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GB/T 18114.8-2025: Chemical analysis methods for rare earth concentrates - Part 8: Determination of rare earth oxide contents and distribution
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Chemical analysis methods for rare earth concentrates - Part 8: Determination of rare earth oxide contents and distribution
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GB/T 18114.8-2025
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| GB/T 18114.8-2010 | English | 209 |
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Chemical analysis methods of rare earth concentrates -- Part 8: Determination of fifteen rare earth oxide relative contents -- Inductively coupled plasma emission spectrometry
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GB/T 18114.8-2010
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| GB/T 18114.8-2000 | English | 199 |
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Methods for chemical analysis of monazite concentrates. Determination of yttrium oxide content
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GB/T 18114.8-2000
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Standard similar to GB/T 18114.8-2025 GB/T 18114.11 GB/T 18114.3 GB/T 18114.9 Basic data | Standard ID | GB/T 18114.8-2025 (GB/T18114.8-2025) | | Description (Translated English) | Chemical analysis methods for rare earth concentrates - Part 8: Determination of rare earth oxide contents and distribution | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | H14 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 22,293 | | Date of Issue | 2025-08-01 | | Date of Implementation | 2026-02-01 | | Older Standard (superseded by this standard) | GB/T 18114.8-2010 | | Issuing agency(ies) | State Administration for Market Regulation, Standardization Administration of China | GB/T 18114.8-2025: Chemical analysis methods for rare earth concentrates - Part 8: Determination of rare earth oxide contents and distribution
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National Standard of the People's Republic of China
ICS 77.120.99CCS H 14
Chemical analysis methods for rare earth concentrates
Part 8.Rare earth oxide content and
Determination of dosage
Chemical analysis methods for rare earth concentrates-
Part 8.Determination of rare earth oxide contents and distribution
Released on August 1, 2025
2026-02-01 Implementation
State Administration for Market Regulation
The National Standardization Administration issued
Replaces GB/T 18114.8-2010
Preface
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1.Structure and drafting rules for standardization documents"
Drafting is required.
This document is Part 8 of GB/T 18114 Chemical Analysis Methods for Rare Earth Concentrates. GB/T 18114 has been published for the following
part.
-- Part 1.Gravimetric method for determination of total amount of rare earth oxides;
-- Part 2.Determination of thorium oxide content;
-- Part 3.Determination of calcium oxide content;
-- Part 4.Determination of niobium oxide, zirconium oxide and titanium oxide content - Inductively coupled plasma optical emission spectrometry;
-- Part 5.Determination of aluminum oxide content - Inductively coupled plasma optical emission spectrometry;
-- Part 6.Determination of silicon dioxide content;
-- Part 7.Determination of iron oxide content - Potassium dichromate titration method;
-- Part 8.Determination of rare earth oxide content and proportion;
-- Part 9.Determination of phosphorus pentoxide content;
-- Part 10.Determination of water content by gravimetric method;
--Part 11.Determination of fluorine content.
This document replaces GB/T 18114.8-2010 “Chemical analysis methods for rare earth concentrates Part 8.Fifteen rare earth element oxides”
Determination of components by inductively coupled plasma optical emission spectrometry”, compared with GB/T 18114.8-2010, except for structural adjustment and editorial changes,
In addition to the dynamic, the main technical changes are as follows.
a) The measurement range has been changed (see Chapter 1, Chapter 1 of the.2010 edition);
b) Added the step of preparing the analytical solution by dissolving the sample in hydrochloric acid or perchloric acid for inductively coupled plasma optical emission spectrometry (Method 1).
(See 4.5.4.2);
c) Modified the preparation of the series of standard solutions in the inductively coupled plasma optical emission spectrometry (Method 1) (see 4.5.5,.2010 Edition).
6.4);
d) Changed the precision in Inductively Coupled Plasma Optical Emission Spectrometry (Method 1) from “Permissible Difference” to “Reproducibility Limit”
(See 4.7.2, 8.2 of the.2010 edition);
e) X-ray fluorescence spectrometry (Method 2) has been added to determine the content of rare earth oxides (see Chapter 5).
