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General methods of test for pigments and extenders - Part 14: Determination of residue on sieve - Mechanical flushing procedure
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GB/T 5211.14-1988 | English | 199 |
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Determination of residue on sieve of pigment. Mechanical flushing procedure
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Basic data Standard ID | GB/T 5211.14-2021 (GB/T5211.14-2021) | Description (Translated English) | General methods of test for pigments and extenders - Part 14: Determination of residue on sieve - Mechanical flushing procedure | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | G53 | Word Count Estimation | 14,179 | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration |
GB/T 5211.14-2021: General methods of test for pigments and extenders - Part 14: Determination of residue on sieve - Mechanical flushing procedure ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
General methods of test for pigments and extenders - Part 14.Determination of residue on sieve - Mechanical flushing procedure
ICS 87.060.10
CCSG53
National Standards of People's Republic of China
Replace GB/T 5211.14-1988
General test methods for pigments and extender pigments
Part 14.Determination of the residue on the sieve, mechanical flushing method
(ISO 787-18.1983,Generalmethodsoftestforpigmentsandextenders-
Released on 2021-08-20
2022-03-01 implementation
State Administration of Market Supervision and Administration
Issued by the National Standardization Management Committee
Foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
Drafting.
This document is part 14 of GB/T 5211.GB/T 5211 has released the following parts.
---Cold extraction method for determination of water-soluble pigments;
---Pigment water soluble matter determination thermal extraction method;
---General test methods for pigments and extenders. Part 3.Determination of volatiles at 105°C;
---Determination of pigment filling volume and apparent density;
---Pigment resistance test method;
---General test methods for pigments and extender pigments Part 6.Determination of pH value of aqueous suspension;
---Determination of pigment water-soluble sulfate, chloride and nitrate;
---Determination of electrical resistivity of pigment water extract;
---Determination of pH of pigment water extract;
--- General test methods for pigments and extender pigments. Part 14.Determination of sieve residues. Mechanical flushing method;
--- General test methods for pigments and extender pigments Part 15.Determination of oil absorption;
---Comparison of the decoloring power of white pigments;
---Comparison of white pigment contrast ratio (hiding power);
--- General test methods for pigments and extender pigments. Part 18.Determination of residue on sieve water method (manual operation);
--- Visual comparison method for determination of relative tinting strength and diluted color of colored pigments;
---Comparative chromaticity method for the colors of white, black and colored pigments in the natural color system.
This document replaces GB/T 5211.14-1988 "Mechanical Flushing Method for the Determination of Pigment Sieve Residues", and is consistent with GB/T 5211.14-1988
In addition to structural adjustments and editorial changes, the main technical changes are as follows.
---The normative reference document "GB/T 6005" was added, and "GB 9285" was changed to its revised version "GB/T 3186" (see Chapter 2, 1988
Chapter 2 of the Year Edition);
---Changed terms and definitions (see 3.1, Chapter 3 of the 1988 edition);
--- Deleted the content about pressurized tap water injection (see 5.1 in the 1988 edition);
---The material and size requirements of the container have been added (see 6.1.2); the water flow requirements have been changed (see 6.1.3, 6.1.2 of the 1988 edition),
The content of the test sieve requirements (see 6.1.4, 6.1.3 of the 1988 edition), the description and requirements of the accuracy of the balance (see 6.3, the 1988 edition of 6.1.3)
6.3);
---Changed the preparation method of the dispersion (see 8.3, 7.2 of the 1988 edition); added the judgment that the fine particles almost completely pass the test sieve
The method and the requirements for recording the corresponding time (see 8.4.1); added that if the sieve residue contains foreign matter, its storage should be recorded.
In and nature of the provisions (see 8.5);
---Changed the provisions of test data processing (see Chapter 9, Chapter 8 of the 1988 edition);
---Change the content of the test report (see Chapter 10, Chapter 9 of the 1988 edition).
