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GB/T 3253.5-2008: Methods for chemical analysis of antimony and antimony trioxide -- Determination of copper content -- Flame atomic absorption spectrometric method
Status: Valid GB/T 3253.5: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 3253.5-2008 | English | 139 |
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Methods for chemical analysis of antimony and antimony trioxide -- Determination of copper content -- Flame atomic absorption spectrometric method
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GB/T 3253.5-2008
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| GB/T 3253.5-2001 | English | 199 |
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Methods for chemical analysis of antimony -- Determination of selenium content
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GB/T 3253.5-2001
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| GB/T 3253.5-1982 | English | RFQ |
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Chemical analysis of antimony--The atomic absorption spectrophotometric method for determination of lead, iron and copper
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GB/T 3253.5-1982
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PDF similar to GB/T 3253.5-2008
Basic data | Standard ID | GB/T 3253.5-2008 (GB/T3253.5-2008) | | Description (Translated English) | Methods for chemical analysis of antimony and antimony trioxide -- Determination of copper content -- Flame atomic absorption spectrometric method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | H13 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 6,663 | | Date of Issue | 2008-03-31 | | Date of Implementation | 2008-09-01 | | Older Standard (superseded by this standard) | GB/T 3253.3-2001; GB/T 3254.4-1998 | | Regulation (derived from) | National Standard Approval Announcement 2008 No.5 (Total No.118) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the determination of antimony trioxide, antimony and copper content. This section applies to the determination of antimony and antimony in copper content. Measurement range: 0. 0002% to 0. 30%. | GB/T 3253.5-2008: Methods for chemical analysis of antimony and antimony trioxide -- Determination of copper content -- Flame atomic absorption spectrometric method
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Methods for chemical analysis of antimony and antimony trioxide. Determination of copper content. Flame atomic absorption spectrometric method
ICS 77.120.99
H13
National Standards of People's Republic of China
Replacing GB/T 3253.3-2001, GB/T 3254.4-1998
Methods for chemical analysis of antimony and antimony trioxide
Determination of copper content - Flame atomic absorption spectrometry
Posted 2008-03-31
2008-09-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 3253 "Methods for chemical analysis of antimony and antimony trioxide," a total of 11 parts.
--- GB/T 3253.1 chemical analysis of antimony trioxide and arsenic content of molybdenum blue spectrophotometric determination of arsenic
--- GB /antimony trioxide and chemical analysis of iron content measured T 3253.2 phenanthroline spectrophotometry
--- GB/T 3253.3 antimony trioxide and chemical analysis of lead content - Flame Atomic Absorption Spectrometry
--- Determination of GB/T 3253.4 antimony trioxide and sulfur content of chemical analysis methods
--- GB/T 3253.5 antimony trioxide and chemical analysis of copper content - Flame Atomic Absorption Spectrometry
--- GB/T 3253.6 and antimony trioxide of selenium content - Atomic Fluorescence Spectrometry
--- GB T 3253.7 antimony trioxide and chemical analysis methods Determination of bismuth content /
--- Determination of GB/T 3253.8 antimony trioxide and antimony trioxide amount of chemical analysis methods
--- Determination of GB/T 3253.9 antimony trioxide and chemical analysis of cadmium content
--- Determination of GB/T 3253.10 antimony trioxide and chemical analysis of mercury content
Determination --- GB/T 3253.11 antimony trioxide and analysis of lead, copper, bismuth, cadmium, iron, selenium, chromium, arsenic, mercury, tin content
This is Part 5.
This Part replaces GB/T 3253.3-2001 "Methods for chemical analysis of lead, antimony, copper content determination" (copper portion), GB/T 3254.4-
1998 "Methods for chemical analysis of antimony trioxide Determination of copper content." Compared with GB/T 3253.3-2001, GB/T 3254.4-1998, this
Part of the following changes.
--- Canceled diethyl dithiocarbamate, dicyclohexyl ketone hydrazone oxalic acid bis (BCO) spectrophotometry, atomic absorption reserved
Spectroscopy;
--- Detection limit extends from 0.0030% to 0.0002%;
--- Complements the precision and quality assurance and control provisions.
This part is proposed by the China Nonferrous Metals Industry Association.
The non-ferrous metal part by the National Standardization Technical Committee.
This part of tin mining Twinkling Star Antimony Industry Co., Ltd., China Nonferrous Metals Industry Institute of Standards Metrology and Quality is responsible for drafting.
This section was drafted by the tin mining flash-antimony industry limited liability company.
This in part by Hunan Nonferrous Metals Research Institute, Hunan Chenzhou Mining Co., Ltd. participated in the drafting.
The main drafters of this section. Zong Yi, Song should ball, Cuide Hai.
This part certifier. Pangwen Lin, Wu Shaobo, Yang Deli.
This part of the standard replaces the previous editions are.
--- GB/T 3253.4-82, GB/T 3253.5-82, GB/T 3253.3-2001;
--- GB/T 3254.4-1998.
Methods for chemical analysis of antimony and antimony trioxide
Determination of copper content - Flame atomic absorption spectrometry
1 Scope
This section provides antimony trioxide and determination of copper content.
This section applies to the determination of antimony trioxide and copper content. Measurement range. 0.0002% to 0.30%.
2 Method summary
Sample with nitric acid or hydrochloric acid and hydrobromic acid dissolved and evaporated to dryness, repeat adding hydrobromide volatile except antimony. In dilute hydrochloric acid medium, using air - B
Alkyne flame atomic absorption spectrometer the absorbance at a wavelength of 324.7nm measured at copper, antimony trioxide and other impurities do not interfere
Determination.
3 Reagents
3.1 commercially available reagents
3.1.1 hydrochloric acid (ρ1.19g/mL).
3.1.2 nitrate (ρ1.42g/mL).
3.1.3 hydrobromic acid (ρ1.50g/mL).
3.2 solution
3.2.1 hydrochloric acid (1 + 1).
3.2.2 nitric acid (1 + 1).
3.3 standard solution
3.3.1 copper standard stock solution
Weigh 1.0000g copper (≥99.99%) in 200mL beaker, add 20mL of nitric acid (3.2.2), heat gently to dissolve completely, boil drive
In addition to oxides of nitrogen, cooled to room temperature. Moved into 1000mL volumetric flask, dilute with water to volume, and mix. 1mL solution containing 1mg of copper.
3.3.2 Copper standard solution
Pipette 10.00mL copper standard stock solution (3.3.1) in 100mL flask, make up 5mL hydrochloric acid was added (3.2.1), diluted with water
To the mark, and mix. This solution 1mL containing 100μg copper.
4 Instrument
Atomic absorption spectrometer, with copper hollow cathode lamp.
Under optimum working conditions for those who can reach the following indicators can be used.
--- Characteristic concentration. a solution in the measurement matrix consistent solution features copper concentration should not exceed 0.10μg/mL.
--- Precision. standard solution with the highest concentration of 10 times the absorbance measurements, the standard deviation should not exceed the average absorbance of 1.0%;
With the lowest concentration of standard solution (not "zero" concentration of the standard) measuring the absorbance of 10 times, the standard deviation should not exceed the maximum
0.5% concentration of the standard average absorbance.
--- Linear curve. The curve is divided into five sections according to concentration, absorbance difference between the absorbance difference between the highest and the lowest segment of the segment
Ratio of not less than 0.8.
Atomic absorption spectrometer reference operating conditions.
--- Wavelength 324.7nm;
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