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Coating powders -- Part 3: Determination of density by liquid displacement pycnometer
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GB/T 21782.3-2008
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Basic data | Standard ID | GB/T 21782.3-2008 (GB/T21782.3-2008) | | Description (Translated English) | Coating powders -- Part 3: Determination of density by liquid displacement pycnometer | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | A80 | | Classification of International Standard | 13.300 | | Word Count Estimation | 6,688 | | Date of Issue | 2008-05-12 | | Date of Implementation | 2008-09-01 | | Quoted Standard | GB/T 3186-2006; GB/T 21782.2-2008; ISO 787-10-1993; ISO 3696-1987 | | Adopted Standard | ISO 8130-3-1992, IDT | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This standard specifies the determination of the density of the powder coating liquid displacement pycnometer method. This method is based on the quality and the sample volume was measured. This method specifies the equipment is relatively cheap, but the liquid displacement pycnometer method may give incorrect results, especially in the powder with the liquid displacement is expanded, or replacement of the liquid is not completely replace the air in the powder particles. When the liquid displacement method uses slower than GB/T 21782. 2-2008 " compare the proportion of gas analyzer measured density (Arbitration Act) " is more inaccurate, but also in comparison with the gas specific gravity proven method to get the same result instrument when it is used this method. |
GB/T 21782.3-2008: Coating powders -- Part 3: Determination of density by liquid displacement pycnometer ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Coating powders Part 3. Determination of density by liquid displacement pyknometer
ICS 13.300
A80
National Standards of People's Republic of China
GB/T 21782.3-2008/ISO 8130-3.1992
Powder Coatings
Part 3. Determination of the density of liquid displacement pyknometer method
(ISO 8130-3.1992, IDT)
Posted 2008-05-12
2008-09-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
GB/T 21782 "powder coating" is divided into 14 parts, the structure and corresponding international standards are as follows.
--- Part 1. Determination of particle size distribution by sieving (ISO 8130-1.1992, IDT);
--- Part 2. Determination of density (Arbitration Act) compare the proportion of gas meter method (ISO 8130-2.1992, IDT);
--- Part 3. Determination of liquid displacement pycnometer density (ISO 8130-3.1992, IDT);
--- Part 4. Calculation of lower explosive limit (ISO 8130-4.1992, IDT);
--- Part 5. Powder/air mixture Determination of flow characteristics (ISO 8130-5.1992, IDT);
Measured at a given temperature thermosetting powder coating of gel time (ISO 8130-6..1992, IDT) --- Part 6;
--- Part 7. Determination (ISO 8130-7.1992, IDT) mass loss during baking;
--- Part 8. Evaluation of the storage stability of thermosetting powders (ISO 8130-8.1994, IDT);
--- Part 9. Sampling (ISO 8130-9.1992, IDT);
--- Part 10. Determination of deposition efficiency (ISO 8130-10.1998, IDT);
--- Part 11. ramp flow test (ISO 8130-11.1997, IDT);
--- Part 12. Determination of compatibility (ISO 8130-12.1998, IDT);
--- Part 13. Laser diffraction particle size analysis (ISO 8130-13.2001, IDT);
--- Part 14. Terminology (ISO 8130-14.2004, IDT).
This is Part 3 GB/T 21782 of.
This part identical with ISO 8130-3.1992 "powder coatings - Part 3. Determination of liquid displacement pycnometer density" (in English).
For ease of use, this section made the following editorial changes.
--- With "GB/T 3186-2006 Paints, varnishes and raw materials for paints and varnishes - Sampling (ISO 15528.2000, IDT)" instead of
"ISO 842. 1984 Paints and varnishes - Sampling of raw materials" (ISO 842. 1984 has been canceled, the ISO 15528.2000 Generation
for);
--- With "ISO 787-10.1993" instead of "ISO 787-10. 1981";
"." --- With a decimal point instead of a comma as the decimal point, "";
--- Delete international standards foreword.
This part of the National Chemicals Management Standardization Technical Committee dangerous (SAC/TC251) and focal points.
Drafting this Part. Guangdong CIQ, in the construction of Changzhou coating Chemical Research Institute, Marine Chemicals Research Institute, the Chemical
Standardization Institute, Hubei Exit Inspection and Quarantine, China National Institute of Standardization.
The main drafters of this section. Liang Meiqiong, Linhong Xiong, Mei Jian, Chen Wenjie, Chen Qiang, Chen Gufeng, Peng-speed standard, Shen Jiang Su, Mao Leilei, Wang Fan,
Liqing Xiang.
This section first release.
GB/T 21782.3-2008/ISO 8130-3.1992
Powder Coatings
Part 3. Determination of the density of liquid displacement pyknometer method
1 Scope
This section GB/T 21782 specifies the determination of the density of the powder coating of liquid displacement pyknometer method. This method is based on the quality of the sample
Determination of the amount and volume.
This method specifies the equipment is relatively inexpensive, but the liquid displacement pyknometer method may give incorrect results, especially with the powder
Disposable fluid expands when the liquid is not replaced or replaced entirely when the powder particles in the air. Liquid displacement method using a slower than
"Determination of density (Arbitration Act) compare the proportion of gas meter method" GB/T 21782.2-2008 less accurate, but also proved to be in proportion with the gas comparison
Measuring and come to the same result when it is using this method.
2 Normative references
The following documents contain provisions which, through reference GB/T 21782 in this section constitute provisions of this section. For dated reference documents
Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section
Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this
section.
GB/T 3186-2006 Paints, varnishes and raw materials for paints and varnishes - Sampling (ISO 15528.2000, IDT)
GB/T 21782.2-2008 powder coatings - Part 2. Determination of density (Arbitration Act) (ISO 8130-2 compare the proportion of instrument gas law.
1992, IDT)
1993 General methods of test for pigments and extenders - Part 10.. ISO 787-10 Density Pycnometer method
ISO 3696. 1987 for analytical laboratory use specifications and test methods
Principle 3
By liquid displacement pyknometer method (pycnometer comply with ISO 787-10.1993 regulations) measuring the density of the powder coating, the liquid used should
Completely wetted with the sample and does not swell or dissolve the sample.
4 Materials
4.1 Water
Freshly distilled and cooled, and its technical indicators should at least comply with ISO 3696. 1987 provided three water.
4.2 displacement liquid
A mixture of aliphatic or aliphatic hydrocarbon free of aromatic compounds, boiling range 80 ℃ ~ 140 ℃. We found positive in many instances
Heptane for the determination of the density of the thermosetting powder coating, however, if the n-heptane with which a sample or a component can play a role, it should be used
He Suitable liquid.
4.3 acetone
AR.
5 Instruments
5.1 pycnometer
It shall comply with ISO 787-10.1993 requirements.
GB/T 21782.3-2008/ISO 8130-3.1992
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