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GB/T 4103.13-2012 English PDF (GB/T 4103.13-2000)

GB/T 4103.13-2012_English: PDF (GB/T4103.13-2012)
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GB/T 4103.13-2012English169 Add to Cart 3 days [Need to translate] Methods for chemical analysis of lead and lead alloys -- Part 13: Determination of aluminium content Valid GB/T 4103.13-2012
GB/T 4103.13-2000English199 Add to Cart 2 days [Need to translate] Methods for chemical analysis of lead and lead alloys Determination of aluminium content Obsolete GB/T 4103.13-2000


BASIC DATA
Standard ID GB/T 4103.13-2012 (GB/T4103.13-2012)
Description (Translated English) Methods for chemical analysis of lead and lead alloys. Part 13: Determination of aluminium content
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard H13
Classification of International Standard 77.120.60
Word Count Estimation 7,714
Older Standard (superseded by this standard) GB/T 4103.13-2000
Quoted Standard GB/T 6682; GB/T 12806; GB/T 12808; GB/T 12809; GB/T 12810
Drafting Organization Zhuzhou Smelter Group Co., Ltd.
Administrative Organization National Standardization Technical Committee of non-ferrous metals
Regulation (derived from) National Standards Bulletin No. 41 of 2012
Issuing agency(ies) General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Summary This standard specifies the lead and lead alloys Determination of aluminum content. This standard applies to lead and lead alloys Determination of aluminum content.

BASIC DATA
Standard ID GB/T 4103.13-2000 (GB/T4103.13-2000)
Description (Translated English) Methods for chemical analysis of lead and lead alloys Determination of aluminium content
Sector / Industry National Standard (Recommended)
Classification of Chinese Standard H13
Classification of International Standard 77.120.99
Word Count Estimation 4,464
Date of Issue 2000/8/28
Date of Implementation 2000/12/1
Drafting Organization Shenyang smelter
Administrative Organization National Non-ferrous metals Standardization Technical Committee
Regulation (derived from) National Standards Bulletin 2012 No. 41
Summary This Standard specifies determination of lead and lead alloy aluminum content. This Standard is applicable to lead, lead-calcium alloy, tin and lead-calcium bearing alloys Determination of aluminum content. Measurement range: 0. 0050% to 0. 10%.


GB/T 4103.13-2012 ICS77.120.60 H13 National Standards of People's Republic of China Replacing GB/T 4103.13-2000 Lead and lead alloys - Analysis Part 13. Determination of aluminum content Part 13. Determinationofaluminiumcontent Issued on. 2013-10-01 2012-12-31 implementation Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China Standardization Administration of China released Foreword GB/T 4103 "Methods for chemical analysis of lead and lead alloys" is divided into 16 parts. --- Part 1. Determination of tin content; --- Part 2. Determination of antimony content; --- Part 3. Determination of copper content; --- Part 4. Determination of iron content; --- Part 5. Determination of bismuth content; --- Part 6. Determination of arsenic content; --- Part 7. Determination of the amount of selenium; --- Part 8. Determination of tellurium content; --- Part 9. Determination of calcium; --- Part 10. Determination of the amount of silver; --- Part 11. Determination of zinc content; --- Part 12. Determination of thallium content; --- Part 13. Determination of aluminum content; --- Part 14. Determination of cadmium content by flame atomic absorption spectrometry; --- Part 15. Determination of nickel content by flame atomic absorption spectrometry; --- Part 16. copper, silver, bismuth, arsenic, antimony, tin, zinc contents Optical emission spectroscopy. This is Part 13 GB/T 4103's. This Part replaces GB/T 4103.13-2000 "of lead and lead alloys - Determination of aluminum content", and GB/T 4103.13- Compared to 2000, the main changes are as follows. --- Analysis of the color buffer system changes; --- Supplementary terms of precision. The non-ferrous metal part by the National Standardization Technical Committee (SAC/TC243) centralized. This section is responsible for drafting unit. Zhuzhou Smelter Group Co., Ltd., Beijing Mining Research Institute, Shaanxi Dongling Smelting Co., Ltd., White Silver colored copper Northwest Limited. Participated in the drafting of this section. Henan Yuguang Gold & Lead Co., Ltd., Zhuzhou Smelter Group Co., Ltd., the gold Lingnan Shaoguan Smelter Refinery. The main drafters of this section. Zhou Junling, Majin Mei, Zhang Dongguang, to Delei, Yeshi Yuan, Huang Ping. This Part replaces the previous editions are. --- GB/T 4103.13-2000. Lead and lead alloys - Analysis Part 13. Determination of aluminum content 1 Scope This section GB/T 4103 provisions of the determination of lead and lead alloy aluminum content. This standard applies to the determination of lead and lead alloy aluminum content. 2 Normative references The following documents for the application of this document is essential. For dated references, only the dated edition applies to this article Member. For undated references, the latest edition (including any amendments) applies to this document. GB/T 6682 analytical laboratory use specifications and test methods (ISO 3696) GB/T 12806 laboratory glassware single marking flask (ISO 1042) GB/T 12808 laboratory glassware single marking pipette (ISO 648) GB/T 12809 Laboratory glassware Glass Container design and construction principles (ISO 384) GB/T 12810 laboratory glassware gauge capacity calibration and use (ISO 4787) 3 General 3.1 Unless otherwise stated, the use of analytical reagent only recognized in the analysis; the water is distilled or deionized water or equivalent purity, Shall comply with the provisions of GB/T 6682's. 3.2 instruments shall be within the test cycle, the performance indicators should meet the technical parameters required for verification; glass containers GB/T 12808, GB/T 12809, GB/T 12806 specified in Class A, with reference to the specific use requirements GB/T 12810 in. 4 The chrome Azure S Spectrophotometry 4.1 Determination of Range This method is suitable for battery grids with lead calcium alloy ingots, secondary lead calcium alloy of aluminum content determination Determination of the range of 0.0050% 0.100%. 4.2 Principle -EDTA Sample with dilute nitric acid dissolved in acetic acid - sodium acetate buffer solution, aluminum and chrome azure S generated purple complex in spectroscopic Photometer at a wavelength of 555nm absorbance was measured obtaining. Fe3, Cu2 interference, can be added ascorbic acid, thiourea hidden. 4.3 Reagents 4.3.1 hydrochloric acid (ρ1.19g/mL). 4.3.2 nitrate (ρ1.42g/mL). 4.3.3 nitric acid (37). ......

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