|
US$609.00 · In stock
Delivery: <= 4 days. True-PDF full-copy in English will be manually translated and delivered via email.
SN/T 1922-2007: Determination of residues of paracetamol and acetylsalic acid in foodstuffs of animal origin for import and export. LC-MS/MS method
Status: Valid
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 1922-2007 | English | 609 |
Add to Cart
|
4 days [Need to translate]
|
Determination of residues of paracetamol and acetylsalic acid in foodstuffs of animal origin for import and export. LC-MS/MS method
| Valid |
SN/T 1922-2007
|
PDF similar to SN/T 1922-2007
Basic data | Standard ID | SN/T 1922-2007 (SN/T1922-2007) | | Description (Translated English) | Determination of residues of paracetamol and acetylsalic acid in foodstuffs of animal origin for import and export. LC-MS/MS method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | C53 | | Classification of International Standard | 67.020 | | Word Count Estimation | 19,149 | | Date of Issue | 2007-05-23 | | Date of Implementation | 2007-12-01 | | Regulation (derived from) | National-accreditation-Science [2011] 63 | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the animal-derived foods acetaminophen, acetylsalicylic acid residues adjacent liquid chromatography mass spectrometry/mass spectrometry. This standard applies to animal tissues, organs, eggs and milk acetaminophen, o- acetylsalicylic acid residues detected. | SN/T 1922-2007: Determination of residues of paracetamol and acetylsalic acid in foodstuffs of animal origin for import and export. LC-MS/MS method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of residues of paracetamol and acetylsalic acid in foodstuffs of animal origin for import
Exit inspection and quarantine industry standard book People's Republic of China
Import and export of animal-derived foods acetaminophen,
O-acetylsalicylic acid residues in the detection method
Liquid chromatography - mass spectrometry/mass spectrometry
Posted 2007-05-23
2007-12-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
The Standard Appendix A and Appendix B is an informative annex.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard by the Chinese Academy of Inspection and Quarantine, Shenzhen People's Republic of China Exit Inspection and Quarantine is responsible for drafting.
The main drafters of this standard. Peng Tao, Yu Jing, Li Xiaojuan, Yuezhen Feng, Li Jianzhong, Guo Wei, Tang Ying Zhang, Chu Xiaogang.
This standard is the first release of the entry-exit inspection and quarantine industry standards.
Import and export of animal-derived foods acetaminophen,
O-acetylsalicylic acid residues in the detection method
Liquid chromatography - mass spectrometry/mass spectrometry
1 Scope
This standard specifies the paracetamol, o-acetylsalicylic acid residues in food of animal origin liquid chromatography on - mass spectrometry/mass spectrometry.
This standard applies to animal tissues, organs, eggs and milk to detect acetaminophen, o-acetylsalicylic acid residues.
2 Sample Preparation and Storage
2.1 animal tissues and organs
Samples taken from the original representative sample of about 500g, with a full organization stamp mill crushed mix, are divided into two, respectively, into a clean container
As a sample, sealed and marked with tags. The sample was placed in -18 ℃ freezer stored.
2.2 Egg
Samples taken from the original representative sample of about 500g, peeled with a tissue after stirring thoroughly mixed stamp mill, are divided into two, respectively, into
Clean as a sample container, sealed and marked with tags. The sample was placed at 4 ℃ stored.
2.3 milk
Samples taken from the original representative sample of about 500g, with a stamp mill and mix well organized, are divided into two, respectively, into a clean container for
As a sample, sealed and marked with tags. The sample was placed at 4 ℃ stored.
In the sample preparation procedure, it should prevent sample contamination or the occurrence of the change of residue content.
3 Method summary
Samples were extracted with acetonitrile residual acetaminophen, o-acetylsalicylic acid (marker residue. salicylic acid), the n-hexane to remove fat,
After the solid-phase extraction (SPE), liquid chromatography - mass spectrometry/mass spectrometry, external standard.
4 Reagents and materials
Unless otherwise noted, all reagents were of analytical grade, water is deionized water or equivalent purity.
4.1 acetonitrile. HPLC fractions.
4.2 hexane. HPLC fractions.
4.3 Methanol. HPLC fractions.
4.4 phosphoric acid.
4.5 formic acid. HPLC fractions.
4.6 ammonium acetate.
4.7 acetonitrile saturated with n-hexane. 100mL to 100mL acetonitrile was added n-hexane, followed by sufficient shaking, standing layer, the upper layer of acetonitrile
spare.
4.8 0.1% aqueous formic acid (containing 0.5mmol/L ammonium acetate). The exact amount of formic acid and 1mL weighed 0.0386g ammonium acetate in 1L
Flask, water volume to 1L.
4.9 SPE eluent. 0.02mol/L phosphoric acid + methanol (80 + 20, volume ratio).
4.10 Standard. acetaminophen, purity ≥99%; salicylic acid, the purity of ≥99%.
4.11 standard stock solution. Weigh paracetamol, salicylic acid standard (accurate to 0.0001g), dissolve with acetonitrile, formulated as concentrated
Tips & Frequently Asked Questions:Question 1: How long will the true-PDF of SN/T 1922-2007_English be delivered?Answer: Upon your order, we will start to translate SN/T 1922-2007_English as soon as possible, and keep you informed of the progress. The lead time is typically 2 ~ 4 working days. The lengthier the document the longer the lead time. Question 2: Can I share the purchased PDF of SN/T 1922-2007_English with my colleagues?Answer: Yes. The purchased PDF of SN/T 1922-2007_English will be deemed to be sold to your employer/organization who actually pays for it, including your colleagues and your employer's intranet. Question 3: Does the price include tax/VAT?Answer: Yes. Our tax invoice, downloaded/delivered in 9 seconds, includes all tax/VAT and complies with 100+ countries' tax regulations (tax exempted in 100+ countries) -- See Avoidance of Double Taxation Agreements (DTAs): List of DTAs signed between Singapore and 100+ countriesQuestion 4: Do you accept my currency other than USD?Answer: Yes. If you need your currency to be printed on the invoice, please write an email to [email protected]. In 2 working-hours, we will create a special link for you to pay in any currencies. Otherwise, follow the normal steps: Add to Cart -- Checkout -- Select your currency to pay.
|