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Determination of impurities in copper concentrates for import.Inductively coupled plasma atomic emission spectrometry
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SN/T 2047-2008
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Basic data | Standard ID | SN/T 2047-2008 (SN/T2047-2008) | | Description (Translated English) | Determination of impurities in copper concentrates for import.Inductively coupled plasma atomic emission spectrometry | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | H11 | | Word Count Estimation | 8,838 | | Date of Issue | 2008-04-29 | | Date of Implementation | 2008-11-01 | | Quoted Standard | GB/T 602; GB/T 14263 | | Regulation (derived from) | Industry standard filing Notice 2008 No. 7 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the imported copper concentrates of lead, zinc, cobalt, nickel, magnesium, cadmium, arsenic, antimony, bismuth, mercury and other elements in the method. This standard applies to imports of copper concentrates of lead, zinc, cobalt, nickel, magnesium, cadmium, arsenic, antimony, bismuth, mercury and other elements in the determination of the measurement range of each element are shown in Table 1. | SN/T 2047-2008: Determination of impurities in copper concentrates for import.Inductively coupled plasma atomic emission spectrometry
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Determination of impurities in copper concentrates for import.Inductively coupled plasma atomic emission spectrometry
Exit inspection and quarantine industry standard book People's Republic of China
Determination of impurity elements in imports of copper concentrate
Inductively coupled plasma atomic emission spectrometry
Posted 2008-04-29
2008-11-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
The Standard Annexes A and B are informative appendices.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard is mainly drafted by. People's Republic of China Anhui CIQ.
The main drafters of this standard. Ma Hongyan, Sunzhi An, Li Dejun, Wang Wei.
This standard is the first release of the entry-exit inspection and quarantine industry standards.
Determination of impurity elements in imports of copper concentrate
Inductively coupled plasma atomic emission spectrometry
1 Scope
This standard specifies the method for determination of copper concentrate imports of lead, zinc, cobalt, nickel, magnesium, cadmium, arsenic, antimony, bismuth, mercury and other nutrient contents.
This standard applies to the determination of imported copper concentrates of lead, zinc, cobalt, nickel, magnesium, cadmium, arsenic, antimony, bismuth, mercury and other elements in the content determination of each element Fan
Wai in Table 1.
Table 1 of the elements of the measurement range in%
Element measurement range (mass fraction)
Lead 0.01 to 6.0
Zinc 0.01 to 6.0
0.01 to 2.0 cobalt
Nickel 0.005 to 1.0
Magnesium 0.001 to 3.0
Element measurement range (mass fraction)
Cadmium 0.001 to 0.5
Arsenic 0.005 to 1.5
Sb 0.01 to 1.0
Bismuth 0.01 to 0.5
Mercury 0.001 to 0.1
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
Preparation of standard solution of GB/T 602 Determination of impurities in chemical reagents
GB/T 14263 bulk flotation of copper concentrate sampling, sample preparation method
3 Method summary
Sample after microwave digestion using inductively coupled plasma atomic emission spectrometer content of each element.
4 Reagents
Unless otherwise stated, when analyzed using recognized as analytical grade reagents and distilled water or equivalent purity.
Nitrate 4.1 (ρ1.42g/mL).
4.2 hydrochloride (ρ1.19g/mL).
4.3 mixed acid (hydrochloric acid. nitric acid = 3.2).
4.4 mixed acid (1 + 9). the mixed acid (4.3) prepared by diluting.
4.5 single element standard solution. the elements lead, zinc, cobalt, nickel, magnesium, cadmium, arsenic, antimony, bismuth, mercury standard solution according to GB/T 602 method of preparation, or
Direct use of standard materials, which are concentration 10mg/mL.
4.6 mixed standard solution. Pipette lead, the elements zinc, cobalt, nickel, magnesium, cadmium, arsenic, antimony, bismuth, mercury standard stock solution (4.5) into a number of
100mL volumetric flask, dilute with mixed acid (4.4) and to volume, and mix.
5. Apparatus
5.1 Inductively coupled plasma atomic emission spectrometer. The instrument should be able to provide a stable plasma flame torch. Stability of the instrument must comply
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