious eye damage/eye irritation "; (4) See GB 30000.21-2013" classification and labeling of chemicals - Part 21. Breathing Tract or skin sensitization "; (5) See GB 30000.22-2013" chemical classification and labeling specifications - Part 22. Germ cell mutagenicity "; (6) See GB 30000.23-2013 "classification and labeling of chemicals - Part 23. carcinogenic"; (7) See GB 30000.24-2013 "classification of chemicals and Label specifications - Part 24. Reproductive toxicity "; (8) See GB 30000.25-2013" chemical classification and labeling Part 25. Specific target Organ toxicity, single exposure. "; (9) See GB 30000.26-2013" chemical classification and labeling specifications - Part 26. Specific target organ toxicity Repeated exposure "; (10) See GB 30000.27-2013" chemical classification and labeling specifications - Part 27. Inhalation Hazard. " Note 2. Appendix A shows the widespread use of the provisions of the purity of the colorant; Table A.1 colorants can be divided into the following categories. Food coloring; cosmetic colorant; meet the requirements of other pigments 4.1. 4.2.2 Finger paints may not contain one or more may be lost by degrading azo group to generate Table 3 and Table 4 primary aromatic listed in Amine azo dyes. 4.3 Preservatives Finger paints only use preservatives listed in Appendix B, the maximum allowable limits and restrictions and requirements shall comply with Appendix B requirements. 4.4 adhesives, fillers, humectants and surfactants Not use carcinogenic, teratogenic, reproductive toxicity, highly toxic, toxic, harmful, corrosive, irritant or induced allergic adhesive, filled Filling agents, humectants and surfactants. Appendix C lists allow the use of adhesives, fillers, humectants and surfactants. 4.5 pH value Finger paints a pH should be between 4.0 to 10.0. 4.6 specific elements can limit migration The results migration particular element of finger paints corrected (corrected according to Table 2) shall not exceed the maximum limits specified in Table 1 Volume requirements. Table 1 Finger paints requirements of maximum levels for certain elements migration Element antimony arsenic barium cadmium chromium lead, mercury and selenium Material Maximum limit/(mg/kg) 10 10 350 15 25 25 10 50 Table 2 Analysis of correction coefficients Element antimony arsenic barium cadmium chromium lead, mercury and selenium Analysis of the correction coefficient /% 6,060,303,030,305,060 4.7 limit free primary aromatic amines 4.7.1 Finger paints not detected in table 3 free primary aromatic amines listed. Table 3 Finger paints may not be detected in the primary aromatic amines No. Name primary aromatic amines CAS Number (CAS) 1 benzidine (benzidine) 92-87-5 22- naphthylamine (2-naphthylamine) 91-59-8 34- chloro-2-methylaniline (4-chloro-o-toluidine) (4-chloro-2-methyl-aniline) (4-chloro-o-toluidine) 95-69-2 44- aminobiphenyl (4-aminobiphenyl) 92-67-1 4.7.2 In addition to aromatic amines listed in Table 3, the finger paints contained in any of the aromatic primary aromatic amines should not exceed the total amount of 20mg/kg, and Hong amine content should not exceed 10mg/kg. This restriction does not apply to an aromatic amino acid or amino acid. Table 4 lists the primary aromatic amines other concerns. Table 4 concern other primary aromatic amines No. Name primary aromatic amines CAS Number (CAS) 1 o aminoazobenzene toluene (o-aminoazotoluene) (4-o-tolylazo-o-toluidine) 97-56-3 22- amino-4-nitrotoluene (2-amino-4-nitro-toluene) (5-nitro-o-toluidine) 99-55-8 34- chloroaniline (4-chloroaniline) 106-47-8 4-amino-2,4-anisole (2,4-diaminoanisole) 615-05-4 5 4,4'-diaminodiphenylmethane (4,4'-diaminodiphenylmethane) 101-77-9 6 3,3'-dichloro-benzidine (3,3'-dichlorobenzidine) 91-94-1 7-dimethoxy-3,3'-benzidine (3,3'-dimethoxybenzidine) 119-90-4 8-methyl-3,3'-benzidine (3,3'-dimethylbenzidine) 119-93-7 3,3'-dimethyl-4,4'-diamino-xylene dioxane (3,3'-dimethyl-4,4'-diaminodiphenylemethane) 838-88-0 102--methoxy-5-methylaniline (p-cresidine) (6-methoxy-m-toluidine) 120-71-8 2,2'-dichloro-4,4'-diaminodiphenyl methane-amino (4,4 'diamino-3,3' dichlorodiphenyl methane) (2,2'-dichloro-4,4'-methylenedianiline) (4,4'-methylene-bis-2-chloroaniline) 101-14-4 12 diaminodiphenyl ether (4,4'-oxydianiline) 101-80-4 13 4,4'-diaminodiphenyl sulfide (4,4'-thiodianiline) 139-65-1 142- methylaniline (o-toluidine) 95-53-4 15 2,4-dimethylaniline (2,4-xylidine) 95-68-1 16 2,6-dimethylaniline (2,6-xylidine) 87-62-7 174- amino-3-fluorophenol (4-amino-3-fluorophenol) 399-95-1 18 o-anisidine (2-methoxyaniline) (o-anisidine) 90-04-0 194- aminoazobenzene (4-aminoazobenzene) 60-09-3 20 2,4-diaminotoluene (4-methl-m-phenylenediamine) (toluene-2,4-diamine) 95-80-7 21 2,4,5-trimethyl aniline (2,4,5-trimethylaniline) 137-17-7 22 62-53-3 Aniline 4.8 taste and smell Finger paints should not have sweetness, flavor or other flavors to attract children, should be added to any of the following bittering agent to minimize children Swallowing possibility pigment. In the product life cycle, bitterness should always be maintained. Finger paints diluted with water 100 times, should still feel bitter Taste exists. --- Naringin (CAS10236-47-2); --- Denatonium benzoate (CAS3734-33-6). NOTE. naringin and that the degree of bitterness ammonium benzoate ratio of about 1.3000 (naringin. denatonium benzoate). Bitters add a single reference concentration. 1% naringin, 0.0004% denatonium benzoate (4mg/kg).

