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GB 8318-2008: Food additive -- Oil of ginger, distilled (Zingiber officinale rosc.)
Status: Obsolete GB 8318: Evolution and historical versions
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| GB 8318-2008 | English | 319 |
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Food additive -- Oil of ginger, distilled (Zingiber officinale rosc.)
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GB 8318-2008
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| GB 8318-1987 | English | 199 |
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Food additive--Oil of ginger (distilled)
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GB 8318-1987
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PDF similar to GB 8318-2008
Basic data | Standard ID | GB 8318-2008 (GB8318-2008) | | Description (Translated English) | Food additive -- Oil of ginger, distilled (Zingiber officinale rosc.) | | Sector / Industry | National Standard | | Classification of Chinese Standard | X41 | | Classification of International Standard | 71.100.60 | | Word Count Estimation | 8,819 | | Date of Issue | 2008-12-03 | | Date of Implementation | 2009-06-01 | | Older Standard (superseded by this standard) | GB 8318-1987 | | Quoted Standard | GB/T 5009.74; GB/T 5009.76; GB/T 11540; GB/T 14454.2; GB/T 14454.4; GB/T 14454.5; GB/T 14455.6 | | Adopted Standard | FCC V-2004, NEQ | | Regulation (derived from) | Announcement of Newly Approved National Standards No. 19 of 2008 (No. 132 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Chinese standard specifies the food additives ginger (refined) oil (distillation) requirements, test methods, inspection rules, marking, packaging, transportation, storage and shelf life. This standard applies to steam distillation from ginger (Zingiber officinale Rose.) Ginger rhizome extract (refined) oil. | GB 8318-2008: Food additive -- Oil of ginger, distilled (Zingiber officinale rosc.)---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food additive.Oil of ginger, distilled (Zingiber officinale rosc.)
ICS 71.100.60
X41
National Standards of People's Republic of China
Replacing GB 8318-1987
Ginger Food Additives (refined) oils (distilled)
Published 2008-12-03
2009-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China issued
Foreword
4.2,4.7,4.8 this standard is mandatory, the rest are recommended.
This standard and the US Food Chemicals Codex FCCⅤ.2004 "Ginger oil," it is not equivalent.
Instead of the standard GB 8318-1987 "Food Additives Ginger oil (distilled)."
This major change compared to the standard GB 8318-1987 as follows.
--- increased range Chapter 1, Chapter 2 normative references, Chapter 3 Terms and definitions;
--- The relative density of the measurement temperature was changed from 25 ℃ 20 ℃;
--- Added Appendix A typical gas chromatogram.
Appendix A of this standard is an informative annex.
The standard proposed by China Light Industry Federation.
This standard by the National Standardization Technical Committee on Food Additives.
Responsible for the drafting of this standard. Shanghai Institute of spices, spices Kunshan Development Zone drift Run Industrial Co., Ltd., Guangxi People's Republic of China
Entry-Exit Inspection and Quarantine Bureau and Anhui Fengle spices limited liability company.
The main drafters. Jin Qizhang, Zhou En Yu, Xu Yi, Fu Xuefu, Sun Qinghua, Yu Lei, Zheng Ling, Cao Yi.
This standard supersedes the previous editions are.
--- GB 8318-1987.
Ginger Food Additives (refined) oils (distilled)
Range 1
This standard specifies the ginger food additive (fine) claims an oil (distilled), test methods, inspection rules, marking, packaging, transportation, storage and
Shelf life.
2 Normative references
Terms of the following documents become provisions of this standard by reference in this standard. For dated reference documents, all later
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to agreements based on this standard
Whether the latest versions of these documents. For undated references, the latest version applies to this standard.
GB/T heavy metals in food additives 5009.74 limit test
Determination of arsenic in food additives 5009.76 GB/T
Determination GB/T 11540 perfume relative density (GB/T 11540-2008, ISO 279.1998, MOD)
GB/T 14454.2 spice aroma evaluation method
GB T 14454.4 Determination/perfume refractive index (GB/T 14454.4-2008, ISO 280.1998, MOD)
Determination GB/T 14454.5 perfume optical rotation (GB/T 14454.5-2008, ISO 592.1998, MOD)
GB/T 14455.6 perfume ester or a value measured amount of ester-containing (GB/T 14455.6-2008, ISO 709.2001, MOD)
3 Terms and Definitions
The following terms and definitions apply to this standard.
3.1
4 Requirements
4.1 Appearance. light yellow to yellow liquid.
4.2 Odor. characteristic aroma of ginger.
4.3 Relative density (20 ℃/20 ℃). 0.873 ~ 0.885.
4.4 Refractive index (20 ℃). 1.488 ~ 1.494.
4.5 Optical rotation (20 ℃). - 26 ° ~ -45 °.
4.6 Saponification value. ≤20.
4.7 Heavy metal content (as Pb). ≤10mg/kg.
4.8 arsenic content. ≤3mg/kg.
