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GA/T 1601-2019: Forensic sciences--Examination methods for fentanyl in biological samples-LC-MS
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Forensic sciences--Examination methods for fentanyl in biological samples-LC-MS
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GA/T 1601-2019
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Basic data | Standard ID | GA/T 1601-2019 (GA/T1601-2019) | | Description (Translated English) | Forensic sciences--Examination methods for fentanyl in biological samples-LC-MS | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.310 | | Word Count Estimation | 10,152 | | Date of Issue | 2019 | | Date of Implementation | 2019-12-01 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1601-2019: Forensic sciences--Examination methods for fentanyl in biological samples-LC-MS---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences--Examination methods for fentanyl in biological samples-LC-MS
ICS 13.310
A92
Public Safety Industry Standards of the People's Republic of China
Fentanyl test in forensic scientific biological materials
Liquid chromatography-mass spectrometry
Published on October 14,.2019
2019-12-01 Implementation
Issued by the Ministry of Public Security of the People's Republic of China
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some content of this document may involve patents. The issuer of this document does not assume responsibility for identifying these patents.
This standard was proposed by the National Toxic Analysis Subcommittee of Criminal Technical Standardization Technical Committee (SAC/TC179/SC1) and
Be in charge.
This standard was drafted by. Physical Evidence Appraisal Center of the Ministry of Public Security, Hangzhou Public Security Judicial Appraisal Center.
The main drafters of this standard. Dong Ying, Wang Ruihua, Luan Yujing, Ren Xinxin, Song Ge, Dong Linpei, Yu Zhongshan, He Yi, Wang Fanglin, Zhang Leiping,
Chang Jing, Wang Jiong, Zhang Yunfeng, Ying Jianbo, Zhuo Xiaocong, Li Xiaofei, Tian Guogang.
Fentanyl test in forensic scientific biological materials
Liquid chromatography-mass spectrometry
1 Scope
This standard specifies the liquid chromatography-mass spectrometry (LC-mass spectrometry) of fentanyl in forensic biological samples (blood, urine, liver, kidney, stomach and stomach contents, etc.)
MS) qualitative and quantitative test method.
This standard applies to the qualitative and quantitative analysis of fentanyl in forensic biological samples. Qualification of fentanyl in other suspicious samples
Analysis and quantitative analysis can refer to use.
2 Normative references
The following documents are essential for the application of this document. For dated references, only the dated version applies to this article
Pieces. For the cited documents without date, the latest version (including all amendments) applies to this document.
GB/T 6682 Analysis laboratory water specifications and test methods
GA/T 122 Nomenclature of poison analysis
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principle
Use blank samples and added samples as controls, and extract, purify, and concentrate biological samples in accordance with the requirements of parallel operation.
Qualitative quantification of spectrum-mass spectrometry, with retention time, characteristic ion fragment peak of mass spectrometry and relative abundance ratio as the basis for qualitative judgment; based on peak area
According to data, quantitative analysis was performed using external standard method.
5 Reagents and materials
5.1 Reagent
The experimental water shall comply with the first-grade water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis are of analytical grade,
Reagents include.
a) Methanol (chromatographically pure);
b) Acetonitrile (chromatographically pure);
c) ammonia water;
d) hydrochloric acid;
e) ammonium acetate;
f) Standard solution.
1) 1.0mg/mL standard substance solution. After conversion to fentanyl standard substance purity and salt type, prepare 1.0mg/mL with methanol
The standard substance solution of fentanyl was stored in the refrigerator for a period of 6 months. Or use a commercially available standard solution.
2) 0.1mg/mL standard working solution. Pipette 1.0mg/mL standard substance solution 1.0mL and dilute with methanol to
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