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US$189.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 31407-2015: Determination of iodopropynyl butylcarbamate in cosmetics -- Gas chromatography method Status: Valid
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| GB/T 31407-2015 | English | 189 |
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Determination of iodopropynyl butylcarbamate in cosmetics -- Gas chromatography method
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GB/T 31407-2015
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Basic data | Standard ID | GB/T 31407-2015 (GB/T31407-2015) | | Description (Translated English) | Determination of iodopropynyl butylcarbamate in cosmetics -- Gas chromatography method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 9,998 | | Date of Issue | 2015-05-15 | | Date of Implementation | 2015-09-30 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | National Standard Announcement 2015 No. 15 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Standard specifies the cosmetics iodopropynyl butylcarbamate esters by gas chromatography (GC) measurement method and gas chromatography - mass spectrometry (GC-MS) method was confirmed. This Standard is applicable to the determination of iodine propynyl butyl carbamate alcohol in cosmetics. |
GB/T 31407-2015: Determination of iodopropynyl butylcarbamate in cosmetics -- Gas chromatography method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of iodopropynyl butylcarbamate in cosmeties. Gas chromatography method
ICS 71.100.70
Y42
National Standards of People's Republic of China
Determination of cosmetics iodopropynyl butylcarbamate ester
Gas chromatography
Issued on. 2015-05-15
2015-09-30 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard by the National Quality Supervision key product testing method Standardization Technical Committee (SAC/TC374) and focal points.
This standard was drafted. Guangzhou Quality Supervision and Testing Institute, Guangzhou Liby Enterprise Group Co., Limited Guangzhou Jie Bao daily necessities
The company, the State Quality Supervision and Inspection Center Cosmetics (Guangzhou), Guangzhou City Branch of cosmetics research, Ltd., Guangdong pill Biotech Shares
Limited.
The main drafters of this standard. Xian Yanping, Yu-luan, Liu Chunsheng, Luo Haiying, Chen meaning light, Chen Liwei, Wang Li, Wang, Yang Xin, Dong Hao,
Huang Yufeng, Guo Changhong, Xie Jian, Yangzuo Yi, Ling Chao, Ouyang Bu Qing, Fang Yongsheng.
Determination of cosmetics iodopropynyl butylcarbamate ester
Gas chromatography
1 Scope
This standard specifies the cosmetics iodopropynyl butylcarbamate esters by gas chromatography (GC) and gas chromatography measurement method - mass spectrometry
(GC-MS) method was confirmed.
This standard applies to the determination iodopropynyl butylcarbamate esters in cosmetics.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Sample of iodopropynyl butyl carbamate alcohol by ultrasonic extraction solvent, dehydrated over anhydrous sodium sulfate, determined by gas chromatography, the external standard method
Quantified by gas chromatography - mass spectrometry (SIM).
4 Reagents and materials
4.1 Water. GB/T 6682 provided a water.
4.2 Methanol. chromatographically pure.
4.3 THF. AR.
4.4 ol iodopropynyl butylcarbamate standard substance. purity ≥99%; CAS. 55406-53-6.
4.5 anhydrous sodium sulfate. AR, burning at 650 ℃ 4h, stored in a sealed desiccator.
4.6 Sodium chloride. AR.
4.7 methanol - tetrahydrofuran. V (methanol) V (THF) = 73.
4.8 methanol - water. V (methanol) V (water) = 73.
4.9 standard stock solution (5.0mg/mL). Weigh accurately standard substance (4.4) 50.0mg, dissolved in methanol and set the volume to 10mL.
4.10 standard working solution. Pipette appropriate amount of stock standard solution (4.9), a stepwise diluted with methanol concentrations were 0μg/mL,
0.050μg/mL, 0.20μg/mL, 1.00μg/mL, 2.00μg/mL, 5.00μg/mL series of standard working solution.
5. Apparatus
5.1 Gas chromatograph. with electron capture detector (ECD) detector.
5.2 Gas chromatography - mass spectrometry. source with electron impact (EI) source.
5.3 Analytical balance. accuracy of 0.1mg and 0.01g.
5.4 ultrasonic cleaning. ultrasonic power 250W.
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