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Determination of dioxane residue in cosmetics -- Headspace gas chromatography-mass spectrometry
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GB/T 30932-2014
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Basic data | Standard ID | GB/T 30932-2014 (GB/T30932-2014) | | Description (Translated English) | Determination of dioxane residue in cosmetics -- Headspace gas chromatography-mass spectrometry | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | Y42 | | Classification of International Standard | 71.100.70 | | Word Count Estimation | 10,135 | | Date of Issue | 7/8/2014 | | Date of Implementation | 11/1/2014 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | 2014 National Standards Bulletin No. 18 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the cosmetics residual amount of dioxane headspace gas chromatography - mass spectrometry. This standard applies to creams, liquid, shampoo Cosmetics chew two alkyl residues determination. The standard for dioxane detection limit o |
GB/T 30932-2014: Determination of dioxane residue in cosmetics -- Headspace gas chromatography-mass spectrometry ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of dioxane residue in cosmetics. Headspace gas chromatography-mass spectrometry
ICS 71.100.70
Y42
National Standards of People's Republic of China
Disable dioxane in cosmetics residues of substances in the Determination
Headspace gas chromatography - mass spectrometry
Issued on. 2014-07-08
2014-11-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
The standard proposed by China National Light Industry Council.
This standard by the National Standardization Technical Committee of Fragrance Flavor and Cosmetic (SAC/TC257) centralized.
This standard was drafted. China Inspection and Quarantine Science Research Institute, Shanghai Institute of Daily Chemical Industry.
The main drafters of this standard. Wang Chao, Ma Qiang, Lijing Rui, Li Wentao, birch, Ding Lan, Ma Kuaijuan, Wu Xiao Jian, Li Qiong.
Introduction
This standard test substance is banned substances of "Hygienic Standard for Cosmetics" shall consist of not as a cosmetic raw material, component Tim
Added to cosmetics. If technically unavoidable banned substances as impurities into cosmetics, the finished cosmetic products shall comply with the "cosmetic Wei
Health standard "General requirements for cosmetics, that is, under normal and reasonably foreseeable conditions of use, should not cause harm to human health.
At present, China has not yet specified the substance of limited value, the present standards, the determination of these substances in cosmetics only provide detection methods.
Disable dioxane in cosmetics residues of substances in the Determination
Headspace gas chromatography - mass spectrometry
1 Scope
This standard specifies the cosmetics residual amount of dioxane headspace gas chromatography - mass spectrometry.
This standard applies to creams, liquid, shampoo cosmetics dioxane residues determination.
The standard for dioxane detection limit of 0.8mg/kg, the limit of quantification of 2.5mg/kg.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
Principle 3
After the sample vial heated extracted by headspace gas chromatography - mass spectrometry, internal standard.
4 Reagents and materials
Unless otherwise indicated, the reagents used were of analytical grade water as a water GB/T 6682 regulations.
4.1 sodium chloride.
4.2-dioxane standard substance. Formula C4H8O2, CAS No. 123-91-1, purity of not less than 99%, the formula refer to Appendix A of FIG.
A.1.
4.3 deuterated dioxane standard substance. Formula C4D8O2, CAS No. 17647-74-4, purity of not less than 99%, the formula in Appendix A
Figure A.2.
4.4 dioxane standard stock solution. accurately weighed amount of dioxane standard substance (accurate to 0.0001g), with deionized water to a concentration
Standard stock solution 1000μg/mL, and stored at 4 ℃.
4.5 deuterated dioxane standard stock solution. accurately weighed amount of deuterated dioxane standard substance (accurate to 0.0001g), with deionized water
Having a concentration of 1000μg/mL standard stock solution, and stored at 4 ℃.
5. Apparatus
5.1 Gas chromatography - mass spectrometry (GC-MS) instrument. with electron impact ionization ion source (EI).
5.2 air injector.
5.3 empty vials. 20mL.
5.4 Analysis of balance. a sense of the amount of 0.0001g and 0.001g.
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