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GA/T 1613-2019: Forensic sciences--Examination methods for lidocaine, ropivacaine and bupivacaine in biological samples--GC-MS and LC-MS
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Forensic sciences--Examination methods for lidocaine, ropivacaine and bupivacaine in biological samples--GC-MS and LC-MS
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GA/T 1613-2019
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Basic data | Standard ID | GA/T 1613-2019 (GA/T1613-2019) | | Description (Translated English) | Forensic sciences--Examination methods for lidocaine, ropivacaine and bupivacaine in biological samples--GC-MS and LC-MS | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.310 | | Word Count Estimation | 14,151 | | Date of Issue | 2019 | | Date of Implementation | 2019-12-01 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1613-2019: Forensic sciences--Examination methods for lidocaine, ropivacaine and bupivacaine in biological samples--GC-MS and LC-MS
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Forensic sciences--Examination methods for lidocaine, ropivacaine and bupivacaine in biological samples--GC-MS and LC-MS
ICS 13.310
A92
Public Safety Industry Standards of the People's Republic of China
Lidocaine,
Ropivacaine and bupivacaine test
Gas chromatography-mass spectrometry and liquid chromatography-mass spectrometry
Published on October 14,.2019
2019-12-01 Implementation
Issued by the Ministry of Public Security of the People's Republic of China
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some content of this document may involve patents. The issuer of this document does not assume responsibility for identifying these patents.
This standard was proposed by the National Toxic Analysis Subcommittee of Criminal Technical Standardization Technical Committee (SAC/TC179/SC1) and
Be in charge.
This standard was drafted by. Physical Evidence Appraisal Center of the Ministry of Public Security, Criminal Investigation Corps of the Public Security Department of Guangxi, People's Public Security University of China, Scientific Research on Judicial Expertise
Research Institute, Shanxi Medical University.
The main drafters of this standard. Zhang Leiping, Yu Zhongshan, Du Hongyan, Huang Kejian, Liu Xiaofeng, He Hongyuan, Zhang Yunfeng, Dong Ying, Luan Yujing, Liu Wei,
Shen Min, Yun Keming, Wang Fanglin, He Yi, Li Hongsen.
Lidocaine,
Ropivacaine and bupivacaine test
Gas chromatography-mass spectrometry and liquid chromatography-mass spectrometry
1 Scope
This standard specifies the lidocaine, ropivacaine and bupivacaine in forensic scientific biological materials (blood, urine, liver, kidney, stomach and stomach contents, etc.)
The qualitative and quantitative inspection methods of gas chromatography-mass spectrometry (GC-MS) and liquid chromatography-mass spectrometry (LC-MS).
This standard applies to the qualitative and quantitative analysis of lidocaine, ropivacaine and bupivacaine in forensic scientific biological samples. other
The qualitative and quantitative analysis of lidocaine, ropivacaine and bupivacaine in suspicious samples can be used by reference.
2 Normative references
The following documents are essential for the application of this document. For dated references, only the dated version applies to this article
Pieces. For the cited documents without date, the latest version (including all amendments) applies to this document.
GB/T 6682 Analysis laboratory water specifications and test methods
GA/T 122 Nomenclature of poison analysis
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principle
Using blank samples and added samples as controls, according to the requirements of parallel operation, extract, purify and concentrate biological samples, using gas-phase color
Qualitative quantification of spectrum-mass spectrometry and liquid chromatography-mass spectrometry, with retention time, characteristic ion fragment peaks and relative abundance ratio of mass spectrometry as qualitative judgment
Basis; Based on the peak area, the external standard method was used for quantitative analysis.
5 Reagents and materials
5.1 Reagent
Gas chromatography-mass spectrometry experimental water should meet the third grade water specified in GB/T 6682, and liquid chromatography-mass spectrometry experimental water should meet
Grade 1 water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis are of analytical grade, and the reagents include.
a) dichloromethane;
b) ethyl acetate;
c) Borax;
d) Sodium dihydrogen phosphate;
e) Disodium hydrogen phosphate;
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