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GB/T 24800.6-2009: Determination of 21 sulfonamides in cosmetics by high performance liquid chromatography method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 24800.6-2009 | English | 279 |
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Determination of 21 sulfonamides in cosmetics by high performance liquid chromatography method
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GB/T 24800.6-2009
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Basic data | Standard ID | GB/T 24800.6-2009 (GB/T24800.6-2009) | | Description (Translated English) | Determination of 21 sulfonamides in cosmetics by high performance liquid chromatography method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 12,154 | | Date of Issue | 2009-11-30 | | Date of Implementation | 2010-05-01 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | National Standard Approval Announcement 2009 No.14 (Total No.154) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard provides high-performance liquid chromatographic method cosmetic twenty-one kinds of sulfonamides. This standard applies to the determination of cosmetics twenty-one kinds of sulfonamides. | GB/T 24800.6-2009: Determination of 21 sulfonamides in cosmetics by high performance liquid chromatography method
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Determination of 21 sulfonamides in cosmetics by high performance liquid chromatography method
ICS 71.100.70
Y42
National Standards of People's Republic of China
Determination of cosmetics twenty-one kinds of sulfonamides
High Performance Liquid Chromatography
Posted 2009-11-30
2010-05-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
The Standard Appendix A, Appendix B is an informative annex.
The standard proposed by China National Light Industry Council.
This standard by the National Standardization Technical Committee of Fragrance Flavor and Cosmetic (SAC/TC257) centralized.
This standard is drafted by. China Inspection and Quarantine Science Research Institute, Shanghai Daily Chemical Industry Research Institute, Shanghai Institute of spices.
The main drafters of this standard. Ma Qiang, Zhang, Wang Chao, Xiao Haiqing, Wu Ting Kang Wei, Cui Jian Jie.
Introduction
The standard test substance is banned substances of "Hygienic Standard for Cosmetics" shall consist of not as a cosmetic raw material, component
Added to cosmetics. If technically unavoidable banned substances as impurities into cosmetics, the finished cosmetic products should follow the "Cosmetics
Health standards "General requirements for cosmetics, that is, under normal and reasonably foreseeable conditions of use, should not cause harm to human health.
At present, China has not yet specified the substance of limited value, the present standards, the determination of these substances in cosmetics only provide detection methods.
Determination of cosmetics twenty-one kinds of sulfonamides
High Performance Liquid Chromatography
1 Scope
This standard specifies a high performance liquid chromatographic method cosmetics twenty-one kinds of sulfonamides.
This standard applies to the determination of cosmetics twenty-one kinds of sulfonamides.
The standard detection and quantitation limits. sulfa guanidine, sulfonamides, sulfacetamide, of sulfonamide sulfadiazine, Sulfathiazole, sulfonamides topiramate
Piperidine, sulfamethyldiazine, sulfamethazine triazole, sulfamethazine, among sulfadimethoxine, sulfa quinoline morpholine, and the detection limit was sulfanitran
0.2mg/kg, the limit of quantification of 0.6mg/kg; sulfamethoxazole thiadiazole sulfa methoxy pyridazine, succinyl Sulfathiazole, sulfa chlorine pyridazine, sulfamethoxazole
Isobutyl yl, among methoxy pyrimidine sulfonamides, o-methoxy pyrimidine sulfonamides, sulfamethazine different azole detection limit of 0.4mg/kg, the limit of quantification
1.2mg/kg.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Sample by solvent extraction and centrifugal filtration, HPLC, external standard, liquid chromatography - mass spectrometry confirmed.
4 Reagents and materials
Unless otherwise noted, all reagents were of analytical grade water as a water GB/T 6682 regulations.
4.1 Methanol. chromatographically pure.
4.2 tetrahydrofuran. chromatography.
4.3 Sodium hydroxide solution (0.1mol/L). Weigh accurately 4g of sodium hydroxide in 1L flask, and dissolved in water to volume, mix
Even after use.
4.4 formic acid solution (0.1%). The exact amount of 1mL acid in 1L flask with water to volume, mix standby.
4.5 methanol aqueous solution. accurate amount of 50mL of methanol and 50mL water, mix and reserve.
4.6 sulfadoxine, sulfonamides, sulfacetamide, of sulfonamide sulfadiazine, Sulfathiazole, sulfasalazine, sulfamethyldiazine, sulfadiazine
A azole, sulfamethazine, sulfamethoxazole thiadiazole sulfa methoxy pyridazine, succinyl Sulfathiazole, sulfa chlorine pyridazine, sulfamethoxazole yl,
Suladimethoxypyrimidine, o-methoxy pyrimidine sulfonamides, sulfamethazine different yl, among sulfadimethoxine, sulfa quinoline morpholine, sulfanitran standard
Products. purity of greater than 97%.
Stock standard solution 4.7 twenty-one kinds of sulfonamides. Accurately weigh each sulfa standard substance (4.6) for each 100mg, were placed in 100mL brown
Volumetric flask, dissolved in aqueous methanol (4.5) and dilute to the mark, shake, formulated to concentrations of 1000μg/mL standard stock
Liquid stored in the dark at 4 ℃, can be used for three months.
Note. sulfa quinoline morpholine standard stock solution preparation, can be added a few drops of sodium hydroxide solution (4.3) Auxiliary dissolved.
Mixed standard stock solution 4.8 twenty-one kinds of sulfonamides. accurate Pipette respectively twenty-one kinds sulfa 4mL each stock standard solution in 100mL brown
Color volumetric flask with aqueous methanol (4.5) to the mark, the concentration of the solution twenty-one kinds of sulfonamides are 40μg/mL.
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