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GB/T 32951-2016: Determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline content for organic fertilizers -- HPLC method
Status: Valid
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| GB/T 32951-2016 | English | 279 |
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Determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline content for organic fertilizers -- HPLC method
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GB/T 32951-2016
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PDF similar to GB/T 32951-2016
Basic data | Standard ID | GB/T 32951-2016 (GB/T32951-2016) | | Description (Translated English) | Determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline content for organic fertilizers -- HPLC method | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | G20 | | Classification of International Standard | 65.080 | | Word Count Estimation | 14,140 | | Date of Issue | 2016-08-29 | | Date of Implementation | 2017-03-01 | | Regulation (derived from) | National Standard Notice No. 14 of 2016 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | GB/T 32951-2016: Determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline content for organic fertilizers -- HPLC method
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of oxytetracyline, tetracyline, chlortetracycline and doxycycline content for organic fertilizers - HPLC method
ICS 65.080
G20
National Standards of People's Republic of China
Organic fertilizers in oxytetracycline, tetracycline, chlortetracycline with potency
Determination of the content of mycacin by high performance liquid chromatography
Determination ofoxytetracyline, tetracyline, chlortetracyclineanddoxycycline
2016-08-29 released
2017-03-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
China National Standardization Management Committee released
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
This standard is proposed by the China Petroleum and Chemical Industry Association.
This standard is regulated by the National Technical Committee on Standardization of Fertilizers and Soil Conditioners (SAC/TC105).
The drafting of this standard. Shanghai Chemical Industry Research Institute, Shanghai Entry-Exit Inspection and Quarantine Bureau of industrial products and raw materials testing technology center, Taizhou City
Product Quality Supervision and Inspection Institute, Shanghai Jiaotong University.
The main drafters of this standard. Zhou Hui, Zhou Yun, Sun Mingxing, business photo Cong, Ye Ping, Ma Ming, Min Hong, Shen Guoqing, Zhao Jie, Hong Liling.
Organic fertilizers in oxytetracycline, tetracycline, chlortetracycline with potency
Determination of the content of mycacin by high performance liquid chromatography
WARNING. The use of this standard may involve hazardous materials, operations and equipment, but this standard is not intended to be relevant to all
All questions are made. It is the responsibility of the user to establish safety and protective measures before use and to determine the relevant regulations.
The use of the system.
1 Scope
This standard specifies the high performance liquid chromatography (HPLC) method for the determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline in organic fertilizers.
This standard is applicable to the determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline in organic fertilizers and organic-inorganic compound fertilizers.
This standard does not apply to the determination of oxytetracycline, tetracycline, chlortetracycline and doxycycline in soybean cake fertilizer.
The detection limits of this method are. oxytetracycline 0.75mg/kg, tetracycline 0.75mg/kg, chlortetracycline 1.0mg/kg, strong mold
The amount of 0.75mg/kg.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
GB/T 6379.1 Accuracy of measurement methods and results (accuracy and precision) - Part 1. General and definitions
GB/T 6379.2 Accuracy of measurement methods and results (accuracy and precision) - Part 2. Determination of standard measurement methods
The basic method of sex and reproducibility
GB/T 6682 Analytical laboratory water specifications and test methods
3 principle
The oxytetracycline, tetracycline, chlortetracycline and doxycycline were extracted by Na2EDTA-Mclvaine-methanol extract, and the solid phase extraction column
Purification treatment after injection, high performance liquid chromatography UV detector determination, external standard quantitative.
4 reagents and materials
Unless otherwise stated, all reagents are of analytical grade and water is a primary water specified in GB/T 6682.
4.1 methanol. pure chromatography.
4.2 acetonitrile. pure chromatography.
4.3 disodium hydrogen phosphate (Na2HPO4 · 12H2O).
4.4 Citric acid (C6H8O7 · H2O).
4.5 disodium EDTA (Na2EDTA · 2H2O).
4.6 Hydrated oxalic acid (C2H2O4 · 2H2O).
4.7 disodium hydrogen phosphate solution. 0.4mol/L. Weigh 143.26g disodium hydrogen phosphate, dissolved in water, volume to 1000mL.
4.8 citric acid solution. 0.2mol/L. Weigh 42.03g citric acid, dissolved in water, set to 1000mL.
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