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US$399.00 · In stock Delivery: <= 3 days. True-PDF full-copy in English will be manually translated and delivered via email. GB/T 22462-2008: Nano, Sub-micron scale film on steel -- Quantitative depth profile analysis -- Glow discharge atomic emission spectrometry Status: Valid
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Nano, Sub-micron scale film on steel -- Quantitative depth profile analysis -- Glow discharge atomic emission spectrometry
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GB/T 22462-2008
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PDF similar to GB/T 22462-2008
Basic data | Standard ID | GB/T 22462-2008 (GB/T22462-2008) | | Description (Translated English) | Nano, Sub-micron scale film on steel -- Quantitative depth profile analysis -- Glow discharge atomic emission spectrometry | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | G04 | | Classification of International Standard | 17.180 | | Word Count Estimation | 17,187 | | Date of Issue | 2008-10-30 | | Date of Implementation | 2009-06-01 | | Regulation (derived from) | Announcement of Newly Approved National Standards No. 17 of 2008 (No. 130 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the quantitative determination of nano- steel surface, sub-micron scale thin-film (metal coating and the oxide film) in thickness, the coating quality (per unit area) and the depth distribution of the elements of the film. This method is applicable to the determination of a thickness of 3nm ~ 1000nm steel surface film, suitable elements include: iron, chromium, nickel, copper, titanium, manganese, aluminum, carbon, phosphorus, oxygen, nitrogen and silicon. |
GB/T 22462-2008: Nano, Sub-micron scale film on steel -- Quantitative depth profile analysis -- Glow discharge atomic emission spectrometry ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Nano, Sub-micron scale film on steel.Quantitative depth profile analysis.Glow discharge atomic emission spectrometry
ICS 17.180
G04
National Standards of People's Republic of China
Steel surface nano, submicron films
Quantitative determination of element depth profile
Glow Discharge Atomic Emission Spectrometry
Posted 2008-10-30
2009-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Table of Contents
Introduction Ⅲ
1 Scope 1
2 Normative references 1
3 Terms and definitions
4 Principle 1
5 Apparatus 2
5.1 Overview 2
5.2 Instrument Performance Requirements 2
6 Sample Preparation 3
7 Procedure 3
7.1 Selection line 3
7.2 Optimization of glow discharge atomic emission spectrometer discharge parameters 3
7.3 curve 5
7.4 confirmation curve 7
7.5 drift correction 8
7.6 Sample Analysis 8
Analysis of the results indicates 8 8
8.1 Quantitative depth profiling of representation 8
8.2 and thickness of the coating mass (per unit area) measured 9
9 9 Precision
9 10 test reports
Appendix A (informative) Recommended elements characteristic of wavelengths 10
Annex B (informative) common oxide density 11
Annex C (normative) Additional Information 12 joint experiments
Foreword
The Standard Appendix A, Appendix B are informative annex, Annex C is normative appendix.
This standard by the National Standardization Technical Committee microbeam analysis made.
The standard micro-beam analysis by the National Standardization Technical Committee (SAC/TC38) centralized.
This standard is drafted by. Baoshan Iron & Steel Co., Ltd., Institute of Physics, Chinese Academy of Sciences, Institute of Chemistry, the rule of
Metallurgical Industry Information Standards Institute.
The main drafters. Zhang Yi, Chen Yingying, electric Shen Hong, Liu Fen, He Xiaolei, Vivian fly, Luan Yan.
Steel surface nano, submicron films
Quantitative determination of element depth profile
Glow Discharge Atomic Emission Spectrometry
1 Scope
This standard glow discharge atomic emission spectrometry for quantitative determination of the steel surface nano, submicron thin film (metal oxide coating
Film) in the thickness of the coating mass (per unit area) and the depth distribution of elements in the film.
This method is applicable to the determination of 3nm ~ 1000nm steel surface of the film thickness, the applicable elements include. iron, chromium, nickel, copper, titanium, manganese, aluminum,
Carbon, phosphorus, oxygen, nitrogen and silicon.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Study whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions
GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat
And basic methods of reproduction
GB/T 19502 Surface chemical analysis - Glow discharge optical emission spectrometry method General
GB/T 20066 Steel and iron - Sampling and determination of the chemical composition of the sample with a sample preparation method
GB/T 22461-2008 Surface chemical analysis - Vocabulary (ISO 18115.2001, IDT)
ISO 5725-3 measurement methods and results of Accuracy (trueness and precision) --- Part 3. Standard Methods of measurement precision
Intermediate measures (Accuracy (truenessandprecision) ofmeasurementmethodsandresults-Part 3. Intermedi-
atemeasuresoftheprecisionofastandardmeasurementmethod)
ISO 6955. 1982 - Flame emission spectroscopy analysis, atomic absorption and atomic fluorescence vocabulary (Analyticalspectro-
scopicmethods-Flameemission, atomicabsorption, andatomicfluorescence-Vocabulary)
3 Terms and Definitions
In ISO 6955. 1982 terms and definitions and GB/T 22461-2008 given apply to this standard.
Principle 4
The basic principle of glow discharge atomic emission spectrometry as follows.
a) a dc or rf glow light source device, cathode sputtering surface of the sample;
b) by ion sputtering and the energy generated in a glow discharge process the transfer, so that analyte atomization, and then in the plasma
Be excited;
c) The analysis of the elements characteristic spectral line emission intensities measured. When the depth of analysis, emission intensity is recorded as a function of time;
d) In-depth analysis by (quantitative) curve, the intensity function of time into the mass fraction of the sputtering depth letter
number. Known by measuring the composition of the reference sample sputtering rate can be established this calibration system.
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