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US$319.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB 4926-2008: Food additive -- Red kojic rice (powder) Status: Obsolete GB 4926: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB 4926-2008 | English | 319 |
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Food additive -- Red kojic rice (powder)
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GB 4926-2008
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| GB 4926-1985 | English | 239 |
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Food additive--Red kojic rice
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GB 4926-1985
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PDF similar to GB 4926-2008
Basic data | Standard ID | GB 4926-2008 (GB4926-2008) | | Description (Translated English) | Food additive -- Red kojic rice (powder) | | Sector / Industry | National Standard | | Classification of Chinese Standard | X41 | | Classification of International Standard | 67.220.20 | | Word Count Estimation | 8,851 | | Date of Issue | 2008-12-03 | | Date of Implementation | 2009-06-01 | | Older Standard (superseded by this standard) | GB 4926-1985 | | Quoted Standard | GB 1354; GB/T 4789.3; GB/T 4789.4; GB/T 4789.5; GB/T 4789.10; GB/T 5009.3; GB/T 5009.11; GB/T 5009.22; GB/T 5009.74; GB/T 6682 | | Regulation (derived from) | Announcement of Newly Approved National Standards No. 19 of 2008 (No. 132 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Chinese standard specifies the food additive red yeast rice < precision > product definition, product classification, requirements, test methods, inspection rules, marking, packaging, transport and storage. This standard applies to red yeast rice (powder> the production, testing and marketing. |
GB 4926-2008: Food additive -- Red kojic rice (powder)---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food additive.Red kojic rice (powder)
ICS 67.220.20
X41
National Standards of People's Republic of China
Replacing GB 4926-1985
Food additives Red yeast rice (powder)
Published 2008-12-03
2009-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China issued
Foreword
5.3, 5.4 of this standard is mandatory, the rest are recommended.
Instead of the standard GB 4926-1985 "red rice food additive."
This major change compared to the standard GB 4926-1985 as follows.
--- cancel the product classification;
--- increased red yeast powder product type, and to develop appropriate indicators;
--- canceled BHC and DDT indicators;
--- an increase of heavy metals, coliform bacteria, pathogens indicators.
This standard is proposed and managed by the National Standardization Technical Committee on Food Additives.
This standard was drafted. Zhang Yiwu Ge Biological Engineering Co., Ltd., Shandong Food Co., Ltd., China Academy of Food and Fermentation Industry,
Wuhan good as biological products Co., Ltd., Yongkang Sunshine natural pigment factory.
The main drafters. Ding Ge, Zhao Jixing, Zhang Wei, Yao Jicheng, Xu Hui, Ding, Zhang, Yang Guohua, Guo Xinguang, Wei Ping, Zhu Jinbo.
This standard supersedes the previous editions are.
--- GB 4926-1985.
Food additives Red yeast rice (powder)
Range 1
This standard specifies the food additive red yeast rice (powder) product definition, product classification, requirements, test methods, inspection rules, marks, package
Loading, transport and storage.
This standard applies to the red yeast rice (powder) production, testing and marketing.
2 Normative references
Terms of the following documents become provisions of this standard by reference in this standard. For dated reference documents, all later
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to agreements based on this standard
Whether the latest versions of these documents. For undated references, the latest version applies to this standard.
GB 1354 rice
GB/T 4789.3 learn food hygiene inspection Coliform bacteria microbes
GB/T 4789.4 Microbiological examination of food hygiene inspection salmonella
GB/T 4789.5 Microbiological examination of food hygiene Shigella test
GB/T 4789.10 Microbiological examination of food hygiene inspection Staphylococcus aureus
Determination GB/T 5009.3 moisture in food
GB/T 5009.11 Determination of total arsenic and inorganic food arsenic
Determination of aflatoxin B1 GB/T 5009.22 aflatoxin in food
GB/T heavy metals in food additives 5009.74 limit test
GB/T 6682 for analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)
3 Terms and Definitions
The following terms and definitions apply to this standard.
