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GB/T 32788.5-2016: Test method for properties of prepreg -- Part 5: Determination of resin content
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Test method for properties of prepreg -- Part 5: Determination of resin content
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GB/T 32788.5-2016
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Basic data | Standard ID | GB/T 32788.5-2016 (GB/T32788.5-2016) | | Description (Translated English) | Test method for properties of prepreg -- Part 5: Determination of resin content | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Q23 | | Classification of International Standard | 83.120 | | Word Count Estimation | 10,115 | | Date of Issue | 2016-06-14 | | Date of Implementation | 2017-05-01 | | Quoted Standard | GB/T 1446 | | Adopted Standard | ISO 11667-1997, MOD | | Regulation (derived from) | National Standard Announcement No. 8 of 2016 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the extraction method, dissolution method, the principle of burning method, test conditions, instruments and equipment, samples, test procedures, test results and test reports for the determination of the content of impregnated resin. This standard applies to the carbon fiber, glass fiber, aramid fiber as a reinforcing material to thermosetting resin matrix for the determination of prepreg resin content. The firing method applies only to prepregs with glass fibers as reinforcing material. The extraction and dissolution methods are not suitable for prepregs where the reinforcing material is soluble in the solvent or the resin matrix is ??not completely soluble in the solvent. | GB/T 32788.5-2016: Test method for properties of prepreg -- Part 5: Determination of resin content---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Test method for properties of prepreg.Part 5. Determinatino of resin content
ICS 83.120
Q23
National Standards of People's Republic of China
Test method for performance of prepregs
Part 5. determination of resin content
Part 5. Determination ofresincontent
(ISO 11667..1997, Fiber-reinforcedplastics-Mouldingcompoundsand
prepregs-Determination ofresin, reinforced-fibreandmineral-filer
content-Dissolutionmethods, MOD)
2016-06-14 release
2017-05-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
China National Standardization Management Committee released
Foreword
GB/T 32788 "Prepreg performance test method" is divided into six parts.
Part 1. Determination of gel time;
- Part 2. Determination of resin fluidity;
Part 3. Determination of volatile matter content;
- Part 4. Determination of tensile strength;
- Part 5. Determination of resin content;
Part 6. Determination of mass per unit area.
This part is part 5 of GB/T 32788.
This part is drafted in accordance with the rules given in GB/T 1.1-2009.
This part uses the re-drafting method to modify ISO 11667..1997 "fiber reinforced molding compound molding and prepreg resin,
Determination of dissolution of strong fibers and mineral fillings ".
This section has a greater structural adjustment compared to ISO 11667..1997, which is listed in Appendix A and ISO 11667..1997
Of the chapter number of the control list.
The technical differences between this part and ISO 11667..1997 are as follows.
This part of the scope of the expansion of the scope of application, not to limit the molding compound, the "standard provisions of the two methods to determine the dissolution of molding materials and
Impregnated resin, reinforced fiber and mineral filler content. "Modified as" This part applies to carbon fiber, glass fiber, aramid fiber
And the like is used as a reinforcing material, and the content of the prepreg resin based on the thermosetting resin is measured. ";
--- Replace ISO 291..1997 with GB/T 1446, ISO 472. 1988 and ISO 4793. 1980;
- the definition of "definition" was deleted;
--- increase the "burning method" principle;
- the addition of the "test conditions" chapter, in coordination with the rest of the standard (see Chapter 4);
--- Change the contents of "Sampling" to the "Samples" section (see 5.2, 6.2);
Replace the "reagent" with "and then add the right amount of solvent, such as acetone, dichloromethane, methyl ethyl ketone and industrial alcohol or prepreg technical conditions
Prescribed solvent. (See 5.3.3, 6.3.6);
--- The formula for the content of the prepreg to enhance the fiber content and the prepreg resin content is edited and sorted (see 5.4.2, 6.4.1);
--- Added "burning method" to determine the glass fiber prepreg resin content of the chapter, according to GB/T 2577-2005 "glass fiber
Reinforced plastic resin content test method ", delete the contents of this part has nothing to do with the increase in the provisions of the sampling, an increase of the pre-
The formula for the impregnated fiber content (see Chapter 7);
--- The contents of the mineral filler are deleted and the contents are not related to this part.
This section makes the following editorial changes.
- Change the standard name to "Prepreg performance test method Part 5. Determination of resin content";
- Added Appendix A (informative) "This section is in contrast to chapter 11 of ISO 11667..1997."
This section is proposed by the China Building Materials Federation.
This part of the National Fiber Reinforced Plastics Standardization Technical Committee (SAC/TC39) centralized.
This part is responsible for the drafting unit. Harbin FRP Research Institute.
This part participates in the drafting unit. AVIC Composite Material Co., Ltd., Hebei Haozheng Non-metallic Material Testing Service Co., Ltd., Lei Ke
Germany (polymer) Tianjin Co., Ltd., Jiangsu Hengshen Co., Ltd., Qihe County, Xingda Composite Materials Co., Ltd.
This part of the main drafters. Sun Yuanjun, Wang Baorui, Ding Xinjing, Ren Kun, Li Jinliang, Liu Dongxun, Zhang Rongqi, Yu Hao, Li Hongjiang, He Tao.
Test method for performance of prepregs
Part 5. determination of resin content
1 Scope
This part of GB/T 32788 specifies the extraction method, dissolution method, burning principle, test conditions, instrumentation
And equipment, samples, test procedures, test results and test reports.
This part is suitable for carbon fiber, glass fiber, aramid fiber as a reinforcing material, thermosetting resin as the base of the prepreg resin
Quantitative determination.
The burning method is only applicable to prepregs with glass fiber as a reinforcing material.
The extraction and dissolution methods are not suitable for the prepregs that can be dissolved in the solvent, or the resin matrix can not be completely dissolved in the solvent
Leaching.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
GB/T 1446 Fiber reinforced plastics - Test methods - General
3 principle
3.1 extraction method
The sample is placed in a Soxhlet extractor and extracted with a suitable solvent to completely dissolve the resin in the prepreg. Relative to the initial quality
Quantity, mass loss of sample.
3.2 Dissolution method
The sample was placed in a beaker containing a solvent and thoroughly washed to completely dissolve the resin in the prepreg. Relative to the initial mass, sample quality
Percentage of loss.
3.3 burning method
Place the sample in a muffle furnace and heat it to the specified temperature and time. Relative to the initial mass, the percentage of sample mass loss.
4 test conditions
4.1 Test environment
The test environment shall comply with the relevant provisions of GB/T 1446.
4.2 State adjustment
4.2.1 The following conditions do not require state adjustment of the prepreg.
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