This document uses the redrafting method to amend and adopt ISO 787-18.1983 ``General Test Methods for Pigments and Extender Pigments Part 18.Sieve
Determination of residue by mechanical flushing method.
Compared with ISO 787-18.1983, this document is different in structure. Appendix A lists the differences between this document and ISO 787-18.1983.
A list of chapter number comparisons.
Compared with ISO 787-18.1983, this document has technical differences.
The vertical single line (|) of the position is marked, and the corresponding technical differences and their reasons are listed in Appendix B.
The following editorial changes have been made to this document.
---Changed the file name, in order to be consistent with the existing standard numbering method, the file name was changed to "Pigment and Extender Pigment General Test Method
Method Part 14.Determination of Sieve Residues Mechanical Flushing Method.
Please note that some of the contents of this document may involve patents. The issuing agency of this document is not responsible for identifying patents.
This document was proposed by the China Petroleum and Chemical Industry Federation.
This document is under the jurisdiction of the National Standardization Technical Committee for Coatings and Pigments (SAC/TC5).
Drafting organizations of this document. CNOOC Changzhou Coating Chemical Research Institute Co., Ltd., Shandong Dongjia Group Co., Ltd., Anhui Shenlanhua
Color Material Co., Ltd., Baihe Group Co., Ltd., Changsha Zuxing New Material Co., Ltd., Yixing Huayi Yipin Coloring Technology Co., Ltd.
Company, Shuangle Pigment Taixing City Co., Ltd., Yinchuan Baihong New Material Technology Co., Ltd., Dragon Mang Baililian Group Co., Ltd., Hefei Xu
Yang Aluminum Pigment Co., Ltd., Zhejiang Huayuan Pigment Co., Ltd., Anshan Qicai Chemical Co., Ltd., Longkou United Chemical Co., Ltd.,
Anhui Linghu Paint Co., Ltd., Biaogeda Precision Instrument (Guangzhou) Co., Ltd., Fujian Wanan Industrial Group Co., Ltd., Xuzhou Daguangtu
Material Factory, Dongguan Dabao Chemical Products Co., Ltd., Meichao Group Co., Ltd., Zhejiang Mingquan Industrial Coating Co., Ltd., Deqing County Jinqiu Plastic Powder
Co., Ltd., Zhejiang Tianhe Resin Co., Ltd., Shunde Vocational and Technical College, Pushen Testing Instrument (Shanghai) Co., Ltd., Guohengxin (Changzhou) Testing
Certification Technology Co., Ltd., Fujian Tenglong Industrial Company, Huierming (Fujian) Chemical Industry Co., Ltd., Zhangzhou Xianghao Paint Industry and Trade Co., Ltd.
Limited company.
The main drafters of this document. Wu Zhiping, Li Huaquan, Xu Zaihan, Xiong Yongke, Zeng Mengjin, Cai Yun, Zhao Qin, Wang Binbin, Ma Yanping, Dong Qiannian,
Li Jinhua, Li Yan, Ji Wei, Zhou Lei, Wu Zuogui, Suna, Huang Wen, Ling Xiao, Cai Yanru, Shan Xiaogang, Mao Li'an, Li Ka-shing, Ma Yong, Chen Yanwu, Sun Dewang,
Huang Wanglie, Fang Bin, Cai Dehe.
The previous releases of this document and the documents it replaced are as follows.
---First published in 1988 as GB/T 5211.14-1988;
---This is the first revision.
Introduction
GB/T 5211 is a series of standards for general test methods for pigments and extender pigments. Due to historical reasons, the names of some of the standards formulated earlier
The unified guiding element "General Test Methods for Pigments and Extender Pigments" is not used. In addition, there are a few common test methods for pigments and extender pigments.
The independent number of the standard is not included in the various parts of the national standard GB/T 5211.It will be gradually processed in recent years and in the future formulation or revision work.
