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GB 30980-2014: Assessment procedure for marine dumping of dredged material
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Standard similar to GB 30980-2014

GB/T 33584.2   GB/T 33584.3   GB 18420.1   GB/T 42631   GB/T 17923   GB/T 33584.1   

Basic data

Standard ID GB 30980-2014 (GB30980-2014)
Description (Translated English) Assessment procedure for marine dumping of dredged material
Sector / Industry National Standard
Classification of Chinese Standard Z17
Classification of International Standard 07.060; 13.020.30; 13.060.01
Word Count Estimation 42,487
Date of Issue 7/24/2014
Date of Implementation 6/1/2015
Quoted Standard GB 17378.1; GB 17378.2; GB 17378.3; GB 17378.4; GB 17378.5; GB 17378.6; GB 17378.7; GB 18421
Regulation (derived from) National Standards Bulletin No. 19, 2014
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the evaluation of ocean dumping of dredged material requirements, evaluation limits, classification, chemical and biological testing methods, and dredged material disposal. This standard applies to ocean dumping of dredged material

GB 30980-2014: Assessment procedure for marine dumping of dredged material

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Assessment procedure for marine dumping of dredged material ICS 07.060; 13.020.30; 13.060.01 Z17 National Standards of People's Republic of China Ocean dumping of dredged material substance Assessment Protocol Issued on. 2014-07-24 2015-06-01 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released

Table of Contents

Preface Ⅰ 1 Scope 1 2 Normative references 1 3 Terms and definitions 4 ocean dumping of dredged material evaluation requirements 2 5 dredged material category Chemical Evaluation limit 2 6 dredged material Category 3 7 3 Dredging physical and chemical tests 8 biological tests of dredged material 4 Disposal of dredged material 9 10 11 10 Quality Control and Assurance 11 evaluation reports and report data 11 Appendix A (normative) dredged material sample collection methods and principles 12 Appendix B (normative) aqueous phase of dredged material to mysid shrimp and goby fish toxicity test experiment 15 Annex C (informative) Introduction to Biological test 18 Annex D (normative) dredged material to a solid phase Amphipoda biological toxicity test experiment 20 Appendix E (normative) bivalves of dredged material in the chemical composition of the cumulative test experiment 26 Annex F (normative) ocean dumping of dredged material inspection evaluation report 30 References 38

Foreword

The standard Chapter 4, Section 5, Chapter 6 and Chapter 9 is mandatory, the rest are recommended. This standard was drafted in accordance with GB/T 1.1-2009 given rules. This standard by the National Standardization Technical Commission for Oceanography (SAC/TC283) centralized. This standard was drafted. National Marine Environmental Monitoring Center, State Oceanic Administration, Marine Consulting Center. The main drafters of this standard. Korean Dragon, Kai Lun Yan, Han Jianbo, Wang Lijun, to the Friends of the right, Red Star Chen, Ma Yuyan, Linxin Zhen, Jingze. Ocean dumping of dredged material substance Assessment Protocol

1 Scope

This standard specifies requirements for evaluation of ocean dumping of dredged material, evaluation limits, classification, chemical and biological testing methods, and dredged material at Set mode. This standard applies in the People's Republic of China waters, territorial sea, contiguous zone, exclusive economic zone, continental shelf and under the jurisdiction of People's Republic of China Marine dredged material other waters of dumping.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document. GB 17378.1 marine monitoring Part 1. General GB 17378.2 specification for marine monitoring Part 2. Data processing and quality control analysis GB 17378.3 specification for marine monitoring Part 3. Sample collection, storage and transportation GB 17378.4 specification for marine monitoring Part 4. Seawater Analysis GB 17378.5 specification for marine monitoring Part 5. Sediment analysis GB 17378.6 specification for marine monitoring Part 6. Analysis of the organism GB 17378.7 specification for marine monitoring Part 7. Ecological survey of offshore pollution and biological monitoring GB 18421 Marine life quality

3 Terms and Definitions

The following terms and definitions apply to this document. 3.1 Environmentally sensitive areas environmentalsensitivearea Coastline and beach, sea or scenic area of great cultural and historical significance, having a particular scientific or ecological value Meaning area. Note. The specific example of protected areas, spawning grounds, seed breeding field, swimming animal migration routes, seasonal and temporary habitat, a closed military zone, seabed mining areas, Submarine cable area, area of water desalination, energy conversion area. 3.2 Dredged material dredgedmaterials For the protection of ports, terminals, waterways, use smooth passage of anchorage, port facilities and meet other sea-related construction projects need to dig out from under Deposits. 3.3 Dredged material bioassay dredgedmaterialbiologicaltesting By biological experiments directly exposed to the aqueous phase and solid phase method for dredged material to determine the biological effects of contaminants in the dredged material, according to Biological test results of dredged material to predict whether the toxicity of dredged material will harm planktonic and benthic communities. 3.4 Overlying water overlyingwater Dredged material bioassay test vessel was added solid cover experimental sea of dredged material.

