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GB 6772-2008 English PDF

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GB 6772-2008: Food additive -- Oil of lemon, cold pressed
Status: Obsolete

GB 6772: Evolution and historical versions

Standard ID	Contents [version]	USD	STEP2	[PDF] delivered in	Standard Title (Description)	Status	PDF
GB 6772-2008	English	319	Add to Cart	3 days [Need to translate]	Food additive -- Oil of lemon, cold pressed	Obsolete	GB 6772-2008
GB 6772-1986	English	199	Add to Cart	2 days [Need to translate]	Food additive--Lemon oil, cold pressed	Obsolete	GB 6772-1986

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Basic data

Standard ID	GB 6772-2008 (GB6772-2008)
Description (Translated English)	Food additive -- Oil of lemon, cold pressed
Sector / Industry	National Standard
Classification of Chinese Standard	X44
Classification of International Standard	71.100.60
Word Count Estimation	8,839
Date of Issue	2008-12-03
Date of Implementation	2009-06-01
Older Standard (superseded by this standard)	GB 6772-1986
Quoted Standard	GB/T 5009.74; GB/T 5009.76; GB/T 11540; GB/T 14454.2; GB/T 14454.4; GB/T 14454.5; GB/T 14454.6; GB/T 14454.13-2008; GB/T 14455.5
Regulation (derived from)	Announcement of Newly Approved National Standards No. 19 of 2008 (No. 132 overall)
Issuing agency(ies)	General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary	This Chinese standard specifies the food additive citric cold mill oil requirements, test methods, inspection rules, marking, packaging, transportation, storage and shelf life. This standard applies to right to citric (Citruslimon L.) fruit as raw material, cold milling, refining the resulting food additive citric cold mill oil quality analysis and evaluation.

GB 6772-2008: Food additive -- Oil of lemon, cold pressed

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food additive.Oil of lemon, cold pressed ICS 71.100.60 X44 National Standards of People's Republic of China Replacing GB 6772-1986 Food Additives cold mill lemon oil Published 2008-12-03 2009-06-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China issued

Foreword

Chapter 4 of this standard requirements are mandatory, others are recommended. This standard and the US Food Chemicals Codex FCC (Ⅴ).2004 "cold mill lemon oil," it is not equivalent. This standard replaces GB 6772-1986 "Food Additives cold mill lemon oil." Compared with this standard GB 6772-1986, the main modifications are as follows. --- added "2 Normative references" chapter; --- Added "3 Terms and Definitions" chapter; --- After evaporation the residue from the content of "1.6% to 3.9%" to "≤4.0%"; arsenic changed from "≤2 mg/kg" "≤3mg/kg"; Heavy metal content (as Pb) from the "≤5mg/kg" to "≤10mg/kg"; --- Added Appendix A typical gas chromatogram. Appendix A of this standard is an informative annex. The standard proposed by China Light Industry Federation. This standard by the National Standardization Technical Committee on Food Additives. This standard by the Shanghai Institute of Plant Chengdu spices and spice responsible for drafting. The main drafters. Ren Qimin, Zhang Xinjun, Xu Yi, Jin Qizhang. This standard supersedes the previous editions are. --- GB 6772-1986. Food Additives cold mill lemon oil Range 1 This standard specifies the food additive cold mill lemon oil requirements, test methods, inspection rules, marking, packaging, transportation, storage and security Shelf life. Quality analysis and evaluation.

2 Normative references

Terms of the following documents become provisions of this standard by reference in this standard. For dated reference documents, all later Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to agreements based on this standard Whether the latest versions of these documents. For undated references, the latest version applies to this standard. GB/T heavy metals in food additives 5009.74 limit test Determination of arsenic in food additives 5009.76 GB/T Determination GB/T 11540 perfume relative density (GB/T 11540-2008, ISO 279.1998, MOD) GB/T 14454.2 spice aroma evaluation method GB T 14454.4 Determination/perfume refractive index (GB/T 14454.4-2008, ISO 280.1998, MOD) Determination GB/T 14454.5 perfume optical rotation (GB/T 14454.5-2008, ISO 592.1998, MOD) Evaluation residue content after evaporation of perfume 14454.6 GB/T (GB/T 14454.6-2008, ISO 4715. 1978, MOD) Determination GB/T 14454.13-2008 fragrance carbonyl compound content value and a carbonyl group (ISO 1271. 1983, ISO 1279.1996, MOD) GB/T 14455.5 perfume acid value or acid content was measured (GB/T 14455.5-2008, ISO 1242.1999, MOD)

3 Terms and Definitions

The following terms and definitions apply to this standard. 3.1 Lemon oil.

