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Determination method of formaldehyde emission of wood-based panels and finishing products. High performance liquid chromatography method
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SN/T 4129-2015
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Basic data Standard ID | SN/T 4129-2015 (SN/T4129-2015) | Description (Translated English) | Determination method of formaldehyde emission of wood-based panels and finishing products. High performance liquid chromatography method | Sector / Industry | Commodity Inspection Standard (Recommended) | Classification of Chinese Standard | B70 | Classification of International Standard | 79.060 | Word Count Estimation | 8,820 | Date of Issue | 2015-02-09 | Date of Implementation | 2015-09-01 | Quoted Standard | GB/T 6682; LY/T 1612 | Regulation (derived from) | State-Quality-Inspection-Accreditation [2015] 59 | Issuing agency(ies) | General Administration of Customs | Summary | This standard specifies the wood-based panel products formaldehyde emission was measured by high performance liquid chromatography. This standard applies to the determination of plywood and their products formaldehyde emission. |
SN/T 4129-2015: Determination method of formaldehyde emission of wood-based panels and finishing products. High performance liquid chromatography method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(Determination of plywood and their products formaldehyde emission HPLC)
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Products and wood-based panels Determination of formaldehyde emission
High Performance Liquid Chromatography
Issued on. 2015-02-09
2015-09-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
Please note that some of the content of this document may involve patents. Distribution of this document
Institutions do not assume the responsibility to identify these patents.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Shandong Entry Inspection and Quarantine Bureau, People's Republic of China Guangdong Entry-Exit Inspection and
Quarantine Bureau.
The main drafters of this standard. Han Jingwei, Zhang Zhihui, Xu Meiling, Guoren Hong, WANG Zheng, Yang Juan, Dong Lijun, Sun Jingzhong.
Products and wood-based panels Determination of formaldehyde emission
High Performance Liquid Chromatography
1 Scope
This standard specifies the wood-based panel products formaldehyde emission was measured by high performance liquid chromatography.
This standard applies to the determination of plywood and their products formaldehyde emission.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
LY/T 1612 formaldehyde emission detection 1m3 climate chamber
3 Method summary
The surface area of 1m2 of sample into the temperature, relative humidity, air velocity and air exchange rate was controlled at a certain value of the climate chamber. Armor
Aldehyde released from the sample, mixed with air inside, regular sampling of air inside the air extracted by absorption bottle filled with distilled water, air
All formaldehyde gas dissolved in water; after absorbing liquid formaldehyde and 2,4-dinitrophenylhydrazine derivatization process, the direct use of high performance liquid chromatography
Spectrum Determination of formaldehyde content.
4 Reagents
Unless otherwise stated, the use of water as the only three confirmed analytically pure reagents and GB/T 6682 stipulated or deionized water.
4.1 acetic acid. AR.
4.2 2,4-dinitrophenylhydrazine. AR, CAS number. 119-26-6 Chemical formula. (NO2) 2C6H3NH2NH.
4.3 acetonitrile. chromatography.
4.4 2,4-dinitrophenylhydrazine solution (0.5mg/mL). Weigh accurately 50mg (accurate to 1mg) 2,4- dinitrophenylhydrazine (4.2) in 100mL capacity
Flask, was added 0.5mL of acetic acid (4.1) with acetonitrile (4.3) and dissolve to volume.
4.5 Formaldehyde standard solution. 100mg/L.
4.6 formaldehyde standard solution. Pipette 15mL formaldehyde standard solution (4.5) in 100mL flask, the water volume of the standard solution
Formaldehyde concentration of 15mg/L.
5 Apparatus and materials
5.1 High performance liquid chromatograph. with diode array detector (DAD) or UV - visible detector (UV-VIS).
5.2 constant temperature water bath. (60 ± 2) ℃.
5.3 Analysis of balance. a sense of the amount of 1mg.
5.4 filter. 0.45μm organic membrane filters, syringe or other forms.
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