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US$649.00 · In stock Delivery: <= 5 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 3845-2014: Determination of multiple synthetic dyes in bottom material of chafing dish for export Status: Valid
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| SN/T 3845-2014 | English | 649 |
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Determination of multiple synthetic dyes in bottom material of chafing dish for export
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SN/T 3845-2014
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Basic data | Standard ID | SN/T 3845-2014 (SN/T3845-2014) | | Description (Translated English) | Determination of multiple synthetic dyes in bottom material of chafing dish for export | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | X04 | | Classification of International Standard | 67.050 | | Word Count Estimation | 25,255 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine | | Issuing agency(ies) | General Administration of Customs | | Summary | This Standard specifies the pot at the end export a variety of synthetic pigment compound liquid chromatography detection methods. This Standard applies to pot bottom feed new red, amaranth red, carmine, the temptation to red, erythrosine, sunset yellow, |
SN/T 3845-2014: Determination of multiple synthetic dyes in bottom material of chafing dish for export ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of multiple synthetic dyes in bottom material of chafing dish for export
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Determination of synthetic pigment feed export hot pot more
Issued on. 2014-01-13
2014-08-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
Please note that some of the content of this document may involve patents. Distribution of this document
Institutions do not assume the responsibility to identify these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. Chongqing, People's Republic of China Exit Inspection and Quarantine.
The main drafters of this standard. Xi significant deposit, Tang Bobin, Zhang Lei, Lixian Liang, Zheng Xiaoling, Wang Guomin Li Ying State.
Determination of synthetic pigment feed export hot pot more
1 Scope
This standard specifies the pot at the end of export feed more synthetic pigment liquid chromatography detection methods.
This standard applies to hot pot feed new red, amaranth red, carmine, the temptation to red, erythrosine, sunset yellow, Acid Red G, acidic red GR,
Rhodamine B, Para Red, Sudan Ⅰ, Sudan Ⅱ, Determination of Sudan Ⅲ, Sudan Ⅳ, Sudan and Sudan Orange G and 7B.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
3 Method summary
The sample was melted at 60 ℃, washed with methanol - extracted sample mixed solution of acetone and methanol and urea solution (containing 5% aqueous ammonia solution)
Synthetic pigment, after liquid-liquid extraction distribution respectively through a polyamide resin column chromatography and gel permeation chromatography purification, liquid chromatography, external standard peak area
Statutory amount.
4 Reagents and materials
Unless otherwise specified, the reagents were of analytical grade water as a water GB/T 6682 regulations.
4.1 Methanol. HPLC fractions.
4.2 acetone. HPLC fractions.
4.3 ethyl acetate.
4.4 cyclohexane.
4.5 phosphoric acid.
4.6 urea.
4.7 Ammonia. a concentration of 28%.
4.8 Anhydrous sodium dihydrogen phosphate.
4.9 sodium phosphate dibasic anhydrous.
4.10 methanol - acetone solution (11 volume). The volume of methanol (4.1) and acetone (4.2), and other mixed.
4.11 ethyl acetate - cyclohexane (11, volume ratio). Ethyl acetate (4.3), and cyclohexane (4.4) uniformly mixed in equal volumes.
4.12 80% methanol solution (containing 0.1% phosphoric acid). Take 80mL of methanol (4.1), was added 0.1mL phosphoric acid (4.5), dilute with water to 100mL.
4.13 2mol/L methanol solution of urea (containing 5% aqueous ammonia solution). Weigh 12g of urea (4.6), was dissolved in methanol (4.1), was added 5mL ammonia
Water (4.7), dilute to 100mL with methanol (4.1).
4.14 50% phosphoric acid. An equal volume of phosphoric acid (4.5) mixed with water uniformly.
4.15 0.1% phosphoric acid solution. Pipette 0.1mL phosphate (4.5), diluted with water to 100mL.
4.16 5% ammonia - methanol solution. amount of 5mL ammonia (4.7) and 95mL of methanol (4.1), mix well.
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