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HYT0283-2020: Determination of cadmium in seawater - Atomic fluorescence spectrometry
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| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| HY/T 0283-2020 | English | 139 |
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Determination of cadmium in seawater - Atomic fluorescence spectrometry
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HY/T 0283-2020
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Basic data | Standard ID | HY/T 0283-2020 (HY/T0283-2020) | | Description (Translated English) | Determination of cadmium in seawater - Atomic fluorescence spectrometry | | Sector / Industry | Marine Industry Standard (Recommended) | | Classification of Chinese Standard | Z10 | | Classification of International Standard | 07.060; 13.060 | | Word Count Estimation | 6,672 | | Date of Issue | 2020-05-29 | | Date of Implementation | 2020-09-01 | | Issuing agency(ies) | Ministry of Natural Resources of the People's Republic of China | HYT0283-2020: Determination of cadmium in seawater - Atomic fluorescence spectrometry---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of cadmium in seawater - Atomic fluorescence spectrometry
ICS 07.060;13.060
Z10
People's Republic of China Marine Industry Standard
Determination of cadmium in sea water by atomic fluorescence method
2020-05-29 release
2020-09-01 Implementation
Issued by the Ministry of Natural Resources of the People's Republic of China
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard was proposed by the Tianjin Seawater Desalination and Comprehensive Utilization Research Institute of the Ministry of Natural Resources.
This standard is under the jurisdiction of the National Marine Standardization Technical Committee (SAC/TC283).
Drafting organizations of this standard. Tianjin Seawater Desalination and Comprehensive Utilization Institute of Ministry of Natural Resources, National Seawater and Brackish Water Utilization Product Quality Supervision
Inspection Center, Tianjin Marine Environment Monitoring Center Station of State Oceanic Administration.
The main drafters of this standard. Li Yanping, Liu Xiaoqi, Tu Jianbo, Wang Cuicui, Zhao Jianchao, Hao Jun, Pan Xianhui, Zhang Qiufeng, He Rong, Xu Guanqiu,
Liu Yang.
Determination of cadmium in sea water by atomic fluorescence method
1 Scope
This standard specifies the atomic fluorescence determination method for cadmium in seawater.
This standard is applicable to the determination of the soluble cadmium content in the discharge water produced by ocean, nearshore, estuarine seawater and seawater utilization.
The detection limit of cadmium is 0.012μg/L, and the detection limit is 0.040μg/L.
2 Normative references
The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this article
Pieces. For undated references, the latest version (including all amendments) applies to this document.
GB/T 6682 Analytical laboratory water specifications and test methods
GB 17378.3 Marine Monitoring Specification Part 3.Sample Collection, Storage and Transportation
3 Principle
Under acidic conditions, the cadmium in the water sample reacts with potassium borohydride to generate volatile cadmium, which is carried into the quartz atomizer by the carrier gas.
The cadmium hollow cathode lamp produces atomic fluorescence under the excitation, and its fluorescence intensity is proportional to the concentration of cadmium in the measured solution within a certain range, and
The standard series are relatively quantitative.
4 Reagents and materials
In the analysis method, except for special regulations, all superior grade pure reagents and secondary water complying with GB/T 6682 are used.
4.1 Nitric acid (HNO3). ρ=1.42g/mL.
4.2 Nitric acid solution (1 1). 1 volume of nitric acid (4.1) is mixed with 1 volume of water.
4.3 Nitric acid solution (1 99). 1 volume of nitric acid (4.1) is mixed with 99 volumes of water.
4.4 Hydrochloric acid (HCl). ρ=1.19g/mL.
4.5 Cobalt solution (0.10mg/mL-Co). Weigh 0.4038g of cobalt chloride hexahydrate (CoCl2 6H2O), dissolve it in a small amount of water, and dilute
To 100mL, shake well and set aside. Dilute 10 times to 0.10mg/mL before use.
4.6 Thiourea solution (10g/L). Weigh 1.0g of thiourea (CH4N2S), dissolve it in water, and dilute to 100mL.
4.7 Sodium pyrophosphate solution. Weigh 2.0g of sodium pyrophosphate (Na4P2O7·10H2O), dissolve in water, and dilute to 100mL.
4.8 Potassium borohydride solution (40g/L). Weigh 1.25g potassium hydroxide (KOH) and dissolve it in a small amount of water, add potassium borohydride (KBH4) 10.0
g, dilute with water to 250mL, shake well, prepare before use.
4.9 Carrier. Pipette 7.6mL hydrochloric acid (4.4) into a small amount of water, add 10mL cobalt solution (4.5), dilute with water to 500mL, shake well for use.
4.10 Cadmium standard stock solution (1.00g/L-Cd). Weigh 0.5000g of metallic cadmium (purity 99.99%) and heat it with 5mL nitric acid solution (4.2)
Dissolve, transfer to a 500mL volumetric flask after cooling, dilute to the mark with nitric acid solution (4.3), shake well. National certified standard material solutions can also be used.
4.11 Cadmium standard intermediate solution (10.0mg/L). Use a single mark pipette to pipette 5mL cadmium standard stock solution (4.10) into a 500mL volumetric flask
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