Smoothly, standardize the format of the standard number and standard name, and improve the standard system. GB/T 5211 "General Test Methods for Pigments and Extender Pigments"
The correspondence between the various parts to be formulated or revised and the current standards are shown in Table 1.
Table 1 Correspondence between each part of GB/T 5211 to be formulated or revised and the current standard
Number of issued document
GB/T 5211.1-2003
Determination of water-soluble pigments by cold extraction
How to take
GB/T 5211.1
General test methods for pigments and extender pigments Part 1
Part. Determination of water-soluble matter by cold extraction method
GB/T 5211.2-2003
Determination of water-soluble pigments by hot extraction
How to take
GB/T 5211.2
General test methods for pigments and extender pigments No. 2
Part. Determination of Water-soluble Matter Hot Extraction Method
GB/T 5211.3-2020
General test of pigments and extender pigments
Method Part 3.Wave at 105℃
Hair determination
GB/T 5211.3
General test methods for pigments and extender pigments No. 3
Part. Determination of Volatile Matter at 105℃
GB/T 5211.4-1985
Pigment filling volume and apparent density
Determination of
GB/T 5211.4
General test methods for pigments and extender pigments No. 4
Part. Determination of Filling Volume and Apparent Density
GB/T 5211.5-2008 Determination of pigment resistance GB/T 5211.5
General Test Methods for Pigments and Extender Pigments No. 5
Part. Tolerance Test
GB/T 5211.6-2020
General test of pigments and extender pigments
Method part 6.water suspension
Determination of pH
GB/T 5211.6
General test methods for pigments and extender pigments No. 6
Part. Determination of pH Value of Water Suspension
GB/T 1864-2012
General test of pigments and extender pigments
Comparison of method pigment colors
GB/T 5211.7
General Test Methods for Pigments and Extender Pigments No. 7
Part. Comparison of colors
GB/T 1713-2008
Determination of pigment density
Bottle method
GB/T 5211.8
General Test Methods for Pigments and Extender Pigments No. 8
Part. Determination of Density Pycnometer Method
GB/T 1710-2008 Comparison of light resistance of similar colored pigments GB/T 5211.9
General test methods for pigments and extender pigments No. 9
Part. the same type of coloring pigments with light resistance
Compare
GB/T 1711-1989
Pigment is thermally stable in drying paint
Qualitative comparison
GB/T 5211.10
General Test Methods for Pigments and Extender Pigments No.
Part 10.Pigments are thermally stable in oven-dried paints
Sexual comparison
GB/T 5211.11-2008
Pigment water-soluble sulfate, chloride and
Nitrate determination
GB/T 5211.11
General Test Methods for Pigments and Extender Pigments No.
Part 11.Water-soluble sulfate, chloride and nitric acid
Salt determination
Table 1 Correspondence between each part of GB/T 5211 to be formulated or revised and the current standard (continued)
Number of issued document
GB/T 5211.12-2007
Resistivity of pigment water extract
Determination
GB/T 5211.12
General Test Methods for Pigments and Extender Pigments No.
Part 12.Determination of electrical resistivity of water extract
GB/T 5211.13-1986
PH of pigment water extract
Determination
GB/T 5211.13
General Test Methods for Pigments and Extender Pigments No.
Part 13.Determination of the pH of the water extract
General test of pigments and extender pigments
Method part 14.residue on sieve
Mechanical flushing method
GB/T 5211.14
General Test Methods for Pigments and Extender Pigments No.
Part 14.Determination of the residue on the sieve, mechanical flushing method
GB/T 5211.15-2014
General test of pigments and extender pigments
Method part 15.oil absorption
Determination of
GB/T 5211.15
General Test Methods for Pigments and Extender Pigments No.
Part 15.Determination of oil absorption
GB/T 5211.16-2007 Comparison of white pigment's decoloring power GB/T 5211.16
General Test Methods for Pigments and Extender Pigments No.