3.1
powder.
4 Products
Morphological divided by product. granular and powdered.
5 Requirements
5.1 Requirements for raw materials
Rice should meet the requirements of GB 1354.
5.2 Sensory requirements
Shall comply with the requirements of Table 1.
Table 1 Sensory requirements
Project granular powder
Exterior
Red to dark purple, crisp texture, no mildew, ignorance
Significant visible impurities, irregular particulate
Brown to dark purple, no mildew, no
Visible impurities, in powder form
Off flour to red -
Aroma has red yeast inherent Hong Qu
5.3 Physical and Chemical Requirements
Shall comply with the requirements of Table 2.
Table 2 Physical and chemical requirements
Project granular powder
Moisture /% ≤ 10.0
Color value/(u/g) ≥ 1000
Fineness (100 mesh pass rate) /% ≥ - 95.0
5.4 hygiene requirements
Shall comply with the requirements of Table 3.
Table 3 hygiene requirements
Project Requirements
Arsenic (As)/(mg/kg) ≤ 1
Heavy Metals (as Pb)/(mg/kg) ≤ 10
Coliforms/(MPN/100g) ≤ 30
Aflatoxin B1/(μg/kg) ≤ 5
Pathogens (disease-causing means the intestinal bacteria and cocci) not detected
6 Test methods
This standard is used in water, when not specified other requirements, refer to meet the requirements of GB/T 6682 is.
This standard reagents used, when the specification does not indicate, refer AR (AR). If the special requirements must be clearly dictates.
This standard was, when formulated with which solvent does not indicate, refer to an aqueous solution.
6.1 sensory inspection
100g samples were taken on a white paper, color viewing, mildew particles (powder) and its impurities with the naked eye; red rice cut with a knife, broken observed
Surface; 10g sample was taken approximately opposite hands, with the smell the odor.
6.2 Water
Testing according to GB/T 5009.3 is.
6.3 Color price
6.3.1 instruments and equipment
In addition to conventional laboratory equipment needed.
6.3.1.1 mill.
6.3.1.2 spectrophotometer.
6.3.1.3 constant temperature water bath. Temperature accuracy ± 0.5 ℃.
6.3.2 Reagents and solutions
70% ethanol solution (volume fraction).
6.3.3 Analysis of step
The sample was crushed with a grinder, which sample may be 40 mesh to 60 mesh sieve.
Weigh accurately a sample pulverized mixed 0.2g (accurate to 0.001g), was dissolved with 70% ethanol and transferred into 100mL
Volumetric flask, dilute to the mark, closure, placed in a water bath at 60 ℃ ± 0.5 ℃, the soaking accuracy IH, cooled to room temperature and removed, supplemented with 70% ethanol
Solution to volume, and mix. Filtered with filter paper, the filtrate collected in a stoppered cuvette standby.
Imbibe above filtrate 2.0mL ~ 5.0mL to 50mL volumetric flask (light absorbance final dilution fall within the range of 0.3 to 0.6
Endo), diluted with 70% ethanol volume to 50mL, shake, with 10mm cuvette, 70% ethanol solution to make the reference, at a wavelength of 505nm
, The measured absorbance of the sample was soaked dilution A.
6.3.4 computing
Sample color value according to formula (1).
(1)
Where.
--- the X1 color value of the sample, the unit for the color value per gram (u/g);
A --- dilutions soaked absorbance;
Qiao --- infusions suction volume of ethanol in milliliters (mL).
The results held until the integer bits.
6.3.5 allows poor
Parallel experiment, the difference between the two measured values should not exceed 2%.
Fineness 6.4
6.4.1 instruments and equipment
6.4.1.1 standard test sieves (corresponding to 200 mesh).
6.4.1.2 Analytical balance. Accuracy ± 0.2mg.
6.4.2 Analysis of step
Red yeast rice weighed 100g (to the nearest 0.2g).