4 ocean dumping of dredged material evaluation requirements

Before ocean dumping of dredged material should be carried out physical and chemical testing, the concentration of dredged material in the main chemical components and chemical categories dredged material Evaluation limit comparison, according to the classification of dredged material, dredged material to be classified. Dredged material into three categories. clean dredged material, dredging contamination And contaminated dredged material. Identified as contamination and contaminated dredged material dredging dredged material shall be three biological tests, including aqueous phase of dredged material Biological toxicity testing, biological solid dredged material toxicity testing and dredged material in the chemical composition of the cumulative test. According to the type of dredged material and Biological test results to determine the ocean disposal of dredged material. Ocean dumping of dredged material classification and evaluation process shown in Figure 1. Figure 1 ocean dumping of dredged material classification and evaluation workflow

5 categories dredged material chemical evaluation limits

Evaluation of ocean dumping of dredged material chemical limits in Table 1. Table 1 Chemical Assessment dredged material category limits Chemical composition ω/10-6 The lower limit Chemical composition ω/10-6 The lower limit Arsenic 20.0 75.0 250.0 100.0 Lead Mercury cadmium 0.80 5.0 0.30 1.0 Chromium 80.0 300.0 200.0 600.0 Zinc Copper Organic Carbon 50.0 300.0 a 2.0 4.0 Table 1 (continued) Chemical composition ω/10-6 The lower limit Chemical composition ω/10-6 The lower limit DDT sulfide 300.0 800.0 0.020 0.10 Total 500.0 1500.0 0.020 0.60 PCBs oils BHC 0.50 1.50 a unit of organic carbon 10-2.

6 dredged material classification

6.1 clean dredged material (Ⅰ class) One of the following conditions of clean dredged material dredged material. a) the content of dredged material in all chemical components does not exceed the lower limit of the evaluation of the chemical; b) dredged material in cadmium, mercury, BHC, DDT, PCBs the total does not exceed the lower limit chemical evaluation, dredged sediments arsenic, chromium, Copper, lead, zinc, organic carbon, sulfides, oils, wherein the lower limit of no more than two of them chemical content exceeds the limits of the evaluation, but not more than The average of upper and lower limits, and a particle size of less than 4μm component content of not more than 5%, less than 63μm particle size fraction containing Not more than 20%. 6.2 contamination dredged material (Ⅱ type) Dredged material in the main chemical component content does not exceed the upper limit of the chemical evaluation of dredged material and meet the following conditions for contamination Dredged material. a) dredged material in cadmium, mercury, BHC, DDT, one or more of the total content of PCBs and other chemical evaluation of exceeded limits Lower limit; b) dredged material of arsenic, chromium, copper, lead, zinc, organic carbon, sulfide, the chemical composition of oil content does not meet the physical 6.1b) provisions Claim. 6.3 contaminated dredged material (Ⅲ class) Chemical component content dredged material in one or more of the chemical than the evaluation limit of a maximum of contaminated dredged material.

7 Dredging physical and chemical tests

7.1 Determination of the project Dredged material should be carried out before dumping analytical testing must be measured at the same time, according to the historical dredging area contamination may select pollution-related Election test project analysis and detection. --- Must be measured. dredged material particle size and arsenic, cadmium, chromium, copper, lead, mercury, zinc, organic carbon, sulfides, oils; --- Selective Projects. BHC and DDT, the total amount of PCBs, PAHs, total phosphorus, total nitrogen and tributyl tin. 7.2 sample collection, transport and storage Sample collection, transport and storage methods, see Appendix A. 7.3 Chemical Methods Tributyltin and polycyclic aromatic hydrocarbons - Determination of reference Method8323/SW-846/EPA and Method8270D/SW-846/EPA, which Determination of his project by the method specified in Table 2. Table 2 Determination of chemical analysis of dredged material Project Analysis The detection limit ω/10-6 Reference Standard Arsenic Atomic Fluorescence Spectrometry 0.06 GB 17378.5 Cadmium flameless atomic absorption spectrophotometry 0.04 GB 17378.5 Chromium flameless atomic absorption spectrophotometry 2.0 GB 17378.5 Copper flameless atomic absorption spectrophotometry 0.5 GB 17378.5 Lead flameless atomic absorption spectrophotometry 1.0 GB 17378.5 Mercury atomic fluorescence spectrometry 0.002 GB 17378.5 Zinc flame atomic absorption spectrophotometry 6.0 GB 17378.5 Potassium dichromate organic carbon oxidation - reduction volumetric method - GB 17378.5 Sulfide methylene blue spectrophotometric 0.3 GB 17378.5 Oil fluorospectrophotometry 1.0 GB 17378.5 BHC a capillary gas chromatography 0.129 GB 17378.5 DDT b capillary gas chromatography 0.11 GB 17378.5 PCBs capillary gas chromatography 0.461 GB 17378.5 TP spectrophotometry - GB 17378.5 TN Kjeldahl titration - GB 17378.5 BHC and DDT and PCBs limits of detection unit 10-9. BHC refers to a detection limit of its four isomers of α-666, β-666, γ-666, δ-666 and the detection limit; b DDT detection limit refers to its three isomers pp'-DDE, pp'-DDD, pp'-DDT and the detection limit of.

