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Methods for chemical analysis of high purity selenium -- Determination of boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead and bismuth contents -- Inductiv
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GB/T 26289-2010
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Basic data Standard ID | GB/T 26289-2010 (GB/T26289-2010) | Description (Translated English) | Methods for chemical analysis of high purity selenium -- Determination of boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead and bismuth contents -- Inductiv | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | H14 | Classification of International Standard | 77.120.01 | Word Count Estimation | 10,163 | Date of Issue | 2011-01-14 | Date of Implementation | 2011-11-01 | Regulation (derived from) | National Standard Approval Announcement 2011 No.56 | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard provides high purity selenium boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, Nickel, copper, gallium, determination of bismuth impurity elements, cadmium, indium, lead. This standard applies to high purity selenium boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, Nickel, copper, gallium, cadmium, indium, Determination of bismuth content, lead. |
GB/T 26289-2010: Methods for chemical analysis of high purity selenium -- Determination of boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead and bismuth contents -- Inductiv
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of high purity selenium. Determination of boron, alumium, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead and bismuth contents. Inductively c
ICS 77.120.01
H14
National Standards of People's Republic of China
Methods for chemical analysis of high purity selenium
Boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury,
Determination of magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead, bismuth content
Inductively Coupled Plasma Mass Spectrometry
Determinationofboron, aluminum, iron, zinc, arsenic, silver, tin, antimony,
telurium, mercury, magnesium, titanium, nickel, copper, galium, cadmium,
indium, leadandbismuthcontents-
Issued on. 2011-11-01 2011-01-14 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard is in accordance with GB/T 1.1-2009 given rules drafted.
This standard by the national non-ferrous metals Standardization Technical Committee (SAC/TC243) centralized.
This standard was drafted. Beijing Nonferrous Metal Research Institute.
Participated in the drafting of this standard. Beijing Institute of Mining and Metallurgy, Emei Semiconductor Material Factory.
The main drafters of this standard. Liu Ying, Gao Yan, Li Jidong, Liu Feng advanced, Wenying, Lihua Chang, Ruan Gui colors.
Methods for chemical analysis of high purity selenium
Boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury,
Determination of magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead, bismuth content
Inductively Coupled Plasma Mass Spectrometry
1 Scope
This standard specifies the selenium in high purity boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead, bismuth impurity element
Measurement method.
This standard applies to the measurement of high purity selenium and boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium, mercury, magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead, bismuth content
set. Determination of the range in Table 1.
Table 1
Element measurement range/measuring range of elements% /%
B 0.0001 ~ 0.0010
Al 0.00005 ~ 0.0010
Fe 0.00005 ~ 0.0010
Zn 0.00005 ~ 0.0010
As 0.00005 ~ 0.0010
Ag 0.00005 ~ 0.0010
Sn 0.00005 ~ 0.0010
Sb 0.00005 ~ 0.0010
Te 0.00005 ~ 0.0010
Hg 0.00005 ~ 0.0010
Mg 0.00001 ~ 0.00020
Ti 0.00001 ~ 0.00020
Ni 0.00001 ~ 0.00020
Cu 0.00001 ~ 0.00020
Ga 0.00001 ~ 0.00020
Cd 0.00001 ~ 0.00020
In 0.00001 ~ 0.00020
Pb 0.00001 ~ 0.00020
Bi 0.00001 ~ 0.00020
- -
2 Method summary
The sample is dissolved in nitric acid, the direct determination of boron, aluminum, iron, zinc, arsenic, silver, tin, antimony, tellurium and mercury content by inductively coupled plasma mass spectrometry;
Cation exchange magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead, bismuth and selenium lot separating matrix and is enriched by inductively coupled plasma
Determination of magnesium, titanium, nickel, copper, gallium, cadmium, indium, lead and bismuth in mass spectrometry.
3 Reagents and materials
Unless otherwise indicated, used in the analysis confirmed only for the gifted class pure reagents; the water is deionized water, the resistivity of not less than
18.2MΩ · cm.
3.1 hydrochloride (ρ1.19g/mL).
Nitrate 3.2 (ρ1.42g/mL).
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