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SN/T 3618.1-2013: Determination of acetophenone in plastic and rubber materials. Part 1: HPLC method
Status: Valid
| Std ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status |
| SN/T 3618.1-2013 | English | 209 |
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Determination of acetophenone in plastic and rubber materials. Part 1: HPLC method
| Valid |
Basic data
| Standard ID | SN/T 3618.1-2013 (SN/T3618.1-2013) |
| Description (Translated English) | Determination of acetophenone in plastic and rubber materials. Part 1: HPLC method |
| Sector / Industry | Commodity Inspection Standard (Recommended) |
| Classification of Chinese Standard | G32 |
| Classification of International Standard | 83.080.01 |
| Word Count Estimation | 8,873 |
| Quoted Standard | GB/T 6682 |
| Regulation (derived from) | National quality recognition (2013), No. 464; industry standard filing Notice No. 1 of 2014 (No. 169 overall) |
| Issuing agency(ies) | General Administration of Customs |
| Summary | This standard specifies a method for detecting plastic material acetophenone - high performance liquid chromatography. This standard applies to the determination of the plastic material acetophenone. |
SN/T 3618.1-2013: Determination of acetophenone in plastic and rubber materials. Part 1: HPLC method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of acetophenone in plastic and rubber materials Part 1. HPLC method
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Determination of plastic material acetophenone
Part 1. High performance liquid chromatography
Part 1. HPLCmethod
Issued on. 2013-08-30
2014-03-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
SN/T 3618 "plastic material acetophenone determination" is divided into two parts.
--- Part 1. High performance liquid chromatography;
--- Part 2. Gas chromatography - mass spectrometry.
This section SN/T 3618 Part 1.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This section proposed and managed by the National Certification and Accreditation Administration Committee.
This section was drafted by. People's Republic of China Guangdong Entry-Exit Inspection and Quarantine Bureau Technology Center, China Inspection and Quarantine Science RESEARCH
Study hospital.
The main drafters of this section. Liang Jinling Liang Ying, Zeng Jiaxin, Guoren Hong, Zhang Zhihui, Zhang, birch, Liuzhuo Qin, Xian Liying, Lan Lili.
Determination of plastic material acetophenone
Part 1. High performance liquid chromatography
1 Scope
SN/T 3618 provisions of this part of the plastic material in the detection method of acetophenone --- High Performance Liquid Chromatography.
This section applies to the determination of the plastic material acetophenone.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Acetone sample of acetophenone extraction, high performance liquid chromatography with diode array detector (HPLC-DAD)
We were determined and confirmed, external standard.
4 Reagents and materials
Unless otherwise specified, use only analytical reagent. Test water line with GB/T 6682 stipulated a water.
4.1 acetone.
4.2 acetophenone standards. CAS No. 98-86-2; purity ≥98%.
4.3 acetonitrile. chromatography.
4.4 Methanol. chromatographically pure.
4.5 preparation of standard solution. Weigh accurately acetophenone standard (4.2) 0.02g (precise to 0.1mg) to 25mL volumetric flask with stopper
(5.3), and dissolved in acetone (4.1) and dilute to the mark, shake, progressively diluting the concentration of 0.5mg/L, 1.0mg/L,
2.0mg/L, 5.0mg/L, 20.0mg/L, 50.0mg/L and 100.0mg/L of standard working solution, in the refrigerator freezer spare.
5. Apparatus
5.1 Microwave extractor. with teflon extraction tank.
5.2 brown volumetric flask. 25mL.
5.3 plastic head glass dropper. 2mL.
5.4 Centrifuge. 8000r/min.
5.5 High performance liquid chromatograph. with DAD detector.
5.6 Electronic balance. a sense of the amount of 0.1mg.
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