8 biological tests of dredged material

8.1 General Contamination and contaminated dredged material dredging, biological testing should be done. Biological tests include the following three categories. --- The aqueous phase dredged material toxicity test. determining the dumping at sea of dredged material in the initial mixing, dissolved and suspended contaminants of raw water The potential impact thereof; --- Solid dredged material toxicity test. After determining dumping deposition potential impact on the surrounding area and its dumping of dredged material benthos; --- Dredged material in the chemical composition of biological accumulation test. to assess the cumulative Benthos from the proposed dumping of dredged material in the relevant pollutants potential. For contamination and contaminated dredged material dredged samples should also be three kinds of biological tests. 8.2 Preparation of test sample The aqueous phase test sample preparation 8.2.1 Take the dredged material and clean sea water, by volume mixing ratio 1.4, vigorously shaken or stirred for 30min after standing 1h. Remove the siphon The supernatant liquid (liquid plus suspended particles), the aqueous phase is the test sample. If the supernatant liquid is too turbid, use 0.45μm membrane filter, or The supernatant liquid was centrifuged, the supernatant is the aqueous phase test sample. 8.2.2 solid test sample preparation Take the dredged material and clean sea water, by volume mixing ratio 1.4, intense shaking or stirring 30min, the mixture was stirred well, the static Set 1h. Settlement in the end to take all the material, namely a solid phase test sample. 8.3 experimental device 8.3.1 biological culture facilities Training aircraft, culture dishes or pots, air pump, pipe, valve. 8.3.2 Toxicity test facilities Toxicity test facilities include. --- Test-bed, built-water bath, lighting, temperature control equipment and pneumatic equipment; --- Water bath, which can accommodate 60 or so 1L beaker; --- Test vessel, the general 1L beaker; --- Lighting equipment, shall ensure that the sediment surface light intensity reach 100lx; --- By the heating wire temperature control equipment and temperature control device, etc., can also be kept constant by the laboratory to complete; --- Inflatable equipment, training and experiments for benthic organisms, inflatable equipment should ensure that during inflation without disturbing the sediment or dredged material. 8.3.3 Experimental protective equipment Goggles, mask, lab coat, gloves. Laboratories should be built with an exhaust device. 8.3.4 Other equipment Refrigerated facilities, fume hood, should be equipped with generators. The aqueous phase was 8.4 dredged material toxicity test 8.4.1 The principle of selection test organisms The aqueous phase was dredged material toxicity tests using biological test should have the following conditions. --- Test organism should choose one in crustaceans, fish or bivalves and echinoderms larvae; --- Easy to obtain and the high sensitivity of larvae or larvae; --- On the reaction of toxic substances have consistency and repeatability; --- Having a more significant ecological or economic significance; --- Test organism cultured in the laboratory can be perennial or natural waters for mining. 8.4.2 Inspection Type The aqueous phase was dredged material toxicity test type and recommend suitable test organisms and their waters are shown in Table 3. Table 3 aqueous phase dredged material toxicity test type Inspection type tested biocompatible Sea 96h mysid shrimp toxicity test Huo Mysis Hoimesiellaaffinis near the Yellow Sea, East China Sea and South China Sea Neomysis each shrimp aNeomysisawatschensis China Sea 96h goby toxicity test Alligator comb goby Ctenogobiusbrevirostris East China Sea, South China Sea A creeping opalescent goby aAbomalactipes Bohai Sea, Yellow Sea and East China Sea Multi-line comb goby aCtenogobiusnotophthalmus South China Sea Bare item comb goby Ctenogobiusgymnauehen South China Sea Boleophthalmus aBoleophthalmuspectinirostris each sea area China 96h amphipod toxicity test Japan enjoys a large claws each aGrandidierellajaponica China Sea River potter wasp enjoys aCorophiumacherusicum Bohai Sea, Yellow Sea Seclusion potter wasp enjoys Corophiuminsidiosum Yellow Sea, East China Sea Bo's eyes Gammarus Ampeliscabocki Yellow Sea, East China Sea, South China Sea Shorthorn eyes each Gammarus Ampeliscabrevicornis China Sea 48h ~ 96h Dual Crustaceans or echinoderms Larvae toxicity test Each mussel bMytilusedulis China Sea Crassostrea gigas each bCrassostreagigas China Sea Rivularis bAcrassostrearivularis East China Sea, South China Sea Purple sea urchin cAnthocidariscrassipina East China Sea, South China Sea Sea Urchin cStrongylocentrotusnudus Bohai Sea, Yellow Sea Hemicentrotus cHemicentrotuspulcherrimus Bohai Sea, Yellow Sea and East China Sea a first priority of the test organism used. b from the fertilized egg to the D-shaped larvae. c from the fertilized egg to the pluteus. 