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GB/T 13747.26-2022: Methods for chemical analysis of zirconium and zirconium alloys - Part 26: Determination of alloying and impurity elements content - Inductively coupled plasma atomic emission spectrometry
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Methods for chemical analysis of zirconium and zirconium alloys - Part 26: Determination of alloying and impurity elements content - Inductively coupled plasma atomic emission spectrometry
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GB/T 13747.26-2022
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Basic data | Standard ID | GB/T 13747.26-2022 (GB/T13747.26-2022) | | Description (Translated English) | Methods for chemical analysis of zirconium and zirconium alloys - Part 26: Determination of alloying and impurity elements content - Inductively coupled plasma atomic emission spectrometry | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | H14 | | Classification of International Standard | 77.120.99 | | Word Count Estimation | 22,210 | | Date of Issue | 2022-12-30 | | Date of Implementation | 2023-04-01 | | Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration | GB/T 13747.26-2022: Methods for chemical analysis of zirconium and zirconium alloys - Part 26: Determination of alloying and impurity elements content - Inductively coupled plasma atomic emission spectrometry
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ICS 77.120.99
CCSH14
National Standards of People's Republic of China
Zirconium and zirconium alloy chemical analysis method
Part 26.Determination of alloys and impurity elements
Inductively Coupled Plasma-Atomic Emission Spectrometry
Posted on 2022-12-30
2023-04-01 Implementation
State Administration for Market Regulation
Released by the National Standardization Management Committee
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules for Standardization Documents"
drafting.
This document is part 26 of GB/T 13747 "Methods for Chemical Analysis of Zirconium and Zirconium Alloys". GB/T 13747 has issued the following
part.
--- Part 1.Determination of tin content potassium iodate titration method and phenylfluorone-polyethylene glycol octylphenyl ether spectrophotometric method;
--- Part 2.Determination of iron content 1,10-phenanthrene spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 3.Determination of the amount of nickel - diacetyl oxime spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 4.Determination of the amount of chromium diphenylcarbazide spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 5.Determination of aluminum content - spectrophotometric method of chromazurin S-tetradecylpyridinium chloride;
--- Part 6.Determination of copper content 2,9-dimethyl-1,10-phenanthroline spectrophotometric method;
--- Part 7.Determination of manganese content potassium periodate spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 8.Determination of cobalt content - Nitroso R salt spectrophotometric method;
--- Part 9.Determination of magnesium content by flame atomic absorption spectrometry and inductively coupled plasma atomic emission spectrometry;
--- Part 10.Determination of tungsten content thiocyanate spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 11.Determination of the amount of molybdenum thiocyanate spectrophotometry;
--- Part 12.Determination of silicon content Molybdenum blue spectrophotometry;
--- Part 13.Polarographic method for determination of lead content;
--- Part 14.Determination of the amount of uranium polarographic method;
--- Part 15.Determination of boron content Curcumin spectrophotometry;
--- Part 16.Determination of chlorine content - silver chloride turbidity method and ion selective electrode method;
--- Part 17.Polarographic method for determination of cadmium content;
--- Part 18.Determination of vanadium content Benzoylphenyl hydroxylamine spectrophotometry and inductively coupled plasma atomic emission light
spectral method;
--- Part 19.Determination of the amount of titanium diantipyrine methane spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 20.Determination of hafnium content Inductively coupled plasma atomic emission spectrometry;
--- Part 21.Determination of hydrogen content Inert gas fusion infrared absorption method/thermal conductivity method;
--- Part 22.Determination of oxygen and nitrogen content Inert gas fusion infrared absorption/thermal conductivity method;
---Distillation separation-Nessler reagent spectrophotometric determination of nitrogen content;
--- Part 24.Determination of carbon content High-frequency combustion infrared absorption method;
--- Part 25.Determination of the amount of niobium 5-Br-PADAP spectrophotometry and inductively coupled plasma atomic emission spectrometry;
--- Part 26.Determination of alloys and impurity elements Inductively coupled plasma atomic emission spectrometry;
--- Part 27.Determination of trace impurity elements Inductively coupled plasma mass spectrometry.
