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Determination of gold, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, lanthanum in copper concentrates. Inductively coupled plasma mass spectrometry method(ICP-MS)
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SN/T 4243-2015
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Basic data Standard ID | SN/T 4243-2015 (SN/T4243-2015) | Description (Translated English) | Determination of gold, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, lanthanum in copper concentrates. Inductively coupled plasma mass spectrometry method(ICP-MS) | Sector / Industry | Commodity Inspection Standard (Recommended) | Classification of Chinese Standard | H13 | Classification of International Standard | 77.120.60 | Word Count Estimation | 10,172 | Date of Issue | 2015-05-26 | Date of Implementation | 2016-01-01 | Quoted Standard | GB/T 602; GB/T 6379.2; GB/T 6682; GB/T 8170; GB/T 14263 | Regulation (derived from) | State Quality-Inspection-Accreditation [2015] No.224 | Issuing agency(ies) | General Administration of Customs | Summary | This standard specifies the gold in copper concentrates, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, lanthanum of inductively coupled plasma mass spectrometry (ICP-MS) spectrometry. This standard applies to gold in copper concentrates, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, quantitative determination of lanthanum, its measurement range shown in Table 1. |
SN/T 4243-2015: Determination of gold, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, lanthanum in copper concentrates. Inductively coupled plasma mass spectrometry method(ICP-MS)
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(Copper concentrate in gold, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, lanthanum measured by Inductively Coupled Plasma Mass Spectrometry)
People's Republic of China Entry-Exit Inspection and Quarantine Standards
In copper concentrates, gold, silver, platinum, palladium, arsenic, mercury, cadmium, gallium,
Inductively coupled indium, germanium, selenium, tellurium, thallium, lanthanum
Plasma Mass Spectrometry
Determinationofgold, silver, platinum, paladium, arsenic, mercury, cadmium,
galium, indium, germanium, selenium, telurium, thalium, lanthanumincopper
concentrates-Inductivelycoupledplasmamassspectrometrymethod (ICP-MS)
Issued on. 2015-05-26
2016-01-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Jiangsu Entry-Exit Inspection and Quarantine Bureau, People's Republic of China Entry-Exit Inspection and Gansu
Quarantine Bureau.
The main drafters of this standard. Zhao, Yan Na, Ya-Hui Feng, Zhao Shengguo, Li Jianjun, Zheng Hongwen.
In copper concentrates, gold, silver, platinum, palladium, arsenic, mercury, cadmium, gallium,
Inductively coupled indium, germanium, selenium, tellurium, thallium, lanthanum
Plasma Mass Spectrometry
1 Scope
This standard specifies the gold in copper concentrates, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, lanthanum of inductively coupled plasma mass spectrometry
(ICP-MS) spectrometry.
This standard applies to gold in copper concentrates, silver, platinum, palladium, arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, quantitative determination of lanthanum, its measurement range, see
Table 1.
Table 1 Unit measurement range of each element in milligrams per kilogram
Platinum and Palladium gold and silver elements Hg, Cd,
Determine
range
0.0050 ~ ~ 2.000.0050 2.000.0050 2.000.0050 ~ ~ ~ 2.00 0.50 20.00 200.0 0.050 - 0.50 to 200.0
Elements Ga Selenium and Tellurium Lanthanum Thallium
Determine
range
0.50 to 200.0 0.50 200.0 0.50 200.0 2.00 200.0 0.50 200.0 0.50 200.0 0.50 to 200.0
2 Normative references
The following documents for the application of this document is essential. And all documents cited a date, only the edition is applicable to this article
Member. For undated references, the latest edition (including any amendments) applies to this document.
Preparation of standard solution of GB/T 602 Determination of impurities in chemical reagents
GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat
Of the basic methods of reproduction
Laboratory use specifications and test methods GB/T 6682 Analysis
GB/T 8170 repair value expressed about the rules and limit values and judgment
GB/T 14263 bulk flotation of copper concentrate sampling, sample preparation method
Principle 3
The sample was mixed with the mixed flux, high temperature melting. Gold, silver, platinum, palladium elements separated by four metals lead capture and other elements,
Get precious metals together tablets, dissolved in aqua regia and nitric acid were used together precious metals silver and gold grains obtained was measured, platinum, palladium solution; sample was dissolved in aqua regia directly
Solution to obtain a solution of arsenic, mercury, cadmium, gallium, indium, germanium, selenium, tellurium, thallium, and ten other elements lanthanum determination. By inductively coupled plasma mass spectrometer
(ICP-MS) and the determination of the value of the signal elements in solutions, the use of external standard.
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