5 Test methods
5.1 Appearance of test
Place the specimen was observed visually than the inner tube color method.
5.2 Evaluation aroma
According to the provisions of GB/T 14454.2 of.
5.3 Determination of Relative Density
As specified in GB/T 11540 of.
5.4 Determination of refractive index
As specified in GB/T 14454.4 of.
5.5 Determination of optical rotation
As specified in GB/T 14454.5 of.
5.6 Determination of the saponification number
As specified in GB/T 14455.6 of. The results do not need to subtract the acid value.
5.7 Determination of heavy metal content (P Chou basis)
As specified in GB/T 5009.74 of.
5.8 Determination of arsenic content
As specified in GB/T 5009.76 of.
A typical gas chromatogram 6
Ginger Food Additives (refined) oils (distilled) typical gas chromatogram (area normalization method) see Appendix A, which by gas chromatography gives
Ginger assay (fine) and the operating conditions characteristic spectrum oil (distilled), the reference for producers and users.
7 Inspection rules
7.1 Food additives ginger (refined) oil (distillation) shall be factory quality inspection department inspection, the manufacturer shall ensure that products are in line with
Requirements of this standard, each batch of products should be accompanied by quality certificate. Like color, aroma, relative density, refractive index, optical rotation of the factory
Test items, and saponification value, content of heavy metals (Pb), arsenic content type test items, test once a year.
7.2 Acceptance shall be entitled in accordance with the provisions of this standard test received product quality meets the requirements of this standard, for each batch
Once acceptance, acceptance of different batches respectively.
7.3 Sampling method. batch packaging units 1 to 2, the whole pumping; 3 ~ 100 extracted 2; 100 or more further extraction increasing portion
3%. Sampling uniformly extracted from each sample 50mL ~ 100mL packing unit, the extracted sample mixed all placed within injector
Mix well, respectively, into two clean and dry, inert sealed containers, protected from light. Container attach a label stating. manufacturer name, product
Name, date of manufacture, batch number, quantity and date of sampling, as tested with a bottle, another bottle retained for future reference.
7.4 As a result there is an acceptance indicator does not meet the standard requirements, in conjunction with the plant extract sample was re-doubled retest. The junction reinspection
If there are indicators of failure, then the product can not be accepted.
7.5 When opposition occurs both supply and demand on product quality, by mutual agreement or arbitration to resolve a legal inspection agency.
8 signs, packaging, transportation, storage and shelf life
8.1 mark
Outer packaging should be marked. "food additive" word, product name, manufacturer name and address, trademark, batch number, net weight, production date
And shelf life, license number, standard number and related marks, and it shall comply with the relevant departments. For special customer requirements, with production plants
Another set protocol.
8.2 Packaging
Ginger Food Additives (refined) oils (distillation) should be installed in a clean coarse taste without food grade plastic or aluminum composite barrels barrel, according to customer requirements, or
package.
8.3 Transport
We should care, during transport, to prevent the sun and rain, not mixed with toxic and hazardous substances, transportation mix, and shall comply with the relevant departments
Provisions.
8.4 Storage
The product should be stored in a cool, dry, ventilated warehouse to avoid mixed air pollution, away from the fire source.
8.5 Shelf Life
Subject to the conditions of storage and transportation, packaging integrity, without the unsealing of the product shelf life of one year.
Appendix A
(Informative)
Ginger Food Additives (refined) oils (distilled) typical gas chromatogram
(Area normalization method)
A. 1 ginger food additive (refined) oils (distilled) typical gas chromatogram
See Figure A. 1.
1 --- α- pinene;
2 --- camphene;
3 --- limonene + 1,8-cineole;
4 --- linalool;
5 --- Long brain;
6 --- neral;
7 --- geranial;
8 --- geranyl acetate;
Aryl. 9 --- curcumene;
10 --- zingiberene;
11 --- α- farnesene;
12 --- β- bisabolene;
13 --- β- sesqui-phellandrene;
14 --- nerolidol.
Figure A. 1
A. 2 operating conditions
Column. length 60m, capillary column of inner diameter of about 0.25mm.
Stationary phase. polydimethylsiloxane [DB-1].
Film thickness. 0.25μm.
Chromatographic oven temperature. 80 ℃ thermostat 3min, followed by a linear temperature programmed from 80 deg.] C to 230 ℃, a rate of 3 ℃/min, and finally at 230 ℃
Constant temperature 20min.
Inlet temperature. 250 ℃.
Detector temperature. 250 ℃.
Detector. flame ionization detector.
Carrier gas. nitrogen.
Carrier gas flow rate. 1.5mL/min.
Injection volume. about 0.2μL.
Split ratio. 1/100.
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