Please note that some contents of this document may refer to patents. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by China Nonferrous Metals Industry Association.
This document is under the jurisdiction of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243).
This document was drafted by. Baoti Group Co., Ltd., Baoji Titanium Industry Co., Ltd., State Nuclear Zirconium and Hafnium Physical and Chemical Testing Co., Ltd., National Standard
(Beijing) Inspection and Certification Co., Ltd., Xi'an Hantang Analysis and Testing Co., Ltd., Western New Zirconium Nuclear Material Technology Co., Ltd., Guangdong Academy of Sciences
Industrial Analysis and Testing Center, Guohe General (Qingdao) Testing and Evaluation Co., Ltd., Guangxi Zhuang Autonomous Region Analysis and Testing Research Center, Baoji Titanium Valley
New Material Testing Technology Center Co., Ltd., Xinjiang Xiangrun New Material Technology Co., Ltd.
The main drafters of this document. Liu Ting, Li Jian, Li Zhenqian, Kang Qiong, Li Rui, Wang Ying, Zhao Xudong, Zhang Jiawei, Luo Feng, Liu Xuan, Mo Shumin,
Zhang Danli, Zhang Sheng, Wang Xingjun, Xie Tao, Du Taohua, Liu Leilei, Wang Changhua, Yang Zaijiang, Wei Lili.
Introduction
Zirconium and zirconium alloys are widely used due to their excellent corrosion resistance, moderate mechanical properties, and low thermal neutron absorption cross section.
In nuclear power, aerospace, chemical industry, light industry, electric power, pharmaceutical, textile, machinery and petrochemical and other fields.
GB/T 13747 aims to establish chemical analysis methods for zirconium and zirconium alloy products, and consists of 27 parts.
--- Part 1.Determination of tin content Potassium iodate titration and phenyl fluorescent copper-polyethylene glycol octylphenyl ether spectrophotometry. Purpose
It is to establish the determination method of tin content.
--- Part 2.Determination of the amount of iron 1,10-phenanthrene spectrophotometry and inductively coupled plasma atomic emission spectrometry. head
The most important thing is to establish a method for the determination of iron content.
--- Part 3.Determination of the amount of nickel dimethylglyoxime spectrophotometry and inductively coupled plasma atomic emission spectrometry. The purpose is
To establish a method for the determination of nickel content.
--- Part 4.Determination of the amount of chromium diphenylcarbazide spectrophotometry and inductively coupled plasma atomic emission spectrometry. Purpose
It is to establish the determination method of chromium content.
--- Part 5.Determination of the amount of aluminum Chromazurin S-tetradecylpyridinium chloride spectrophotometric method. The purpose is to establish the measurement of aluminum content
Determine the method.
--- Part 6.Determination of the amount of copper 2,9-dimethyl-1,10-phenanthroline spectrophotometric method. The purpose is to establish the determination of copper content
method.
--- Part 7.Determination of the amount of manganese Potassium periodate spectrophotometry and inductively coupled plasma atomic emission spectrometry. The purpose is
To establish a method for the determination of manganese content.
--- Part 8.Determination of the amount of cobalt Nitroso R salt spectrophotometric method. The purpose is to establish the determination method of cobalt content.
--- Part 9.Determination of magnesium content flame atomic absorption spectrometry and inductively coupled plasma atomic emission spectrometry. Purpose
It is to establish the determination method of magnesium content.
--- Part 10.Determination of tungsten content Thiocyanate spectrophotometry and inductively coupled plasma atomic emission spectrometry. Purpose
It is to establish the determination method of tungsten content.
--- Part 11.Determination of the amount of molybdenum thiocyanate spectrophotometric method. The purpose is to establish the determination method of molybdenum content.
--- Part 12.Determination of the amount of silicon molybdenum blue spectrophotometry. The purpose is to establish the determination method of silicon content.
--- Part 13.Determination of the amount of lead Polarographic method. The purpose is to establish the determination method of lead content.
--- Part 14.Determination of uranium Polarography. The purpose is to establish a method for the determination of uranium content.
--- Part 15.Determination of boron content Curcumin spectrophotometry. The purpose is to establish the determination method of boron content.
