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Food contact materials. Pulp, paper and board. Determination of 7specified polychlorinated biphenyls(PCBs)
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SN/T 2200-2008
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Basic data | Standard ID | SN/T 2200-2008 (SN/T2200-2008) | | Description (Translated English) | Food contact materials. Pulp, paper and board. Determination of 7specified polychlorinated biphenyls(PCBs) | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | Y33 | | Classification of International Standard | 85.080 | | Word Count Estimation | 14,118 | | Date of Issue | 2008-11-18 | | Date of Implementation | 2009-06-01 | | Quoted Standard | GB/T 450; GB/T 740 | | Adopted Standard | EN ISO 15318-1999, IDT | | Regulation (derived from) | National Quality Inspection [2008] No. 577 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the contact with food pulp, paper and paperboard in seven specified polychlorinated biphenyls (PCBs) measurement method. This standard applies to contact with food pulp, paper and paperboard in seven specified polychlorinated biphenyls (PCBs) determination. | SN/T 2200-2008: Food contact materials. Pulp, paper and board. Determination of 7specified polychlorinated biphenyls(PCBs)
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Food contact materials.Pulp, paper and board.Determination of 7specified polychlorinated biphenyls (PCBs)
Exit inspection and quarantine industry standard book People's Republic of China
Food contact materials pulp, paper and paperboard
Determination of 7 specified polychlorinated biphenyls
Posted 2008-11-18
2009-06-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard is equivalent to using ENISO 15318.1999 "Pulp, paper and paperboard of seven designated PCBs Determination" (in English).
For ease of use, made according to the provisions of this standard GB/T 1.1-2000 and GB/T 20001.4-2001 following editorial changes.
--- Deleting the introduction of the European standards "on the conventional analysis, the results of the analysis if less than 50% of the current limit can be omitted 4.10.5
And in step 7.3.4, and 7.4 in the analysis step to be modified. Response analysis step in the measurement report changes into
Explained. If a dispute, you should use a comprehensive approach, "this part of the text. Reason for the European standard does not describe how sentence
Off "analysis less than 50% of the current limit" This section is intended to unknown language and the use of the standard had no effect;
--- The standard Chapter 1 to Chapter 5, respectively ENISO 15138.1999 Chapter 1 to Chapter 5; Chapter 7 of this standard correspondence
ENISO 15138.1999 of Chapters 7 and 8, this standard Chapter 8 to Chapter 11, respectively ENISO 15138.
Chapter 9 to Chapter 12, 1999. Above modifications in order to ensure a reasonable standard configuration;
--- Removed ENISO 15138.1999 in "conventional laboratory equipment 4.1" and 5.6 "than samples";
--- Delete "4 reagent" in the "Methanol can be replaced by ethanol." This statement;
--- Add "seven kinds of PCBs measured standard sample chromatogram designated" as the present standard Appendix D, is an informative annex, to help with
Body operators to use this standard.
The Standard Appendix A, Appendix B, Appendix C, Appendix D is an informative annex.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Shanghai Entry-Exit Inspection and Quarantine Bureau, People's Republic of China Beijing Entry-Exit Inspection and
Quarantine Bureau.
The main drafters of this standard. Zhou Yuyan, Yang Yong, Ma, Lu Xiaoyu.
This standard is the first release of the entry-exit inspection and quarantine industry standards.
Introduction
Stop using polychlorinated biphenyls (PCB) in 1971 before, PCB as a raw material present in the NCR. Since some paper
These contain carbon, so the recycled pulp with the PCB, may result in contamination of paper and paperboard.
Some PCB pollutants PCB congeners used in earlier NCR, which also can be seen as PCB pollution.
This standard, designated on Seven PCB congeners (PCB18,28,52,101,138,153 and 180) were measured separately. due to
PCB congeners can be considered as PCB sources, the paper can be estimated by the total content of these seven PCB congeners content.
Food contact materials pulp, paper and paperboard
Determination of 7 specified polychlorinated biphenyls
1 Scope
This standard specifies the method for determination of contact with the food pulp, paper and paperboard of seven specified polychlorinated biphenyls (PCBs) in.
This standard applies to the determination of contact with the food pulp, paper and paperboard of seven specified polychlorinated biphenyls (PCBs) in.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard provisions of this standard. For cited documents with dates, with its
After all of the amendments (excluding corrections) or revisions do not apply to this standard, however, encourage the agreement reached in accordance with this standard into
Parties to study the latest versions of these documents. For undated references, the latest edition of the standard.
GB/T 450 paper and cardboard to take samples and specimens to the vertical and horizontal, positive and negative determination (GB/T 450-2008, ISO 186.2002,
MOD)
GB/T 740 pulp samples taken (GB/T 740-2003, ISO 7213. 1981, IDT)
Principle 3
Potassium hydroxide ethanol solution to be tested is boiled PCBs extracted from the paper. After the extract was mixed with water, a one-time solution - Solid
Distribution C18 solid phase extraction column, then eluted with n-hexane or iso-octane.
N-hexane phase containing PCBs use with electron capture detector (ECD) or mass selective detector (MSD) of a given capillary gas chromatography
the amount. Each of the seven PCB congeners PCB standard peak shape and peak physiognomy comparison, if the peak shape is consistent, the total content of the PCB by PCB congeners
Content estimates obtained.
4 instruments and equipment
4.1 Examples of extraction apparatus, see Appendix A, which contains a length of about 200mm, an inner diameter of 30mm glass tube. By the end of the glass tube
Gradient fine in order to ensure air-tightness of the disposable SPE column connected at its top and the formation of droplets.
4.2 disposable SPE, C18 bonded phase (size of 3.0mL, 200mg).
4.3 Gas chromatograph. equipped with electron capture detector (ECD) or mass selective detector (MSD).
5 Reagents
Unless otherwise specified, all reagents were of analytical grade, double distilled water or water of equivalent purity.
5.1 Ethanol. purity ≥99.5%.
5.2 methanol. purity ≥99.8%.
5.3 hexane. purity ≥98.0%.
5.4 Concentrated sulfuric acid. a density of about 1.84.
5.5 potassium hydroxide.
5.6 standard sample. purity ≥99.5%.
5.6.1 2,2 ', 5-trichlorobiphenyl (PCB18, BalschmitNomenclature coding).
5.6.2 trichloro biphenyl (PCB28, BalschmitNomenclature coding).
5.6.3 2,2 ', 5,5'-tetrachlorobiphenyl (PCB52, BalschmitNomenclature coding).
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