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GB 1886.66-2015: National Food Safety Standard -- Food Additives -- Monascus yellow
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National Food Safety Standard -- Food Additives -- Monascus yellow
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GB 1886.66-2015
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Basic data | Standard ID | GB 1886.66-2015 (GB1886.66-2015) | | Description (Translated English) | National Food Safety Standard -- Food Additives -- Monascus yellow | | Sector / Industry | National Standard | | Classification of Chinese Standard | X40 | | Classification of International Standard | 67.220.20 | | Word Count Estimation | 5,575 | | Date of Issue | 2015-11-13 | | Date of Implementation | 2016-05-13 | | Regulation (derived from) | National Health and Family Planning Commission Announcement No | | Issuing agency(ies) | National Health and Family Planning Commission of the People's Republic of China | | Summary | This standard applies to red yeast rice as raw material, alkali elution, separation system was red monascus red (or directly to red yeast rice as raw material), sulfide into, drying food additives Add red yeast yellow pigment. | GB 1886.66-2015: National Food Safety Standard -- Food Additives -- Monascus yellow---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
(National food safety standards for food additives Monascus Yellow Pigment)
National Standards of People's Republic of China
National Food Safety Standard
Food additive Monascus Yellow Pigment
Issued on. 2015-11-13
2016-05-13 implementation
People's Republic of China
National Health and Family Planning Commission released
National Food Safety Standard
Food additive Monascus Yellow Pigment
1 Scope
This standard applies to red yeast rice as raw material, alkaline elution, separation prepared Monascus red (or red to red yeast rice as raw material), the sulfide
Sulfonated, made of dried food additives Monascus yellow pigment.
2 Technical Requirements
2.1 Sensory requirements
Sensory requirements shall comply with the requirements of Table 1.
Table 1 Sensory requirements
Project requires test methods
Orange-red to brown color
State powder
Take the right amount of sample is placed in a clean, dry white porcelain dish, in natural light
Under observe its color and status
2.2 Physical indicators
Physical and chemical indicators should be consistent with the provisions of Table 2.
Table 2. Physical and chemical indicators
Item Index Test Method
The color value of E1 m (476 ± 10) nm ≥ 100 Appendix A A.3
Loss on drying, w /% ≤ 6.0 GB 5009.3 direct drying
Residue on ignition, w /% ≤ 10.0 GB 5009.4
Lead (Pb)/(mg/kg) ≤ 2.0 GB 5009.75
Total arsenic (As)/(mg/kg) ≤ 3.0 GB 5009.11
Citrinin/(mg/kg) ≤ 1.0 GB/T 5009.222
Note. the commercialization of red yeast yellow product shall comply with the standard yellow red yeast rice as raw materials, food and other materials can be added dextrin made its color value in line with the identity value.
Appendix A
Testing method
A.1 General Provisions
Unless otherwise specified in this standard, the use of analytical reagent purity should be more than the standard titration solution, standard solution for measuring impurities,
Preparations and products, should be GB/T 601, the provisions of the preparation of GB/T 602 and GB/T 603, the test water should be consistent with GB/T 6682 in three
Water provisions. Solution was used in the tests did not indicate what is formulated with solvent, it refers to an aqueous solution.
A.2 Identification Test
A.2.1 solubility
soluble in water.
A.2.2 maximum absorption wavelength
Weigh 0.01g sample was dissolved in 100mL of water, with a spectrophotometer, this solution at a wavelength of 476nm ± 10nm scope
The maximum absorption peak.
A.3 color value E1 m (476 ± 10) nm is measured
A.3.1 Instruments and Equipment
Spectrophotometer.
A.3.2 Analysis step
Weigh a sample of about 0.05g ~ 0.1g, accurate to 0.0002g, dissolved in water, dilute to 1000mL, shake. Take this sample was placed
Measuring the absorbance 1cm cuvette, with water as the control, using a spectrophotometer at a wavelength of 476nm ± 10nm of the maximum absorption wavelength
Degree (absorbance should be controlled between 0.3 and 0.7, otherwise the sample concentration should be adjusted and re-measuring the absorbance).
A.3.3 Calculation Results
Color value in the test sample concentration of 1%, with a 1cm cuvette at wavelength of 476nm ± 10nm measured absorbance E1 m (476 ±
10) nm dollars, according to equation (A.1) Calculated.
E1 m (476 ± 10) nm =
c × 100
(A.1)
Where.
A --- measured absorbance of the sample solution;
c --- concentration of the sample solution to be tested, in grams per milliliter (g/mL);
100 --- concentration conversion factor.
The results parallel arithmetic mean of the measurement results shall prevail. Twice under the same condition of independent determination results obtained absolute difference
The ratio of the arithmetic mean value is not more than 2%.
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