5 Test Methods

5.1 colorant 5.1.1 Tables 3 and can produce (except 4-amino azobenzene) 4 primary aromatic amine dyes, according to Annex D for testing. 5.1.2 4-amino azobenzene according to GB/T 23344 for testing. 5.2 Preservatives Press the "Hygienic Standard for Cosmetics" test. 5.3 pH value According to GB/T 1717 testing. 5.4 Migration of certain elements According to GB 6675.4 test. 5.5 free primary aromatic amines Free primary aromatic amines in Appendix D for testing.

6 logo and instructions for use

Finger paints labeling and instructions for use should also comply with. 5296.5 required mandatory provisions of a) GB . b) shall be marked with the following warning on the packaging. "Warning children under 3 years should be used under the supervision of an adult." c) a list of preservatives should be marked on the product packaging and bitters. NOTE. preservatives should be marked chemical name, INCI name or CAS number.

Appendix A

(Informative) Finger paints allowed colorants Table A.1 Finger paints allowed colorants No. Color Index through With Chinese name Color Index No. 1) CAS No color limits and information Pigment Green Green 1 810 006 3) 2 yellow pigment yellow 1 116802512-29-0 4) Pigment Yellow 3 Yellow 3 117106486-23-3 4) 4 Yellow Pigment Yellow 74 117416358-31-2 5 Yellow Pigment Yellow 15,411,781 68134-22-5 6 Orange Pigment Orange 3812367 7 Red Pigment Red 18,812,467 8 Red Pigment Red 17,012,475 9 Pigment Brown Brown 2512510 20812514 Red Pigment Red 10 3212517 Purple Pigment Violet 11 Yellow Pigment Yellow 12 15,113,980 13 Yellow Pigment Yellow 12 210906358-85-6 14 Yellow Pigment Yellow 14 210955468-75-7 15 Pigment Yellow 13 211005102-83-0 yellow 3) 16 Yellow Pigment Yellow 17 211054531-49-1 17 Pigment Orange 13 Orange 211103520-72-7 Pigment Orange 18 15793-73-4 orange 3421115 Pigment Violet 19 purple 19 739001047-16-1 3) 20 2351319 215247-95-3,6358-30-1 Pigment Violet Violet 3) Pigment Yellow 21 13,856,300 30125-47-4 yellow Pigment Yellow 22 13,956,298 36888-99-0 yellow 16859300 Red Pigment Red 23 24 Pigment Orange 43 711054424-06-0 orange 4) 25 Pigment Red 122 73915980-26-7 red 3) Pigment Green 7 26 5 742601328-53-6 green) Pigment Green 27 3674265 14302-13-7 green 28 Pigment White 1977005 White Pigment Brown 29 Brown 2477310 Table A.1 (CONTINUED) No. Color Index through With Chinese name Color Index No. 1) CAS No color limits and information 5377788 Yellow Pigment Yellow 30 31 Yellow Pigment Yellow 155 200 310 68516-73-4 32 82643-43-4 red pigment red 214 200 660 Pigment Red 33 52238-92-3 red 24,220,067 Pigment Red 34 Red 48.4 15865.4 Pigment White 35 777 975 White Orange 36 Solvent Orange 111 920 37 Red Pigment Red 512 490 38 Acid Yellow 913 015 Yellow E1056) Acid Orange 39 614 270 Orange E1036) Red Food Red 40 114 700 Acid Red 41 Red 1414720 Red Food Red 42 214 815 Pigment Red 43 Red 68 155255850-80-6 5115580 Red Pigment Red 44 Pigment Red 45 57.1 15850.12) 5281-04-9 red Pigment Red 46 48.2 15865.22) 7023-61-2 red 47 Red Pigment Violet 63.1 15880.1 48 215 980 Food Orange Orange E1116) 49 Food Yellow 3 159 852) yellow E1106) Food Red 50 red 1716035 Acid Red 51 2716185 Red E1236) Acid Red 52 18 162 552) Red E1246) Acid Red 53 4116290 Red E1266) Acid Red 54 33 172 002) Red 55 1718965 Yellow Acid Yellow Acid Yellow 56 23 191 402) yellow E1026) 57 227 755 Food Black Black E1526) 58 128 440 Food Black Black E1516) Food Orange Orange 59 540 800 60 640 820 Food Orange Orange E160e6) 61 740 825 Food Orange Orange E160f6) 62 840 850 Food Orange Orange E161g6) Table A.1 (CONTINUED) No. Color Index through With Chinese name Color Index No. 1) CAS No color limits and information Acid Blue 63 3 420 512) Blue E1316) 342 053 64 Food Green Green 65 242 090 Food Blue Blue 66 Acid Green 5044090 Green E1426) Solvent Red 67 72 453 702) Orange 2- (6-hydroxy-3-oxo -3H- xanthene-9-yl) Not more than 1% of benzoic acid; 2- (bromo-6-hydroxyhexyl -3H- Xanthene-3-oxo-9-yl) benzoic