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GB/T 28971-2012: Cigarettes -- Determination of tobacco specific N-nitrosamines in side stream smoke -- GC-TEA method
Status: Obsolete
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| GB/T 28971-2012 | English | 399 |
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Cigarettes -- Determination of tobacco specific N-nitrosamines in side stream smoke -- GC-TEA method
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GB/T 28971-2012
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Basic data | Standard ID | GB/T 28971-2012 (GB/T28971-2012) | | Description (Translated English) | Cigarettes -- Determination of tobacco specific N-nitrosamines in side stream smoke -- GC-TEA method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | X87 | | Classification of International Standard | 65.160 | | Word Count Estimation | 10,185 | | Quoted Standard | GB/T 6682; GB/T 19609; YC/T 185 | | Regulation (derived from) | National Standards Bulletin No. 41 of 2012 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the cigarette sidestream smoke of N- nitrosonornicotine (NNN), N- nitroso neonicotinoid (NAT), N- nitroso anabasine (NAB) and 4 (DMN -yl) -1 (3 pyridyl) -1 butanone (NNK) 4 tobacco provides specific nitrosamines by gas chromatograp | GB/T 28971-2012: Cigarettes -- Determination of tobacco specific N-nitrosamines in side stream smoke -- GC-TEA method
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Cigarettes. Determination of tobacco specific N-nitrosamines in sidestream smoke. GC-TEA method
ICS 65.160
X87
National Standards of People's Republic of China
Cigarette sidestream smoke of tobacco-specific nitrosamines N-
Gas chromatography - thermal energy analyzer method
Issued on. 2012-12-31
2013-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
This standard was drafted in accordance with the rules of GB/T 1.1-2009 and GB/T 20001.4-2001 given.
Please note that some of the content of this document may involve patents. Release mechanism of the present document does not assume responsibility for the identification of these patents.
This standard was proposed by the State Tobacco Monopoly Bureau.
This standard by the National Standardization Technical Committee on Tobacco (SAC/TC144) centralized.
This standard drafting units. China Tobacco Corporation, Zhengzhou Tobacco Research Institute, Hongta Tobacco (Group) Co., Ltd.
The main drafters of this standard. Liu Jian, willow, Wang Hongbo, Peng Bin, Zhangfeng Mei, Pang Yongqiang, Zhao, Zhang Xiaobing, Xie Wei complex, Huang hair,
If the white stone.
Cigarette sidestream smoke of tobacco-specific nitrosamines N-
Gas chromatography - thermal energy analyzer method
1 Scope
This standard specifies the cigarette sidestream smoke N- nitroso Nornicotine (NNN), N- nitroso neonicotinoid (NAT), N- nitroso Anabasis
Thieves base (NAB) and 4- (DMN-yl) -1- (3-pyridyl) -1-butanone (NNK) 4 growing tobacco specific nitrosamines GC - heat points
Analyzer measurement method.
This standard applies to the determination of cigarette sidestream smoke NNN, NAT, NAB, NNK four kinds of tobacco-specific nitrosamines.
The method for determining cigarette sidestream smoke NNN detection limit of 1.0ng/cig, the limit of quantification of 3.3ng/cig; NAT detection limit
0.9ng/cig, the limit of quantification of 2.9ng/cig; NAB detection limit of 1.0ng/cig, the limit of quantification of 3.5ng/cig; NNK detection limit
1.0ng/cig, the limit of quantification of 3.5ng/cig.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
GB/T 19609 cigarettes by conventional analytical determination of total particulate matter and tar smoking machine
Determination YC/T 185 sidestream smoke cigarette tar and nicotine
3 Terms and Definitions
The following terms and definitions apply to this document.
3.1
Tobacco-specific nitrosamines N- tobaccospecificN-nitrosamines (TSNAs)
Only present in tobacco and tobacco products in the N- nitrosamines.
Principle 4
After use of ascorbic acid-treated glass fiber filters and sidestream fishtail special suction hood were trapped cigarette sidestream smoke total particulate
Was extracted with dichloromethane particulate matter of TSNAs, the extract was concentrated and purified by column chromatography on basic alumina. By gas chromatography -
Thermal analysis spectrometer (GC-TEA) Determination of extract nitrosamines.
5 Reagents and materials
In addition to special requirements, should use analytical reagent grade water should be consistent with GB/T 6682 stipulated two of water.
Warning --- NNN and NNK is a strong carcinogen. All pre-processing operations should be carried out in a fume hood, laboratory personnel should wear anti
Mitts, masks for safety. After the experiment to the waste collected centrally.
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