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JJG 1104-2015 English PDF

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JJG 1104-2015: Dynamic Light Scattering Particle Size Analyzers
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Basic data

Standard ID JJG 1104-2015 (JJG1104-2015)
Description (Translated English) Dynamic Light Scattering Particle Size Analyzers
Sector / Industry Metrology & Measurement Industry Standard
Classification of Chinese Standard A61
Classification of International Standard 17.02
Word Count Estimation 17,170
Date of Issue 2015-01-30
Date of Implementation 2015-04-30
Quoted Standard GB/T 19627-2005; GB/T 29022-2012
Regulation (derived from) The State Administration of Quality Supervision, Inspection and Quarantine Announcement 2015 No. 19
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine
Summary This Standard applies to dynamic light scattering method to measure liquid insoluble particles having an average particle size of the particle size analyzer initial verification, subsequent verification and the use of checks.

JJG 1104-2015: Dynamic Light Scattering Particle Size Analyzers

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Verification Regulation of Dynamic Light Scattering Particle Size Analyzers State verification procedures People's Republic of China Dynamic light scattering particle size analyzer Issued on. 2015-01-30 2015-04-30 implementation The State Administration of Quality Supervision, Inspection and Quarantine released Dynamic light scattering particle size analyzer test procedures zers Focal point. the National Technical Committee stoichiometric physical The main drafting units. China Institute of Metrology Participated in the drafting unit. Beijing Physical and Chemical Analysis Center This procedure commissioned the National Technical Committee of the stoichiometric physics responsible for the interpretation The main drafters of this procedure. Junjie Liu (China Institute of Metrology) Drafters participate. Zhang Ge (China Institute of Metrology) Zhou Su-hong (Beijing Physical and Chemical Analysis Center)

table of Contents

Introduction (Ⅱ) 1 Scope (1) 2. References (1) 3 Overview (1) 4 metering performance requirements (2) 5 General Requirements (2) 5.1 Visual inspection (2) 5.2 energizing check (2) 6 Control of measuring instruments (2) 6.1 Verification ambient conditions (2) 6.2 Calibration with standard materials and equipment (2) 6.3 Verification Project (2) 6.4 Verification Methods (3) 7 test results processing (4) 8 test cycle (4) Appendix A viscosity of pure water table (5) Appendix B of the refractive index of pure water (6) Preparation and Appendix C concentration select the sample (7) Appendix D test recording format (8) Appendix E calibration certificate/test results in the notice page format (9)

Introduction

The procedure to JJF1002-2010 "national verification procedures write rules", JJF1001-2011 "Universal Measurement Terms and definitions "as the basic norms develop. In making this procedure, reference is made to GB/T 29022-2012 size analysis by dynamic light scattering (DLS) (et With the use of ISO 22412.2008) and GB/T 19627-2005 Particle size analysis by photon correlation spectroscopy (identical with ISO 13321.1999) in part. This procedure is the first release. Dynamic light scattering particle size analyzer test procedures

1 Scope

The order applies to dynamic light scattering method to measure liquid insoluble particles having an average particle diameter of a particle size analyzer first seizure Set, and use the subsequent verification check. 2. References GB/T 19627-2005 size analysis photon correlation spectroscopy GB/T 29022-2012 size analysis by dynamic light scattering (DLS) For dated references, only the dated edition applies to this procedure; undated reference documents Member, the latest edition (including any amendments) applies to this procedure.

3 Overview

Dynamic light scattering particle size analyzer (hereinafter referred to as the instrument) measurement principle. When a monochromatic laser irradiation to be Sample to be measured, it will generate a certain intensity of scattered light at a certain angle. Since the liquid molecules suspended particles by random motion Impact and do irregular Brownian motion, so the observed intensity of scattered light will continue over time the ups and downs. Based on Brownian motion Stokes - Einstein equation, when the temperature of the suspension and the viscosity is known, through the analysis of these To evaluate the function of the scattered light intensity over time fluctuation of an average size of the particles (intensity weighted harmonic average particle diameter). The apparatus generally consists of a laser generator, an optical lens, and the sample cell temperature control tank, a photon detector, a signal processing unit, Calculate and display unit and other components, the structure shown in Figure 1. Figure 1 Schematic of typical dynamic light scattering particle size analyzer 1- laser generator; 2,5-optical lens; 3- sample cell; 4- temperature groove; 6- photon detector; θ- scattering angle; 7- signal processing unit; 8- calculation and display unit

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