acid Not more than 2% Acid Red 68 87 453 802) Red 2- (6-hydroxy-3-oxo -3H- xanthene-9-yl) Not more than 1% of benzoic acid; 2- (bromo-6-hydroxyhexyl -3H- Xanthene-3-oxo-9-yl) benzoic acid Not more than 2% Acid Red 69 92 454 102) Red 2- (6-hydroxy-3-oxo -3H- xanthene-9-yl) Not more than 1% of benzoic acid; 2- (bromo-6-hydroxyhexyl -3H- Xanthene-3-oxo-9-yl) benzoic acid Not more than 2% Acid Red 70 red 9545425 2- (6-hydroxy-3-oxo -3H- xanthene-9-yl) Not more than 1% of benzoic acid; 2- (6-hydroxyhexyl iodo -3H- Xanthene-3-oxo-9-yl) benzoic acid Less than 3% Food Red 71 14 454 302) Red E1276) 2- (6-hydroxy-3-oxo -3H- xanthene-9-yl) Not more than 1% of benzoic acid; 2- (bromo-6-hydroxyhexyl -3H- Xanthene-3-oxo-9-yl) benzoic acid Not more than 2% 72 Acid Yellow 347 005 Yellow E1046) 73 Pigment Red 83 (.1) 58000.1 104074-25-1 red Solvent Violet 74 Violet 1360725 Solvent Green Green 75 361 565 76 Acid Green 2561570 Green Pigment Blue 77 669800 Blue E1306) Pigment Blue 78 Blue 6469825 Pigment Blue 79 Blue 6673000 80 173 015 Food Blue Blue E1326) 81 Red Pigment Red 181 733602379-74-0 3673385 Purple Pigment Violet 82 Table A.1 (CONTINUED) No. Color Index through With Chinese name Color Index No. 1) CAS No color limits and information 83 Blue Pigment Blue 15 74160147-14-8 84 natural yellow 675 100 19 89382-88-7 27876-94-4 yellow natural yellow, natural red 1 85 475 120 Natural Orange Orange E160b6) 86 natural yellow 2775125 yellow E160d6) 87 2675130 natural yellow orange E160a6) 88 natural yellow 2775135 yellow E161d6) 89 natural white 175 170 white 90 natural yellow 375300458-37-7 yellow E1006) 91 Natural Red 4 754701390-65-4 1260-17-9 red E1206) 92 Natural Green 3 758108049-84-1 11006-34-1 green E1406) and E1416) 93 177 000 white metallic pigment E1736) 94 Pigment White 2477002 White Pigment White 95 White 19 770048047-76-5 Pigment Blue 96 Blue 2977007 1317-97-1,57455-37-5 Pigment Red 97 Red mixed 10,177,491 Pigment White 98 White 21 771207727-43-7 99 Pigment White 1477163 White 100 1877220 207-439-9,208-915-9 white pigment white E1706) 101 2577231 91315-45-6 white pigment white 102 677 266 1333-86-4 Pigment Black Black 103 977 267 black pigment black 104 Food Black 3 77268.1 black E1536) 105 Pigment Green 1777288 Green chromate ion 106 Pigment Green 1877289 Green chromate ion 107 2877346 Pigment Blue Green 108 277 400 brown metallic paint 109 3 774807440-57-5 brown metallic pigment E1756) 110 ferrous oxide 77489 Orange E172 (mixed) 6) 111 Pigment Red 101 774911309-37-1 red E1726) Pigment Yellow 112 4277492 51274-00-1 yellow E1726) 113 1177499 12227-89-3 Pigment Black Black E1726) 114 Pigment Blue 2777510 Blue non-cyanide ion 115 1877713 207-439-9,208-915-9 white pigment white magnesium carbonate Table A.1 (CONTINUED) No. Color Index through With Chinese name Color Index No. 1) CAS No color limits and information Pigment Violet Purple 116 1677742 117--77745 red hydrated manganese phosphate 118--77820 White E174 (Silver) 6) 119 677 891 13463-67-7 Pigment White White E1716) 120 White Pigment White 4 779471314-13-2 Riboflavin 121 - yellow E1016) 122 caramel - brown E1506) Red chili/pepper Jade TRs - Orange E160c6) 124 beet red - red E1626) 125 anthocyanins - red E1636) Aluminum stearate, zinc, Manganese and calcium - White 2) an insoluble colorant these barium, strontium, zirconium lakes, salts and pigments can also be allowed to use, they must be determined by the insoluble. 3) the substance is "Hygienic Standard for Cosmetics" restrictions, according to "dedicated only temporary contact with skin and cosmetics." 4) This substance is "Hygienic Standard for Cosmetics" restrictions, according to "dedicated to the cosmetic is not in contact with the mucous membranes." 5) This substance is "Hygienic Standard for Cosmetics" is limited, the "eye in addition to other cosmetic use cosmetics." 6) See 2008/128/EC "on the development of specific standards for the purity of the dye used in foods."