4 Requirements

4.1 Appearance. yellow or greenish yellow liquid, turbid at low temperatures. 4.2 Aroma. having aroma and flavor characteristics of fresh lemon peel. 4.3 Relative density (20 ℃/20 ℃). 0.849 ~ 0.858. 4.4 Refractive index (20 ℃). 1.4740 ~ 1.4770. 4.5 Optical rotation (20 ℃). + 60 ° ~ + 68 °. After evaporation residue content 4.6. ≤4.0%. 4.7 acid value. ≤3.0. The amount of aldehyde 4.8 (citral weight). 3.0% to 5.5%. 4.9 Heavy metal content (as Pb). ≤10mg/kg. 4.10 Arsenic content. ≤3mg/kg.

5 Test methods

5.1 Appearance of test Place the specimen was observed visually than the inner tube color method. 5.2 Evaluation aroma According to the provisions of GB/T 14454.2 of. 5.3 Determination of Relative Density See provisions according to GB T/11540. 5.4 Determination of refractive index As specified in GB/T 14454.4 of. 5.5 Determination of optical rotation As specified in GB/T 14454.5 of. 5.6 Evaluation After evaporation residue content As specified in GB/T 14454.6 of. Determination of acid value 5.7 As specified in GB/T 14455.5 of. 5.8 Determination of the amount of the aldehyde-containing In a first method according 14454.13-2008 GB/T requirements. Food additives typical cold ground lemon oil gas chromatogram (area normalization method) see Appendix A. 5.9 Determination of heavy metal content (P Chou basis) As specified in GB/T 5009.74 of. Determination of arsenic content of 5.10 As specified in GB/T 5009.76 of.

6 Inspection Rules

6.1 Food additives should be cold mill lemon oil factory quality inspection department inspection, the manufacturer shall ensure that products conform to this standard Requirements, each batch of products should be accompanied by quality certificate. Like color, aroma, relative density, refractive index, optical rotation, the acid value, the amount of aldehyde Factory inspection items, and the content evaporated residue, the arsenic content, heavy metal content (as Pb) is a type test items, test every six months once. 6.2 Acceptance shall be entitled in accordance with the provisions of this standard test received product quality meets the requirements of this standard, for each batch Once acceptance, acceptance of different batches respectively. 6.3 Sampling method. batch packaging units 1 to 2, the whole pumping; 3 ~ 100 extracted 2; 100 or more further extraction increasing portion 3%. Sampling uniformly extracted from each sample 50mL ~ 100mL packing unit, the extracted sample mixed all placed within injector Mix well, respectively, into two clean and dry, inert sealed containers, protected from light. Container attach a label stating. manufacturer name, product Name, date of manufacture, batch number, quantity and date of sampling, as tested with a bottle, another bottle retained for future reference. 6.4 As a result there is an acceptance indicator does not meet the standard requirements, in conjunction with the plant extract sample was re-doubled retest. The junction reinspection If there are indicators of failure, then the product can not be accepted. 6.5 When opposition occurs both supply and demand on product quality, by mutual agreement or arbitration to resolve a legal inspection agency. 7 signs, packaging, transportation, storage and shelf life 7.1 marks Outer packaging should be marked. "food additive" word, product name, manufacturer name and address, trademark, batch number, net weight, production date And shelf life, license number and standard number. For special customer requirements, with another plant under an agreement. 7.2 Packaging Lemon oil cold grind food additives should be installed to clean a coarse taste without galvanized iron, aluminum barrel, food-grade plastic bucket, or packaging according to customer requirements. 7.3 Transport We should care, during transport, to prevent the sun and rain, not mixed with toxic and hazardous substances, transportation mix, and shall comply with the relevant departments Provisions. 7.4 Storage The product should be stored in a cool, dry, ventilated warehouse to avoid mixed air pollution, away from the fire source. 7.5 Shelf Life Subject to the conditions of storage and transportation, packaging integrity, without the unsealing of the product shelf life of one year. Late re-examine whether the operator Bonding requirements of this standard can still be used.

Appendix A

(Informative) Food additives typical gas chromatogram cold ground lemon oil (Area normalization method) A. 1 cold ground food additives typical gas chromatogram lemon oil See Figure A. 1. Figure A. 1 A. 2 operating conditions A. 2.1 Column. length 25m ~ 50m, capillary column of inner diameter of about 0.24mm. A. 2.2 Stationary Phase. PEG-20M. A. 2.3 chromatographic oven temperature. 70 ℃ thermostat 10min; then linear temperature programmed from 70 deg.] C to 120 ℃, a rate of 1 ℃/min; linear program Heated from 120 deg.] C to 180 ℃, a rate of 4 ℃/min; 180 ℃ thermostat 10min. A. 2.4 Inlet Temperature. 250 ℃. A. 2.5 Detector temperature. 250 ℃. A. 2.6 Detector. hydrogen flame ionization detector. A. 2.7 Carrier gas. nitrogen. A. 2.8 Injection volume. about 0.2μL. A. 2.9 Split ratio. 100/1.

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