8.4.3 test experiment The aqueous phase was dredged material mysid shrimp and goby fish toxicity test experiment in Appendix B. The aqueous phase was dredged material toxicity test real test for other organisms The aqueous phase was dredged material test reference mysid shrimp and goby fish toxicity test experiments. A creeping opalescent goby and shrimp Neomysis see sidebar Introduction Record C. 8.4.4 Test results to determine The aqueous phase was dredged material toxicity test results determined in Table 4. Table 4 aqueous phase dredged material toxicity test results to determine Inspection type test basis by the end criterion is not 96h mysid shrimp toxicity test 96h fish toxicity test 96h amphipod toxicity test mortality rate The average mortality rate average mortality rate of the control group and test group of dredged material difference Significant differences (p≤0.05) a; or the average mortality rate of dredged material testing large groups At 50% 48h ~ 96h or bivalve larvae of echinoderms Toxicity Test Mortality or not Normal growth rate The average mortality rate dredged material test group or normal development rate of the control group The average mortality rate of normal development or significant difference (p≤0.05) a; or sparsely The average mortality rate was dredging test group or normal development rate of more than 50% a significantly different (P≤0.05) by means of statistical methods, e.g. t- test to test. 8.5 solid dredged material toxicity test 8.5.1 selection principle of the test organisms Solid dredged material toxicity tests using biological test should have the following conditions. --- Biological test tube should be buried amphibians and amphibians optionally A; --- Effect of sediment grain size can withstand a wide range of variation; --- Responses to toxic substances with consistency and repeatability; --- Easy to obtain and the high sensitivity of larvae or larvae; --- Having a more significant ecological or economic significance; --- Test organism cultured in the laboratory can be perennial or natural waters for mining. 8.5.2 Inspection Type Solid dredged material toxicity test type and recommend suitable test organisms and their waters are shown in Table 5. Table 5 solid dredged material toxicity test type Inspection type tested biocompatible Sea 10d amphipod toxicity test Japan enjoys a chelating China Sea each River enjoys a potter wasp Bohai Sea, Yellow Sea Seclusion potter wasp enjoys the Yellow Sea, East China Sea Bo's eyes Gammarus Yellow Sea, East China Sea, South China Sea Shorthorn eyes each Gammarus China Sea 20d polychaete toxicity Japan each thorn Nereis Neanthesjaponica China Sea Polydentate Nereis Nereismultignatha Yellow Sea, East China Sea Each long kiss Nereis Glycerachirori China Sea California Roll each kiss Nereis Neohtyscaliforniensis China Sea Table 5 (Continued) Inspection type tested biocompatible Sea 10d bivalves Toxicity Thin mica clams Yoldiasimiles Bohai Sea, Yellow Sea and East China Sea Lepidolite clam Yoldialepidula South China Sea R.philippinarum aRuditapesphilippinarum each sea area China Variegated clams aRuditapesvariegate South China Sea Purple fringing white cherry clam Macomapraerupta South China Sea Beautiful white cherry clam Macomacandida South China Sea Iso-white cherry clams Macomaincongrua Bohai Sea and the Yellow Sea Yi razor each Sinonovaculaconstricta China Sea a first priority of the test organism used. 8.5.3 test experiment Solid dredged material on amphipods biological toxicity test experiment in Appendix D; solid phase for bivalves dredged material toxicity test experiment to see Appendix E. Solid dredged material to other organisms toxicity test test test reference dredged material to the solid phase or bivalves amphipod toxicity detection Test experiment. Japan chelating gossip and R.philippinarum Profile Appendix C. 8.5.4 Test results to determine Solid dredged material toxicity test results determined in Table 6. Table 6 solid dredged material toxicity test results to determine Inspection type test basis by the end criterion is not 10d end isopods Toxicity Test mortality rate The average mortality rate difference with the control group the average mortality rate of dredged material test was significantly (p≤ 0.05) a; average mortality or dredged material test group more than 50% 20d polychaetes Toxicity Test Growth (dry weight) b The average difference in mean dry weight dry weight of the control group of dredged material test was significantly (p≤ 0.05) a; or