Appendix B

(Normative) Finger paints are allowed to use preservatives Table B.1 Finger paints preservatives allowed No. Substance CAS No. maximum permitted limit restrictions and requirements 1 benzoic acid, salts and esters 1) 0.5% (as acid) Propionic acid and its salts 1 2) 2% (as acid) 3 1 sorbic acid and its salts) 110-44-1 0.6% (as acid) More than four paraformaldehyde 30525-89-4 0.1% (in terms of free formaldehyde) 5-biphenyl-2-ol (o-phenylphenol) and its salts 1) 90-43-7 0.2% (in terms of free phenol) 6 Inorganic sulfites and bisulfite salts 0.2% (as free SO2 meter) 74- hydroxy benzoic acid and its salts and esters 1) Single ester. 0.4% (as acid) Mixed esters. 0.8% (as acid) 8 dehydroacetic acid and its salts 1) 0.6% (as acid) 9-carboxylic acid and its sodium salt 1) 64-18-6 0.5% (as acid) Dibromo hexamidine and its salts, including hydroxyalkyl-dibromo hexamidine Ethanesulfonate 1) 0.1% 11 undecylenic acid and its salts 1) 0.2% (as acid) 12 hexamidine 3811-75-4 0.1% 132--bromo-2-nitropropane-1,3-diol 52-51-7 0.1% to avoid formation of nitrosamines 14 1777-82-8 2,4-dichlorobenzyl alcohol 0.15% 15 triclocarban 101-20-2 0.2% Purity criteria. 3,3 ', 4,4'-tetrachloro-azobis Benzene is less than 1mg/kg; 3,3 ', 4,4'-tetrachloro-oxide Azobenzene less than 1mg/kg 16 Triclosan 3380-34-5 0.3% 17 chloroxylenol 133-53-9 0.5% 18 0.6% imidazolidinyl urea 19 polyhexamethylene biguanide hydrochloride 32289-58-0 0.3% 20 phenoxyethanol 122-99-6 1.0% 21 100-97-0 methenamine 0.15% 22 Polyquaternium -154080-31-3 0.2% 23 climbazole 38083-17-9 0.5% 24 DMDM hydantoin 6440-58-0 0.6% Table B.1 (continued) No. Substance CAS No. maximum permitted limit restrictions and requirements 25 benzyl alcohol 100-51-6 1% 26 68890-66-4 piroctone olamine 0.5% 27-bromo-baclofen 15435-29-7 0.1% 284- isopropyl-3-cresol 3228-02-2 0.1% 292- benzyl-4-chlorophenol 120-32-1 0.2% Its two chlorhexidine gluconate, diacetate And dihydrochloride 0.3% (expressed as chlorhexidine) Alkyl (C12-C22) trimethylammonium bromide or chlorine Compound 0.1% 32 4,4-dimethyl-oxazoline 51200-87-4 0.1% pH manufactures can not Less than 6 33 pairs (hydroxymethyl) 0.5% imidazolidinyl urea 78491-02-8 Hexamidine and its salts, including two hexamidine isethionate Sulfonate and hexamidine p-hydroxybenzoate 1) 0.1% 35 chlorphenesin 104-29-0 0.3% 36 N- methylol 70161-44-3 sodium glycinate 0.5% Methyl chloride isothiazolin-ketone and methyl isothiazolin One with a mixture of magnesium chloride and magnesium nitrate 55965-84-9 0.0015% (chloro-methyl isothiazole Imidazolidinone and methylisothiazolinone to 3.1 mixture dollars) 1) "salt" means a cationic preservative sodium, potassium, calcium, magnesium, ammonium and ammonium alcohol salts formed by; or that a preservative and a chloride anion, bromine , Sulfate and acetate and other salts. Table "Ester" refers to methyl, ethyl, propyl, isopropyl, butyl, isobutyl, and phenyl. twenty one

Appendix C

(Informative) Finger paints used in the production of components Use the following components based on existing experience in the production of finger paints, Table C.1. Table C.1 composition table No. Name Carboxymethyl cellulose and salts thereof dextrin Polyvinyl alcohol Cellulose resin starch Tragacanth Xanthan gum Polyvinylpyrrolidone Casein Alginate Polyacrylate Calcium carbonate (including heroin) Calcium sulfate Silica Magnesia Alumina Magnesium silicate Calcium silicate Kaolin (ceramic clay) Bentonite twenty one twenty two twenty three twenty four Sodium polyphosphate Fatty alcohol ethoxylates Poly (alkylene) glycol ester Fatty acid sodium salt glycerin Polyethylene glycol Propanediol Table C.1 (continued) No. Name Edible fatty acid sodium salt Poly (alkylene) glycol ester Alkyl benzene sulfonate Polyethylene wax

Appendix D

(Informative) Confirmation method specific azo dyes and determination of primary aromatic amines D.1 Overview To detect a specific azo dye, the sample is first placed in sealed containers, 70 ℃ citrate buffer solution (PH = 6.0), and with sodium dithionite reduction treatment. The resulting reduction of aromatic amines by "kieselguhr" category diatomaceous earth column (such as ChromabondXTR or equivalent) After extraction with tert-butyl methyl ether extract. The solution was extracted carefully using a rotary evaporator or phase When the sample concentrator concentrated. Concentrated residue according to the detection/confirmation method requires dissolved in acetonitrile or other suitable solvent. Aromatic amines detection/confirmation method can be used. a diode array detector with high performance liquid chromatography (HPLC/DAD); with hydrogen Flame detector or mass detector gas chromatograph (GC/FID or GC/MS). Identification of aromatic amines may be used in this appendix least one chromatographic separation methods. Unless there is no confirmation method in a question (for example, Using GC/MS and retention time of a known standard methods and materials compared), otherwise positive results need to use another suitable separation technology Surge...

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