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SN/T 4574-2016 English PDF

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SN/T 4574-2016: Determination of 2, 4-dinitro-toluene in paint and inks - Gas chromatography-mass spectrometry
Status: Valid
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SN/T 4574-2016English229 Add to Cart 3 days [Need to translate] Determination of 2, 4-dinitro-toluene in paint and inks - Gas chromatography-mass spectrometry Valid SN/T 4574-2016

PDF similar to SN/T 4574-2016


Standard similar to SN/T 4574-2016

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Basic data

Standard ID SN/T 4574-2016 (SN/T4574-2016)
Description (Translated English) Determination of 2, 4-dinitro-toluene in paint and inks - Gas chromatography-mass spectrometry
Sector / Industry Commodity Inspection Standard (Recommended)
Classification of Chinese Standard G51
Word Count Estimation 10,119
Date of Issue 2016-08-23
Date of Implementation 2017-03-01
Regulation (derived from) State-Quality-Inspection-Certification (2016)438
Issuing agency(ies) General Administration of Customs

SN/T 4574-2016: Determination of 2, 4-dinitro-toluene in paint and inks - Gas chromatography-mass spectrometry


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of 2, 4-dinitro-toluene in paint and inks-Gas chromatography-mass spectrometry People's Republic of China Exit Inspection and Quarantine standards Coatings, inks 2,4-dinitrotoluene Determination Gas chromatography - mass spectrometry Determinationof2,4-dinitro-toluene inaintandinks-Gas 2016-08-23 released 2017-03-01 Implementation People's Republic of China General Administration of Quality Supervision, Inspection and Quarantine released Exit Inspection and Quarantine of People's Republic of China Industry Standard Coatings, inks 2,4-dinitrotoluene Determination Gas chromatography - mass spectrometry China Standard Press First edition of November.2017

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard is drafted by the People's Republic of China Shenzhen Exit Inspection and Quarantine, Shenzhen Inspection and Quarantine Science Institute, Shenzhen vocational school. The main drafters of this standard.Song Bao Liang, Li Yong, Lin Jialu, Liu Zhihong, Li Bin, Wu Jingwu, Zou Chunhai, Feng Junli, Tong Changfei. Coatings, inks 2,4-dinitrotoluene Determination Gas chromatography - mass spectrometry Warning --- personnel using this standard should have the formal laboratory work experience. This standard does not indicate all possible safety problem. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the relevant provisions of the state.

1 Scope

This standard specifies the paint, ink 2,4 - dinitrotoluene content of gas chromatography - mass spectrometry method. This standard applies to coatings, inks 2,4-dinitrotoluene content determination. The detection limit of the method is 20mg/kg.

2 method summary

Using oscillating or ultrasonic extraction, the sample was quantitatively dissolved in methylene chloride organic solvent, filtered through a microporous membrane, the use of gas chromatography - Mass spectrometry determination of 2,4-dinitrotoluene, internal standard method.

3 Reagents and materials

3.1 Carrier gas. Helium, purity greater than 99.999%. 3.2 dichloromethane. Chromatography pure. 3.3 2,4-dinitrotoluene standard material, purity ≥ 99% (mass fraction), or known purity. 3.4 Internal standard .2,6-dinitrotoluene, purity ≥99% (mass fraction), or known purity. 3.5 Internal standard stock solution Accurately weigh internal standard (3.4) 0.25g (accurate to 0.0001g) and place in a 250mL volumetric flask with dichloromethane Alkane (3.2) dissolves to volume. The solution containing the internal standard compound is 1000mg/L. 3.6 Internal standard working solution Accurate Pipette 25mL internal standard stock solution (3.5) in 500mL volumetric flask, with dichloromethane (3.2) to volume Scale. The solution containing the internal standard compound is 50mg/L. 3.7 standard solution stock solution (now with the current) accurately weighed 2,4 - dinitrotoluene standard material (3.3) 0.25g (accurate to 0.0001g) set In a 250mL volumetric flask, dilute to volume with dichloromethane (3.2). The solution contains 2,4-dinitrotoluene 1000 mg/L. 3.8 standard working solution (now with the current allocation.) Pipette 50μL, 300μL, 500μL, 700μL, 1000μL standard solution stock solution (3.7) and 500μL internal standard stock solution (3.5) in a 10mL volumetric flask with dichloromethane (3.2) to volume, as a standard working solution. The series of solutions contain internal standard compound with the concentration of 50mg/L and the concentration of 5mg/L, 30mg/L, 50mg/L, 70mg/L, 100mg/L of 2,4-dinitrotoluene standard working solution.

4 instruments and equipment

4.1 Gas Chromatography - Mass Spectrometer (GC-MS) with EI source. 4.2 Whirlpool mixer. 4.3 micro-syringe .10μL. 4.4 Balance. Sense of 0.1mg. 4.5 With sample bottle. About 20mL glass bottles, with a sealable cap. 4.6 Microporous filter. Organic phase syringe filter, 0.45μm or equivalent.

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