--- Part 16.Determination of chlorine content silver chloride turbidity method and ion selective electrode method. The purpose is to establish the determination of chlorine content
method.
--- Part 17.Determination of the amount of cadmium polarographic method. The purpose is to establish the determination method of cadmium content.
--- Part 18.Determination of vanadium content Benzoyl phenyl hydroxylamine spectrophotometry and inductively coupled plasma atomic emission spectrometry
Law. The purpose is to establish the determination method of vanadium content.
--- Part 19.Determination of the amount of titanium diantipyrine methane spectrophotometry and inductively coupled plasma atomic emission spectrometry.
The purpose is to establish the determination method of titanium content.
--- Part 20.Determination of the amount of hafnium Inductively coupled plasma atomic emission spectrometry. The purpose is to establish the determination of hafnium content
method.
--- Part 21.Determination of hydrogen Inert gas fusion infrared absorption method/thermal conductivity method. The purpose is to establish the determination method of hydrogen content.
--- Part 22.Determination of oxygen and nitrogen Inert gas fusion infrared absorption method/thermal conductivity method. The purpose is to establish the oxygen content and nitrogen content
Quantitative method.
---Distillation separation-Nessler reagent spectrophotometric determination of nitrogen content. The purpose is to establish the determination method of nitrogen content.
--- Part 24.Determination of carbon content High-frequency combustion infrared absorption method. The purpose is to establish a method for the determination of carbon content.
--- Part 25.Determination of the amount of niobium 5-Br-PADAP spectrophotometry and inductively coupled plasma atomic emission spectrometry. head
It is important to establish a method for the determination of niobium content.
--- Part 26.Determination of alloys and impurity elements Inductively coupled plasma atomic emission spectrometry. The purpose is to establish the alloy
And the determination method of impurity element content.
--- Part 27.Determination of trace impurity elements Inductively coupled plasma mass spectrometry. The purpose is to establish trace impurity elements containing
Quantitative method.
Inductively coupled plasma atomic emission spectrometry is characterized by its high sensitivity, good precision, wide linear range, and simultaneous analysis of multiple elements.
With the advantages of high analysis and detection efficiency, it has been widely used in the determination of element content in zirconium and zirconium alloys.
Zirconium and zirconium alloy chemical analysis method
Part 26.Determination of alloys and impurity elements
Inductively Coupled Plasma-Atomic Emission Spectrometry
Caution --- Personnel using this document need to have practical experience in formal laboratory work. This document does not address all possible security issues
question. It is the user's responsibility to take appropriate safety and health measures and ensure compliance with the conditions stipulated in the relevant national laws and regulations.
1 Scope
This document describes the determination of aluminum, beryllium, cobalt, copper, chromium, calcium, iron, germanium,
Method for hafnium, potassium, lithium, manganese, magnesium, molybdenum, niobium, nickel, sodium, lead, silicon, tin, tantalum, titanium, vanadium, tungsten, zinc content.
This document is applicable to the determination of the contents of alloys and impurity elements in zirconium sponge, zirconium and zirconium alloys. The determination range of each element is shown in Table 1.
Table 1 Determination range of each element
element
Measuring range
element
Measuring range
Al 0.0020~0.10 Mo 0.0020~0.10
Be 0.0010~0.020 Nb 0.0050~35.00
Co 0.00050~0.10 Ni 0.0010~0.15
Cu 0.0020~0.10 Na 0.0010~0.10
Cr 0.0010~0.50 Pb 0.0020~0.10
Ca 0.0020~0.10 Si 0.0020~0.10
Fe 0.0050~0.50 Sn 0.0050~4.00
Ge 0.0050~0.10 Ta 0.0020~0.10
Hf 0.0020~5.00 Ti 0.0020~0.10
K 0.0020~0.020 V 0.0020~0.10
Li 0.00010~0.0010 W 0.0020~0.10
Mn 0.0010~0.10 Zn 0.0010~0.10
Mg 0.0010~0.10 - -
2 Normative references
The contents of the following documents constitute the essential provisions of this document through normative references in the text. Among them, dated references
For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to
this document.
GB/T 6682 Analytical laboratory water specifications and test methods
GB/T 8170 Numerical rounding off rules and expression and determination of limit values
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