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US$169.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB 28313-2012: Food additives -- Grape skin red Status: Valid
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Food additives -- Grape skin red
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GB 28313-2012
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Basic data | Standard ID | GB 28313-2012 (GB28313-2012) | | Description (Translated English) | Food additives -- Grape skin red | | Sector / Industry | National Standard | | Classification of Chinese Standard | C54;X40 | | Classification of International Standard | 67.220.20 | | Word Count Estimation | 7,753 | | Regulation (derived from) | Ministry of Health Bulletin No. 7 of 2012 | | Issuing agency(ies) | Ministry of Health of the People's Republic of China | | Summary | This Chinese standard applies to grape skin or grape juice as the main raw material of the skin residue, extracted by water or edible alcohol, refined food additive grape skin red. Its main component is anthocyanin coloration. Red grape skin products may |
GB 28313-2012: Food additives -- Grape skin red---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food gets.Grape skin red
National Standards of People's Republic of China
National standards for food safety
Food additives grape skin red
2012-04-25 release
2012-06-25 Implementation
Issued by the Ministry of Health of the People's Republic of China
National standards for food safety
Food additives grape skin red
1 Scope
This standard applies to grape skin or grape juice after the skin as the main raw material, by water or edible ethanol extraction, refined food Tim
Plus grape skin red. Its main coloring composition is anthocyanin. Grape skin red products can contain dextrin and other accessories.
2 formula, structural formula
2.1 Molecular formula
Peony flower anthocyanin. C16H13O6X
Mallow pigment. C17H15O7X
Fenghua anthocyanin. C15H11O7X
Morning glaucoma anthocyanin. C16H13O7X
X-. acid group
2.2 Structural formula
Peony anthocyanin. R = OCH3; R '= H
Mallow pigment. R, R '= OCH3
Fenghua anthocyanin. R, R '= OH
Morning glaucoma. R = OCH3; R '= OH
3 technical requirements
3.1 sensory requirements. should be consistent with the provisions of Table 1.
Table 1 sensory requirements
The project requires a test method
Odorless or slightly odorous
Color red to purple
Traits of powder, granules or liquids
Take the appropriate amount of sample in a clean, dry white porcelain dish. in natural light,
Observe the color, traits; in the absence of odor environment, smell the smell
3.2 Physical and chemical indicators. should be consistent with the provisions of Table 2.
Table 2 Physical and chemical indicators
project
index
Powder or granular liquid
Testing method
Color Price E1 m (515 ~ 535) nm Compliant in Appendix A A.3
Dry reduction, w /% ≤ 8.0 - GB 5009.3 direct drying method
Sulfur dioxide/(mg/kg) ≤ 500 (converted in terms of one color) Appendix A A.4
Total arsenic (in As)/(mg/kg) ≤ 3 GB/T 5009.11
Lead (Pb)/(mg/kg) ≤ 2 GB 5009.12
Note. Commercial grape skin red products should be in line with this standard grape skin red as raw material, can be made of edible dextrin made, the color price indicators in line with claims.
Appendix A
Testing method
A.1 General provisions
The reagents and water used in this standard, when not specified in other requirements, refer to the analysis of pure reagents and GB/T 6682-2008 in the provisions of the three
Water level. Standard titration solution used in the test, the standard solution for the determination of impurities, preparations and products, without any other requirements,
GB/T 601, GB/T 602, GB/T 603. The solution used in the test refers to water when it is not specified with the formulation of the solvent
Solution.
A.2 Identification test
A.2.1 Maximum absorption peak
Take the sample 0.1g, with pH3.0 citric acid - disodium hydrogen phosphate buffer solution and diluted to 100mL, the sample solution in the 515nm ~
535nm range has the largest absorption peak.
A.2.2 Color response
Take 0.1g sample, dissolved in 50mL water, the solution was red ~ purple, in the solution by adding sodium hydroxide solution (4.3g hydroxide
Sodium dissolved in 100mL water), the solution color to blue or dark green.
A.3 Determination of color price
A.3.1 Reagents and materials
A.3.1.1 0.2mol/L disodium hydrogen phosphate solution. accurately charged disodium hydrogen phosphate (Na2HPO4 · 12H2O) 71.64g, dissolved in water
And set to 1000mL.
A.3.1.2 0.1mol/L citric acid solution. 21.01 g of citric acid (C6H8O7 · H2O) was accurately weighed and dissolved in water and allowed to
1000mL.
A.3.1.3 pH3.0 citric acid - disodium hydrogen phosphate buffer solution. take 0.2mol/L disodium hydrogen phosphate solution 4.11mL and 0.1mol/L
Citric acid solution 15.89mL mixed.
A.3.2 Instruments and equipment
Spectrophotometer.
A.3.3 Analysis steps
Weigh 0.1g ~ 0.2g sample, accurate to 0.0001g, with pH3.0 citric acid - disodium hydrogen phosphate buffer solution, transferred to
100mL volumetric flask, add pH3.0 citric acid - disodium hydrogen phosphate buffer solution volume to the scale, shake. Take this sample solution at 1cm
Pigment, pH3.0 citric acid - disodium hydrogen phosphate buffer solution as a blank control, with a spectrophotometer in the range of 515nm ~ 535nm
Of the maximum absorption wavelength measured absorbance (absorbance should be controlled between 0.3 to 0.7, otherwise it should adjust the concentration of sample solution, and then re-determination
Absorbance).
A.3.4 Calculation of results
The color of the test sample concentration of 1%, with 1cm cuvette, in the range of 515nm ~ 535nm maximum absorption wavelength measured at the suction
Luminosity E1 m (515 ~ 535) nm, calculated according to formula (A.1).
E1 m (515 to 535) nm = Ac ×
(A.1)
Where.
A --- the actual determination of the sample solution of the absorbance value;
c - the value of the test solution concentration in grams per milliliter (g/mL).
The experimental results are based on the arithmetic mean of the parallel measurement results. The absolute difference between the two independent determinations obtained under repeatability conditions
The value is not greater than 2.5%.
A.4 Determination of sulfur dioxide
A.4.1 Method of measurement
The total sulfur dioxide content (x) in the sample was measured by the second distillation method in GB/T 5009.34 and then calculated in accordance with A.4.2
The formula is converted to the sulfur dioxide content (y) at a color price.
A.4.2 Result calculation
The sulfur dioxide content is expressed in mg/kg in terms of the sulfur dioxide mass fraction y in a color product, according to the formula (A.2)
Calculate.
y = x x 1000E1 m (515 to 535) nm
(A.2)
Where.
x --- Total amount of sulfur dioxide in the sample measured according to the second method of distillation in GB/T 5009.34,
Per gram per gram (g/kg);
1000 --- unit conversion factor;
E1 m (515 ~ 535) nm --- the color of the sample to be tested.
The experimental results are based on the arithmetic mean of the parallel measurement results. The absolute difference between the two independent determinations obtained under repeatability conditions
The value must not exceed 10% of the arithmetic mean.
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