US$339.00 · In stock Delivery: <= 4 days. True-PDF full-copy in English will be manually translated and delivered via email. SN/T 2249-2023: (Determination of 34 plasticizers in plastic raw materials and their products by gas chromatography-mass spectrometry) Status: Valid SN/T 2249: Evolution and historical versions
Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
SN/T 2249-2023 | English | 339 |
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4 days [Need to translate]
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(Determination of 34 plasticizers in plastic raw materials and their products by gas chromatography-mass spectrometry)
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SN/T 2249-2023
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SN/T 2249-2009 | English | 399 |
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3 days [Need to translate]
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Determination of phthalates in plastics and plastic articles. Gas chromatography-mass spectrometry(GC-MS)method
| Obsolete |
SN/T 2249-2009
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PDF similar to SN/T 2249-2023
Basic data Standard ID | SN/T 2249-2023 (SN/T2249-2023) | Description (Translated English) | (Determination of 34 plasticizers in plastic raw materials and their products by gas chromatography-mass spectrometry) | Sector / Industry | Commodity Inspection Standard (Recommended) | Classification of Chinese Standard | G31 | Classification of International Standard | 83.080.01 | Word Count Estimation | 16,161 | Date of Issue | 2023-05-05 | Date of Implementation | 2023-12-01 | Issuing agency(ies) | General Administration of Customs |
SN/T 2249-2009: Determination of phthalates in plastics and plastic articles. Gas chromatography-mass spectrometry(GC-MS)method ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of phthalates in plastics and plastic articles.Gas chromatography-mass spectrometry (GC-MS) method
Exit inspection and quarantine industry standard book People's Republic of China
Plastics and articles Phthalates
Determination of Plastics by Gas Chromatography - Mass Spectrometry
Posted 2009-02-20
2009-09-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
Appendix A of this standard is a normative appendix, Appendix B and Appendix C are informative appendix.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard by the People's Republic of China SZCIQ responsible for drafting.
The main drafters of this standard. Wang Chengyun, Zhang Ya, Liu Li, Mak Chi-hi, Wu Jingwu.
This standard is the first release of the entry-exit inspection and quarantine industry standards.
Plastics and articles Phthalates
Determination of Plastics by Gas Chromatography - Mass Spectrometry
1 Scope
This standard specifies the plastic and its products in 12 kinds of phthalate plasticizers gas chromatography - mass spectrometry method.
This standard applies to 12 kinds of plastic products and the determination of phthalate plasticizers. Phthalate plasticizers sub
Substructure is. R1-CO2-C6H4-CO2-R2.12 plasticizers English name, CAS number, and the formula given in Appendix A.
Principle 2
Sample using ethyl acetate as the extraction solvent, the extraction, after extraction fluid volume by gas chromatography - mass spectrometry determination, internal standard method
Quantified.
3 Reagents and materials
Unless otherwise specified, the reagents used were of analytical grade should be.
3.1 ethyl acetate.
3.2 Phthalates standard. Purity ≥97%.
3.3 plasticizer standard stock solution. Weigh accurately respectively dimethyl phthalate (DMP) standard (3.2), diethyl phthalate
(DEP) standard (3.2), dibutyl phthalate ester (DPRP) standard (3.2), di-isobutyl phthalate (DIBP) standard
(3.2), dibutyl phthalate (DBP) standard (3.2), di-n-hexyl ester (DHxP) standard (3.2), phthalic acid
Butyl benzyl phthalate (the BBP) standard (3.2) phthalate, dicyclohexyl phthalate (of DCHP) standard (3.2), bis (2-ethylhexyl) phthalate
(DEHP) standard (3.2) phthalate, di-n-octyl phthalate (DNOP) standard (3.2) each 10.0mg, diisononyl phthalate
(DINP) standard (3.2) and diisodecyl phthalate (DIDP) standard (3.2) each 100.0mg, were placed in 100mL capacity
Flask, dilute to the mark with ethyl acetate (3.1), and mix.
3.4 Internal standard. diamyl phthalate (DAP) (diamylphthalate, referred to as the DAP). purity ≥97%.
3.5 standard internal standard stock solution. accurately weighed amount of amyl phthalate (DAP) standard (3.4), with ethyl acetate (3.1)
Preparation of a concentration of 0.10mg/mL standard stock solution.
3.6 mixed standard working solution. Apply the standard internal standard stock solution (3.5), a plasticizer standard stock solution (3.3), if necessary with ethyl
Acid ethyl ester (3.1) diluted to a mixed standard working solution suitable concentration.
3.7 Internal standard solution. take appropriate internal standard stock solution (3.5), diluted to the appropriate concentration was necessary with ethyl acetate (3.1).
3.8 organic membranes. 0.45μm.
4 Instrument
4.1 Gas chromatography - mass spectrometry (GC-MS). Hotels EI source.
4.2 Analysis of balance. a sense of the amount of 0.1mg.
4.3 microwave extraction instrument.
4.4 flask. 10mL, 50mL, 100mL.
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