The provisions of the standard sieve screen mounted on the chassis, and then said good sample is fully transferred to the standard screen, cover, oscillation screening 5min (knock from time to time
Bang playing screen), allowed to stand 2min, remove the cover, the sieve was carefully transferred to a known mass of all the beaker, weighing scales, is calculated.
6.4.3 computing
The fineness of the sample according to the formula (2).
(2)
Where.
The mass fraction of an X2 --- fineness sample,%;
100 --- sampling amount in grams (G);
The obtained results are shown to an integer.
6.4.4 allows poor
Parallel experiment, the difference between the two measured values should not exceed 1%.
6.5 Arsenic
Testing according to GB/T 5009.11's.
6.6 Heavy Metals
Testing according to GB/T 5009.74's.
6.7 Coliforms
Testing according to GB/T 4789.3 is.
6.8 Aflatoxin B1
Determined according to GB/T 5009.22 method.
6.9 Pathogens
According to GB/T 4789.4, GB/T 4789.5, measured GB/T 4789.10 method.
7 Inspection rules
7.1 Batching
On the same day packaging factory, with the same specifications, quality grade and batch number, and have the same certificate of quality products for the batch.
7.2 Sampling
Table 7.2.1 according to claim 4 randomly selected samples.
Table 4 Sample sampling tables bagged
Batch range/number of samples drawn box/boxes skipping Units/pouch
< 10041
100 to 25,061
251 to 500,101
> 500 201
7.2.2 Sampling rata insert (bag) samples were taken at each 1/2 to 1/3, each of not less than 100g, 250g Insufficient sample
Plus take. Mix carefully, quartering riffling, two were installed in a clean and dry jar, label, specify. product name, specifications
Grade, production date or batch number, quantity, date of sampling, sampling locations and personnel. A bottle sent to laboratory testing; spare bottle storage for three months.
7.3 Inspection Classification
Inspection is divided into factory inspection and type test.
7.3.1 factory inspection
Products manufactured prior to 7.3.1.1, the manufacturer should be responsible for quality inspection department in accordance with this standard batches for testing. Inspection and sign
Hair quality certification of products, before leaving the factory.
7.3.1.2 factory inspection items. sensory, water, color value, fineness (powder), coliform bacteria.
7.3.2 Type inspection
7.3.2.1 type test items. sensory, physical and chemical and health requirements of all the items specified in this standard.
7.3.2.2 When the product under normal production conditions, type of inspection once a year, under any of the following conditions must also type inspection.
--- When such a raw material, process or formulation change greatly;
--- When you change the key technology and equipment;
--- trial production of new products or product long-term shutdown, resumed production;
--- when there is a large difference between the factory inspection results with normal production;
--- Quality Supervision, Inspection agency when requested.
7.4 determine the rules
7.4.1 When the test results if an index does not meet the standard requirements, should be re-extracted from the same batch of product samples be retested twice that amount,
To review the results shall prevail.
7.4.2 When opposition occurs both supply and demand on product quality, mutual consultation arbitration unit selected, re-inspection in accordance with this standard.
8 signs, packaging, transportation and storage
8.1 mark
Food additives must be packaged logo and product brochures, signs content may include. name, place of origin, name, health permits, production
License number, specifications, production date, lot number or code, shelf life, etc., and clearly indicate the words "food additive" on the sign.
8.2 Packaging
Packaged products should be approved by the state, and in accordance with appropriate food packaging materials with health standards.
8.3 Transport
Product during transport, non-toxic, hazardous, corrosive and other contaminants mixed, mixed operation, to avoid the sun and rain and the like.
In the transport process should be rain, moisture, prevent sun exposure.
8.4 Storage
Airiness product, clean, dry place, can not coexist with toxic, hazardous and corrosive substances and the like.
Products from the production date, in conformity with the above storage conditions, the intact original packaging, shelf life should be less than 12 months, businesses can
DETAILED as above indicated.
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