Please note that some of the contents of this document may involve patents. The issuing organization of this document does not assume the responsibility for identifying patents.
This document was proposed and coordinated by the National Rare Earth Standardization Technical Committee (SAC/TC 229).
This document was drafted by. Baotou Rare Earth Research Institute, China Northern Rare Earth (Group) High-Tech Co., Ltd., Qiandong Rare Earth Group Co., Ltd.
Co., Ltd., Hunan Rare Earth Metal Materials Research Institute Co., Ltd., Jiangxi Tungsten and Rare Earth Products Quality Supervision and Inspection Center (Jiangxi Tungsten
and Rare Earth Research Institute), National Standard (Beijing) Inspection and Certification Co., Ltd., Xiamen Rare Earth Materials Research Institute, and Guohe General (Qingdao) Testing and Evaluation Co., Ltd.
Company, Ganzhou Aikerui Testing Technology Co., Ltd.
The main drafters of this document are. Wu Wenqi, Du Yejian, Nie Chenghong, Xue Jianping, Ren Xudong, Jiang Yujuan, Wen Bin, Chen Yan, Wang Guichao, Shi Xuefeng,
Jiang Yuan, Zhang Chunlan, Chen Yanqun, Huang Xiaori, Xu Na, Liu Jiayu, Yu Lei, Zhang Qikai, Ren Sheng, Wang Xiangde, and Liu Xiaojian.
This document was first published in.2000, revised for the first time in.2010, and this is the second revision.
introduction
Rare earth concentrate refers to the product of rare earth ore after beneficiation and enrichment, with rare earth content reaching the smelting requirements, and its rare earth elements are not naturally distributed.
Including fluorocarbon cerium ore concentrate, monazite concentrate, fluorocarbon cerium ore-monazite mixed concentrate, fluorocarbon cerium lanthanum concentrate, etc. Rare earth has
Excellent optical, electromagnetic and other physical properties, can be combined with other materials to form a variety of new raw materials with different properties, which can greatly improve other
The quality and performance of the product. Chemical composition is an important assessment indicator of rare earth concentrate products. It is necessary to develop a scientific and accurate chemical composition analysis method.
Standards, by clarifying the scope of application, standardizing reagents and materials, test equipment and procedures, and giving precise results through repeated tests and verifications.
The data collected can enhance the consistency and comparability of data between different laboratories, and provide a rigorous and standardized method for the quality inspection of rare earth concentrate products.
GB/T 18114 "Chemical Analysis Methods for Rare Earth Concentrates" aims to establish
A complete set of chemical analysis methods and standards applicable to the production and trade needs of rare earth concentrate products.
It consists of 11 parts.
-- Part 1.Determination of the total amount of rare earth oxides. The purpose is to establish a gravimetric method for determining the content of rare earth oxides in rare earth concentrates.
method.
-- Part 2.Determination of thorium oxide content. The purpose is to establish a plasma emission spectrometry and plasma mass spectrometry method for the determination of thorium oxide content in rare earth concentrates.
Method for determining the thorium oxide content in water.
-- Part 3.Determination of calcium oxide content. The purpose is to establish flame atomic absorption spectrometry, EDTA titration, inductively coupled
Method for determination of calcium content in rare earth concentrates by plasma atomic emission spectrometry.
-- Part 4.Determination of niobium oxide, zirconium oxide and titanium oxide content. The purpose is to establish an inductively coupled plasma optical emission spectrometry method for the determination of
Method for determining the content of niobium oxide, zirconium oxide and titanium oxide in rare earth concentrate.
--Part 5.Determination of Alumina Content. The purpose is to establish an inductively coupled plasma optical emission spectrometry method for the determination of oxygen in rare earth concentrates.
Aluminium content method.
