GB/T 4103.13-2012_English: PDF (GB/T4103.13-2012)
Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
GB/T 4103.13-2012 | English | 169 |
Add to Cart
|
3 days [Need to translate]
|
Methods for chemical analysis of lead and lead alloys -- Part 13: Determination of aluminium content
| Valid |
GB/T 4103.13-2012
|
GB/T 4103.13-2000 | English | 199 |
Add to Cart
|
2 days [Need to translate]
|
Methods for chemical analysis of lead and lead alloys Determination of aluminium content
| Obsolete |
GB/T 4103.13-2000
|
Standard ID | GB/T 4103.13-2012 (GB/T4103.13-2012) | Description (Translated English) | Methods for chemical analysis of lead and lead alloys. Part 13: Determination of aluminium content | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | H13 | Classification of International Standard | 77.120.60 | Word Count Estimation | 7,714 | Older Standard (superseded by this standard) | GB/T 4103.13-2000 | Quoted Standard | GB/T 6682; GB/T 12806; GB/T 12808; GB/T 12809; GB/T 12810 | Drafting Organization | Zhuzhou Smelter Group Co., Ltd. | Administrative Organization | National Standardization Technical Committee of non-ferrous metals | Regulation (derived from) | National Standards Bulletin No. 41 of 2012 | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | Summary | This standard specifies the lead and lead alloys Determination of aluminum content. This standard applies to lead and lead alloys Determination of aluminum content. | Standard ID | GB/T 4103.13-2000 (GB/T4103.13-2000) | Description (Translated English) | Methods for chemical analysis of lead and lead alloys Determination of aluminium content | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | H13 | Classification of International Standard | 77.120.99 | Word Count Estimation | 4,464 | Date of Issue | 2000/8/28 | Date of Implementation | 2000/12/1 | Drafting Organization | Shenyang smelter | Administrative Organization | National Non-ferrous metals Standardization Technical Committee | Regulation (derived from) | National Standards Bulletin 2012 No. 41 | Summary | This Standard specifies determination of lead and lead alloy aluminum content. This Standard is applicable to lead, lead-calcium alloy, tin and lead-calcium bearing alloys Determination of aluminum content. Measurement range: 0. 0050% to 0. 10%. |
GB/T 4103.13-2012
ICS77.120.60
H13
National Standards of People's Republic of China
Replacing GB/T 4103.13-2000
Lead and lead alloys - Analysis
Part 13. Determination of aluminum content
Part 13. Determinationofaluminiumcontent
Issued on. 2013-10-01 2012-12-31 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 4103 "Methods for chemical analysis of lead and lead alloys" is divided into 16 parts.
--- Part 1. Determination of tin content;
--- Part 2. Determination of antimony content;
--- Part 3. Determination of copper content;
--- Part 4. Determination of iron content;
--- Part 5. Determination of bismuth content;
--- Part 6. Determination of arsenic content;
--- Part 7. Determination of the amount of selenium;
--- Part 8. Determination of tellurium content;
--- Part 9. Determination of calcium;
--- Part 10. Determination of the amount of silver;
--- Part 11. Determination of zinc content;
--- Part 12. Determination of thallium content;
--- Part 13. Determination of aluminum content;
--- Part 14. Determination of cadmium content by flame atomic absorption spectrometry;
--- Part 15. Determination of nickel content by flame atomic absorption spectrometry;
--- Part 16. copper, silver, bismuth, arsenic, antimony, tin, zinc contents Optical emission spectroscopy.
This is Part 13 GB/T 4103's.
This Part replaces GB/T 4103.13-2000 "of lead and lead alloys - Determination of aluminum content", and GB/T 4103.13-
Compared to 2000, the main changes are as follows.
--- Analysis of the color buffer system changes;
--- Supplementary terms of precision.
The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized.
This section is responsible for drafting unit. Zhuzhou Smelter Group Co., Ltd., Beijing Mining Research Institute, Shaanxi Dongling Smelting Co., Ltd., White
Silver colored copper Northwest Limited.
Participated in the drafting of this section. Henan Yuguang Gold & Lead Co., Ltd., Zhuzhou Smelter Group Co., Ltd., the gold Lingnan Shaoguan Smelter
Refinery.
The main drafters of this section. Zhou Junling, Majin Mei, Zhang Dongguang, to Delei, Yeshi Yuan, Huang Ping.
This Part replaces the previous editions are.
--- GB/T 4103.13-2000.
Lead and lead alloys - Analysis
Part 13. Determination of aluminum content
1 Scope
This section GB/T 4103 provisions of the determination of lead and lead alloy aluminum content.
This standard applies to the determination of lead and lead alloy aluminum content.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated edition applies to this article
Member. For undated references, the latest edition (including any amendments) applies to this document.
GB/T 6682 analytical laboratory use specifications and test methods (ISO 3696)
GB/T 12806 laboratory glassware single marking flask (ISO 1042)
GB/T 12808 laboratory glassware single marking pipette (ISO 648)
GB/T 12809 Laboratory glassware Glass Container design and construction principles (ISO 384)
GB/T 12810 laboratory glassware gauge capacity calibration and use (ISO 4787)
3 General
3.1 Unless otherwise stated, the use of analytical reagent only recognized in the analysis; the water is distilled or deionized water or equivalent purity,
Shall comply with the provisions of GB/T 6682's.
3.2 instruments shall be within the test cycle, the performance indicators should meet the technical parameters required for verification; glass containers GB/T 12808,
GB/T 12809, GB/T 12806 specified in Class A, with reference to the specific use requirements GB/T 12810 in.
4 The chrome Azure S Spectrophotometry
4.1 Determination of Range
This method is suitable for battery grids with lead calcium alloy ingots, secondary lead calcium alloy of aluminum content determination Determination of the range of 0.0050%
0.100%.
4.2 Principle
-EDTA Sample with dilute nitric acid dissolved in acetic acid - sodium acetate buffer solution, aluminum and chrome azure S generated purple complex in spectroscopic
Photometer at a wavelength of 555nm absorbance was measured obtaining. Fe3, Cu2 interference, can be added ascorbic acid, thiourea hidden.
4.3 Reagents
4.3.1 hydrochloric acid (ρ1.19g/mL).
4.3.2 nitrate (ρ1.42g/mL).
4.3.3 nitric acid (37).
......
|