Part 16.Comparison of White Pigment's Color Reducing Power
GB/T 5211.17-1988
White pigment contrast ratio (hiding power)
Comparison
GB/T 5211.17
General Test Methods for Pigments and Extender Pigments No.
Part 17.white pigment contrast ratio (hiding power)
Compare
GB/T 5211.18-2015
General test of pigments and extender pigments
Method part 18.residue on sieve
Determination of water method (manual operation)
GB/T 5211.18
General Test Methods for Pigments and Extender Pigments No.
Part 18.Determination of the residue on the sieve water method (manual
operate)
GB/T 5211.19-1988
The relative tinting power of the colored pigments and
Determination of Diluted Color by Visual Comparison Method
GB/T 5211.19
General Test Methods for Pigments and Extender Pigments No.
Part 19.Relative tinting strength and punching of colored pigments
Determination of light color by visual comparison method
GB/T 5211.20-1999
In the natural color system, white, black and
Comparing color of coloring pigment
Method
GB/T 5211.20
General Test Methods for Pigments and Extender Pigments No.
Part 20.In the natural color system, white, black and
Comparative chromaticity method for the color of colored pigments
Comparison of HG/T 3834-2006 Pigment Bleed Resistance GB/T 5211.21
General Test Methods for Pigments and Extender Pigments No.
Part 21.Comparison of the resistance of pigments to bleeding
HG/T 3835-2006
Determination of pigment density (using centrifuge
(Exclude entrained air)
GB/T 5211.22
General Test Methods for Pigments and Extender Pigments No.
Part 22.Determination of Density (Exclude with Centrifuge
Entrained air)
GB/T 13451.2-1992
Relative tinting strength and whiteness of colored pigments
Determination of the relative scattering power of color pigments
Photometric method
GB/T 5211.23
General Test Methods for Pigments and Extender Pigments No.
Part 23.Relative tinting strength and whiteness of colored pigments
Determination of relative scattering power of pigments by photometric method
--GB/T 5211.24
General Test Methods for Pigments and Extender Pigments No.
Part 24.Determination of the total content of polychlorinated biphenyls (PCB)
Fixed dissolution, purification and GC-MS method
General test methods for pigments and extender pigments
Part 14.Determination of the residue on the sieve, mechanical flushing method
1 Scope
This document describes the general test method for the determination of the residue on the sieve by mechanical flushing of pigments and extender pigments dispersed in water.
This document applies to pigments and extender pigments dispersed in water, as well as other powders or particles that are insoluble in water, but does not apply to water.
Pigments and extender pigments that are difficult to wet or pelletized into balls.
2 Normative references
The contents of the following documents constitute the indispensable clauses of this document through normative references in the text. Among them, dated quotations
Only the version corresponding to that date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
This document.
GB/T 3186 Paint, varnish and raw material sampling for paint and varnish (GB/T 3186-2006, ISO 15528.2000, IDT)
GB/T 6005 Test sieve The basic size of the woven wire mesh, perforated plate and electroformed sheet screen hole (GB/T 6005-
2008, ISO 565.1990, MOD)
3 Terms and definitions
The following terms and definitions apply to this document.
3.1
Residue on sieve
Coarse particles remaining on the test sieve of the specified aperture during the test.
4 Principle
In the washing device, the test pigments or extender pigments dispersed in the water are driven by the rotating water stream to make centrifugal movement, and the water washes the fine particles
After passing through the test sieve, the coarse particles remain on the sieve, and the coarse particles on the sieve are weighed after being dried.
5 Reagents or materials
5.1 Tap water. filtered and pressurized to (300 ± 20) kPa.
5.2 Wetting agent. such as ethanol (95% by volume) or sulfonate, etc., used to wet pigments and extender pigments that are difficult to wet by water. Wetting
The choice of agent should be negotiated by the parties concerned and explained in the test report.
6 Equipment
6.1 Mechanical flushing device
6.1.1 The mechanical flushing device is shown in Figure 1, and consists of the following parts.
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