-- Part 6.Determination of silicon dioxide content. The purpose is to establish molybdenum blue spectrophotometry and inductively coupled plasma optical emission spectrometry
Method for determining silicon dioxide content in rare earth concentrates.
--Part 7.Determination of iron oxide content. The purpose is to establish a potassium dichromate titration method for determining the iron oxide content in rare earth concentrates.
method.
-- Part 8.Determination of rare earth oxide content and proportion. The purpose is to establish an inductively coupled plasma optical emission spectrometry method
(Method 1) Determination of rare earth oxide content in rare earth concentrates and (Method 2) Determination of rare earth oxide content in rare earth concentrates by X-ray fluorescence spectrometry
Method for determining chemical content.
-- Part 9.Determination of phosphorus pentoxide content. The purpose is to establish a bismuth molybdenum blue spectrophotometric method and inductively coupled plasma
Method for determining phosphorus pentoxide content in rare earth concentrates by emission spectrometry.
-- Part 10.Determination of moisture. The purpose is to establish a gravimetric method for the determination of moisture content in rare earth concentrates.
-- Part 11.Determination of fluoride content. The purpose is to establish the EDTA titration method, alizarin spectrophotometry and fluoride ion selective electrophoresis method.
Method for determining the fluorine content in rare earth concentrates by polar method.
GB/T 18114.8-2000 was revised in.2010 after its release to better adapt to the changes in the rare earth industry.
Improve the rare earth mineral product analysis and testing technology and standard system, according to the new industry and market changes and needs, in the original inductively coupled plasma
Based on the volume emission spectrometry (method 1), the method of dissolving the sample with hydrochloric acid and perchloric acid was added; at the same time, X-ray fluorescence spectroscopy was added.
Method 2 covers the indicators of rare earth oxide content and distribution amount in existing rare earth concentrate products, which is the chemical composition of rare earth concentrate.
The determination of oxide content and proportioning amount provides a fast and accurate method standard with good operability.
Chemical analysis methods for rare earth concentrates
Part 8.Rare earth oxide content and
Determination of dosage
1 Scope
This document describes the method for the determination of rare earth oxide content and distribution in rare earth concentrates.
This document is applicable to the determination of rare earth oxide content and distribution amount in rare earth concentrates.
This document contains two methods. Inductively coupled plasma optical emission spectrometry (Method 1) is suitable for the distribution of rare earth oxides in rare earth concentrates.
The determination range is shown in Table 1.X-ray fluorescence spectrometry (method 2) is suitable for the determination of rare earth oxide content in rare earth concentrates.
The fixed range is shown in Table 2.
Table 1 Measurement range of inductively coupled plasma optical emission spectrometry (method 1)
Oxide to be tested
Lanthanum oxide, cerium oxide
Praseodymium oxide, neodymium oxide
Samarium oxide, europium oxide, gadolinium oxide, terbium oxide, dysprosium oxide, holmium oxide,
Erbium oxide, thulium oxide, ytterbium oxide, lutetium oxide, yttrium oxide
Determination range of rare earth oxide content
15.00~60.00
1.00~20.00
0.050~10.00
Table 2 X-ray fluorescence spectrometry (method 2) measurement range
Oxide to be tested
Lanthanum oxide
Cerium oxide
Praseodymium oxide
Neodymium oxide
Samarium oxide, europium oxide, gadolinium oxide, yttrium oxide
Terbium oxide, dysprosium oxide, holmium oxide, erbium oxide
Measurement range (mass fraction)
3.00~30.00
5.00~40.00
1.00~5.00
1.00~15.00
0.050~3.00
0.10~0.50
2 Normative references
The contents of the following documents constitute the essential clauses of this document through normative references in this document.
For referenced documents without a date, only the version corresponding to that date applies to this document; for referenced documents without a date, the latest version (including all amendments) applies to
This document.
GB/T 6379.2 Accuracy (Trueness and Precision) of Measurement Methods and Results Part 2.Determination of Repeatability of Standard Measurement Methods
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