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Determination of 2-methoxyethanol, 2-ethoxyethanol and 2- (2-methoxyethoxy) ethanol in cosmetics -- Gas chromatography
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GB/T 30942-2014
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Basic data | Standard ID | GB/T 30942-2014 (GB/T30942-2014) | | Description (Translated English) | Determination of 2-methoxyethanol, 2-ethoxyethanol and 2- (2-methoxyethoxy) ethanol in cosmetics -- Gas chromatography | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 11,147 | | Date of Issue | 7/8/2014 | | Date of Implementation | 11/1/2014 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | 2014 National Standards Bulletin No. 18 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the cosmetics glycol methyl ether, ethylene glycol detection ether, diethylene glycol dimethyl ether. This standard applies to creams, milk, liquid cosmetics in ethylene glycol monomethyl ether, ethylene glycol Determination of die |
GB/T 30942-2014: Determination of 2-methoxyethanol, 2-ethoxyethanol and 2- (2-methoxyethoxy) ethanol in cosmetics -- Gas chromatography ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of 2-methoxyethanol, 2-ethoxyethanol and 2- (2-methoxyethoxy) ethanol in cosmetics. Gas chromatography
ICS 71.100.70
Y42
National Standards of People's Republic of China
Cosmetics banned substances glycol monomethyl ether,
Glycol ether and diethylene glycol ether
Gas chromatography
Determinationof2-methoxyethanol, 2-ethoxyethanoland
2- (2-methoxyethoxy) ethanolincosmetics-Gaschromatography
Issued on. 2014-07-08
2014-11-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
The standard proposed by China National Light Industry Council.
This standard by the National Standardization Technical Committee of Fragrance Flavor and Cosmetic (SAC/TC257) centralized.
This standard was drafted. Product Quality Inspection Institute of Fujian Province.
The main drafters of this standard. fly swim ming, LIN Qin, Deming, Wang Zheng, Wu Ling, Zheng Xiao Yan, Huang Hongxia.
Introduction
The standard test substance is banned substances of "Hygienic Standard for Cosmetics" shall consist of not as a cosmetic raw material, component
Added to cosmetics. If technically unavoidable banned substances as impurities into cosmetics, the finished cosmetic products should follow the "Cosmetics
Health standards "General requirements for cosmetics, that is, under normal and reasonably foreseeable conditions of use, should not cause harm to human health.
Currently we have not yet provided these substances limited value, the present standards, the determination of these substances in cosmetics only provide detection methods.
Cosmetics banned substances glycol monomethyl ether,
Glycol ether and diethylene glycol ether
Gas chromatography
1 Scope
This standard specifies the cosmetics glycol methyl ether, ethylene glycol detection ether, diethylene glycol dimethyl ether.
This standard applies to creams, milk, liquid cosmetics in ethylene glycol monomethyl ether, ethylene glycol Determination of diethyl ether, diethylene glycol dimethyl ether.
This standard of ethylene glycol monomethyl ether, ethylene glycol diethyl ether, diethylene glycol monomethyl ether detection limit of 15mg/kg, the limit of quantification of 50mg/kg.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
Samples with ethanol ultrasonic extraction, gas chromatography flame ionization detector, retention time qualitative, external standard, gas chromatography
MS spectra.
4 Reagents and materials
Unless otherwise specified, the reagents were of analytical grade water as a water GB/T 6682 regulations.
4.1 ethanol.
4.2 ethylene glycol monomethyl ether, ethylene glycol diethyl ether, diethylene glycol ether standard. not less than 98.5% purity. Three kinds of glycol ethers
Alias, CAS number, molecular formula, molecular mass and structural formula, see Appendix A.
4.3 ethylene glycol monomethyl ether, ethylene glycol diethyl ether, diethylene glycol methyl ether of standard stock solution. Weigh were taken glycol monomethyl ether, ethylene glycol diethyl ether,
Ethylene glycol monomethyl ether (4.2) each 0.1g (accurate to 0.0001g) in 100mL volumetric flask with ethanol (4.1) to volume, and mix.
Standard stock solution concentration of 1.0mg/mL. Preserve refrigerator.
4.4 ethylene glycol monomethyl ether, ethylene glycol diethyl ether, diethylene glycol monomethyl ether mixed standard intermediate solution. Pipette 5.00mL ethylene glycol methyl ether acetate
Glycol ether, diethylene glycol methyl ether standard stock solution (4.3), a 50mL volumetric flask, diluted with ethanol (4.1) to the mark and mix.
Preparation of three kinds of glycol ethers concentration was 0.1mg/mL. Preserve refrigerator.
Mixed standard working solution of 4.5 ethylene glycol monomethyl ether, ethylene glycol diethyl ether, diethylene glycol ether. anhydrous ethanol (4.1) the mixed standard
Use solution (4.4) respectively dubbed a series of concentration 5.00g/mL, 10.0g/mL, 20.0g/mL, 50.0g/mL, 100g/mL of standard work
As a solution to preserve refrigerator.
5 Instruments
5.1 Gas chromatograph. equipped with a flame ionization detector (FID).
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