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| GB/T 5211.11-2008 | English | 114 |
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Determination of water-soluble sulfates, chlorides and nitrates of pigments
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GB/T 5211.11-2008
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| GB/T 5211.11-1986 | English | 199 |
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Determination of water-soluble sulfates chlorides and nitrates of pigments
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GB/T 5211.11-1986
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Basic data | Standard ID | GB/T 5211.11-2008 (GB/T5211.11-2008) | | Description (Translated English) | Determination of water-soluble sulfates, chlorides and nitrates of pigments | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | G53 | | Classification of International Standard | 87.060.10 | | Word Count Estimation | 6,627 | | Date of Issue | 2008-06-04 | | Date of Implementation | 2008-12-01 | | Older Standard (superseded by this standard) | GB/T 5211.11-1986 | | Quoted Standard | GB/T 3186 | | Adopted Standard | ISO 787-13-2002, IDT | | Regulation (derived from) | Announcement of Newly Approved National Standards 2008 No. 9 (No. 122 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the determination of the water soluble pigment samples sulfates, chlorides and nitrates generic test methods. |
GB/T 5211.11-2008: Determination of water-soluble sulfates, chlorides and nitrates of pigments---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of water-soluble sulfates, chlorides and nitrates of pigments
ICS 87.060.10
G53
National Standards of People's Republic of China
GB/T 5211.11-2008/ISO 787-13.2002
Replacing GB/T 5211.11-1986
Soluble pigment sulfate,
Determination of chloride and nitrate
(ISO 787-13.2002, Generalmethodsoftestforpigments
andextenders-Part 13. Determinationofwater-soluble
sulfates, chloridesandnitrates, IDT)
Posted 2008-12-01 2008-06-04 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This part identical with ISO 787-13.2002 "pigments and extenders - Common test methods - Part 13. Water-soluble sulfate, chloride,
Matter and nitrate determination "(in English).
GB/T 5211 Test methods for pigments series of standards is listed below a series of standard components.
--- Part 1. Determination of matter soluble pigments cold extraction method
--- Part 2. Determination of matter soluble pigment heat extraction method
--- Part 3. Determination of paint at 105 ℃ volatiles
--- Part 4. Determination of volume and apparent density pigment loading
--- Part 5. Determination of resistance paint
--- Part 11. soluble pigment sulfate, chloride and nitrate determination
--- Part 12. Determination of resistivity of aqueous extract of pigments in
Determination of pH aqueous extract of pigments. Part --- 13
--- Part 14. Determination of residue on sieve pigment Mechanical flushing procedure
--- Part 15. Determination of oil absorption pigment
Comparison of white pigments achromatic force. --- Section 16
--- Part 17. Comparison of white pigment ratio (hiding power) of
--- Part 18. Determination of pigment sieve residue of water law manual
--- Part 19. Determination of relative tinting strength of colored pigments and color dilute visual comparison
--- Part 20. The character system, white, black and colored pigments colors comparative colorimetric
This section GB/T 5211 Part 11.
This Part replaces GB/T 5211.11-1986 "aqueous pigment sulfate, chloride and nitrate determination."
This part of the previous version GB/T 5211.11-1986 main technical differences are as follows.
--- Changing the concentration of hydrochloric acid;
--- Change the volume of hydrochloric acid was added in 6.1 and 8.1.
This part is proposed by the China Petroleum and Chemical Industry Association.
This part of the National Standardization Technical Committee and the pigment coating (SAC/TC5) centralized.
This section drafted by. CNOOC Changzhou coating Chemical Research Institute.
The main drafters of this section. Chen Gang.
This section was first issued in 1986.
GB/T 5211.11-2008/ISO 787-13.2002
Soluble pigment sulfate,
Determination of chloride and nitrate
1 Scope
This section provides for the determination of water soluble sulfate pigment samples, Common test methods for chloride and nitrate.
Note. The general test method is applicable to specified pigment or extender pigment, as long as the inclusion of the pigment or an extender pigment product standards refer to this part of the article
Models, and indicate the characteristics of the product due to the need to make changes. Only when this generic method does not apply to a specific product, it should provide for a special party
Method to determine.
2 Normative references
The following documents contain provisions cited by GB/T 5211 to the present, constitute provisions of this section. For dated reference documents
Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section
Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this
section.
GB/T 3186 Paints, varnishes and raw materials for paints and varnishes - Sampling (GB/T 3186-2006, ISO 15528.2000, IDT)
3 Reagents
The reagents used were of analytical grade, use distilled water or distilled water equivalent purity water.
3.1 HCl. ρ = 1.18g/mL.
Silver nitrate 3.2. 0.01mol/L standard solution.
3.3 ammonium chloride solution. 17.2mg/L.
3.4 Sodium hydroxide solution.200g/L.
3.5 barium chloride. 50g/L.
3.6 Potassium chromate solution. 50g/L.
Deva 3.7 Jorda (Devarda) alloy powder.
3.8 Nessler (of Nessler) reagents, according to methods a) or b) Preparation.
a) 5g of potassium iodide dissolved in 3.5mL, add cold saturated mercury (HgCl2) chloride solution, stirring until pale red precipitate is generated
So far, was added and stirring was continued at 40mL of potassium hydroxide (500g/L), diluted with water to 100mL, mixing evenly, standing, and pour out
The supernatant was stored in the dark.
b) in 80mL of water was dissolved 3.5g of potassium iodide and 1.25g of mercuric chloride (HgCl2), the addition of cold saturated mercuric chloride (HgCl2) solution,
Sway to have a reddish precipitate formed, then add 12g of sodium hydroxide, shaken until dissolved, and finally add a little saturated mercuric chloride solution
Solution and diluted with water to 100mL, shaking from time to time in a few days and then allowed to settle, supernatant of the test.
4 Instrument
In addition to conventional instruments, but still need the following instruments.
4.1 Sintered filter silica crucible, P10 or of P16 porosity (pore size 4μm ~ 16μm).
Note. Also available with similar porosity glass filter.
4.2 Nessler (Nessler) colorimetric tube capacity 50mL.
4.3 Distillation equipment.
GB/T 5211.11-2008/ISO 787-13.2002
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