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SN/T 2260-2010: Determination chemical compounds of copper cathode. Photoelectric emission spectroscopic method
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Determination chemical compounds of copper cathode. Photoelectric emission spectroscopic method
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Basic data | Standard ID | SN/T 2260-2010 (SN/T2260-2010) | | Description (Translated English) | Determination chemical compounds of copper cathode. Photoelectric emission spectroscopic method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | H13 | | Classification of International Standard | 77.120.30 | | Word Count Estimation | 8,884 | | Date of Issue | 2010-01-10 | | Date of Implementation | 2010-07-16 | | Quoted Standard | GB/T 6682-2008 | | Regulation (derived from) | National Quality Inspection [2010] No. 13 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the method of using optical emission spectroscopic determination of standard high purity copper cathode and copper cathode arsenic, antimony, bismuth, sulfur, selenium, tellurium, iron, silver, tin, nickel, lead, zinc, chromium, cadmium, cobalt, silicon, phosphorus and manganese content. This standard applies to the standard high purity copper cathode and copper cathode arsenic, antimony, bismuth, sulfur, selenium, tellurium, iron, silver, tin, nickel, lead, zinc, chromium, cadmium, cobalt, silicon, phosphorus and manganese content determination. | SN/T 2260-2010: Determination chemical compounds of copper cathode. Photoelectric emission spectroscopic method
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Determination chemical compounds of copper cathode.Photoelectric emission spectroscopic method
Exit inspection and quarantine industry standard book People's Republic of China
Determination of the chemical composition of copper cathode
Optical Emission Spectrometry
Issued on. 2010-01-10
2010-07-16 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
Appendix A of this standard is an informative annex.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Shanghai Entry-Exit Inspection and Quarantine Bureau, People's Republic of China Entry-Exit Inspection and Anhui
Quarantine Bureau.
The main drafters of this standard. Feng Jian, Sun Zhian, Gong Siwei, Li Dejun.
This standard is the first release of the entry-exit inspection and quarantine industry standards.
Determination of the chemical composition of copper cathode
Optical Emission Spectrometry
1 Scope
This standard specifies the method for determination of spectral purity copper cathode and copper cathode standard of arsenic, antimony, bismuth, sulfur, selenium, tellurium, iron with photoemission,
Silver, tin, nickel, lead, zinc, chromium, cadmium, cobalt, silicon, phosphorus and manganese.
This standard applies to high purity copper cathode and copper cathode standard of arsenic, antimony, bismuth, sulfur, selenium, tellurium, iron, silver, tin, nickel, lead, zinc, chromium, cadmium, cobalt, silicon,
Determination of phosphorus and manganese content. Determination of the range in Table 1.
Table 1 Determination of copper cathode in the range of impurity elements%
Element measurement range (mass fraction) element measurement range (mass fraction)
As 0.00001 ~ 0.0150 Sb 0.00001 ~ 0.0200
Bi 0.00001 ~ 0.0050 S 0.00001 ~ 0.0100
Se 0.00001 ~ 0.0050 Te 0.00001 ~ 0.0100
Fe 0.00001 ~ 0.0100 Ag 0.00010 ~ 0.0100
Sn 0.00001 ~ 0.0100 Ni 0.00001 ~ 0.0100
Pb 0.00001 ~ 0.0100 Zn 0.00010 ~ 0.0100
Cr 0.00001 ~ 0.0100 Cd 0.00010 ~ 0.0050
Co 0.00010 ~ 0.0100 Si 0.00010 ~ 0.0100
P 0.00010 ~ 0.0100 Mn 0.00010 ~ 0.0050
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
Laboratory use specifications and test methods GB/T 6682-2008 Analysis
3 Method summary
The sample was processed as an electrode, the sample with the excitation system and the counter electrode excitation light, and the beam splitting system is introduced,
Through the dispersion element is decomposed into a linear spectrum. The intensity of the internal standard line and a selected line of analysis photoelectrically converted and measured according to the standard sample
Standard curve, the computer automatically collect excitation strength values and calculate the amount of analyte in the sample analysis.
4 Reagents and materials
4.1 Water, GB/T 6682-2008 4.2 specified secondary water.
4.2 hydrochloric acid, pure class distinctions.
4.3 hydrochloride, (1 + 10).
4.4 Analytical grade absolute ethanol.
5. Apparatus
5.1 Optical Emission Spectrometer. Instruments used argon purity ≥99.999%, and the pressure and flow rate of argon gas must be kept constant. The instrument should be
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