dredged material test group the mean dry weight of the difference between the average dry weight of the control group of large At 30% 10d bivalve Toxicity Test mortality rate The average mortality rate difference with the control group the average mortality rate of dredged material test was significantly (p≤ 0.05) a; average mortality or dredged material test group more than 50% a significantly different (P≤0.05) should, for example, be determined by the statistical t- test methods. b is the total dry weight of the dry animal deaths and disappearances after deduction of weight. Biological 8.6 dredged material in the chemical composition of the cumulative test 8.6.1 The principle of selection test organisms Dredged material in biological chemical components used in the test biological accumulation test should have the following conditions. --- Biological test tube should be buried amphibians and amphibians optionally A; --- Can provide adequate tissue for biological contaminants analysis; --- Not effectively metabolize pollutants, especially organic pollutants; --- Having a more significant ecological or economic significance; --- Test organism cultured in the laboratory can be perennial or natural waters for mining. 8.6.2 Inspection Type Dredged material in the chemical components of biological accumulation inspection type and recommend suitable test organisms and their waters are shown in Table 7. Table 7 biological dredged material in the chemical composition of cumulative inspection type Inspection type tested biocompatible Sea 28d bivalves accumulation experiment Thin mica clams Bohai Sea, Yellow Sea and East China Sea Lepidolite clam South China Sea R.philippinarum a Chinese each sea area Variegated clams a South China Sea Purple fringing white cherry clam South China Sea Beautiful white cherry clam South China Sea Iso-white cherry clams Bohai Sea and Yellow Sea Yi razor China Sea each 28d polychaete accumulation experiment Japan each thorn Nereis China Sea Yellow Sea and East China Sea multidentate Nereis a first priority of the test organism used. 8.6.3 test experiment Bivalves cumulative test experiment dredged material in the chemical composition, see Appendix E. 8.6.4 Test results to determine Biological dredged material in the chemical composition of the cumulative test results determined in Table 8. Table 8 dredged material in the chemical composition of bioaccumulation test results judgment Inspection type test basis by the end criterion is not 28d bivalves Cumulative test The cumulative amount of pollutants in the body Shellfish experimental group one or more contaminants at concentrations greater than specified in GB 18421 Ocean Shellfish quality standard value of a 28d polychaete Cumulative test The cumulative amount of pollutants in the body The cumulative amount of pollutants in the body of pollutants in vivo cumulative amount of dredged material test group and the control group The difference was significant (p≤0.05) b a marine shellfish quality standard value determined in accordance with the use of functional categories and environmental objectives Dumping area where waters. b significantly different (P≤0.05) should, for example, be determined by the statistical t- test methods.

9 Disposal of dredged material

9.1 dredged material disposal Dredged material disposal methods include. direct dumping; dumping restrictions; after special disposal restrictions dumping; land or other special place Set mode. 9.2 clean dredged material disposal For clean dredged material can be dumped in the designated area. 9.3 contamination of dredged material disposal For dredged material contamination, the aqueous phase and solid phase toxicity tests and bioaccumulation tests all pass directly dumped in the designated areas. Three kinds of biological toxicity test if one verification has not been passed, there may be restrictions in designated areas of the dumping. Three kinds of biological toxicity test, there are two (Includes two) than without such dredged material should be subject to special treatment, it can be limited dumped in designated areas. 9.4 Disposal of contaminated dredged material For contaminated dredged material, the aqueous phase and solid phase toxicity tests and bioaccumulation tests all pass, or only one test has not been passed, this Class of dredged material should be subject to special treatment, it can be limited dumped in designated areas. Contaminated dredged material aqueous phase and solid phase toxicity tests and bioaccumulation test, there are two (includes two) or more test has not been passed, such Ocean dumping of dredged material should in principle, should be disposed of on land. Ruoyin irresisti...

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