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GB 10351-2008: Food additive -- Oil of eucalyptus, containing 80% cineole
Status: Obsolete GB 10351: Evolution and historical versions
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Food additive -- Oil of eucalyptus, containing 80% cineole
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GB 10351-2008
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| GB 10351-1989 | English | 319 |
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Food additive--Oil of eucalyptus, 80% cineole content
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GB 10351-1989
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PDF similar to GB 10351-2008
Basic data | Standard ID | GB 10351-2008 (GB10351-2008) | | Description (Translated English) | Food additive -- Oil of eucalyptus, containing 80% cineole | | Sector / Industry | National Standard | | Classification of Chinese Standard | X44 | | Classification of International Standard | 71.100.60 | | Word Count Estimation | 8,828 | | Date of Issue | 2008-12-03 | | Date of Implementation | 2009-06-01 | | Older Standard (superseded by this standard) | GB 10351-1989 | | Quoted Standard | GB 190; GB/T 5009.74; GB/T 5009.76; GB/T 11539-2008; GB/T 11540; GB/T 144574.2; GB/T 14454.4; GB/T 14454.5; GB/T 14454.7; GB/T 14455.3 | | Adopted Standard | FCC ��-1996, NEQ | | Regulation (derived from) | Announcement of Newly Approved National Standards No. 19 of 2008 (No. 132 overall) | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China | | Summary | This Chinese standard specifies the food additive cineole content of 80% eucalyptus oil requirements, test methods, inspection rules, marking, packaging, transportation, storage and shelf life. This standard applies to right to Eucalyptus (Eucalyptus globulus Labill.) Oil or other products containing certain Eucalyptus essential oil of camphor tree species as raw material, obtained by distillation processed food additives vasopressin levels by 80% eucalyptus oil analysis and evaluation of the quality. | GB 10351-2008: Food additive -- Oil of eucalyptus, containing 80% cineole---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Food additive.Oil of eucalyptus, containing 80% cineole
ICS 71.100.60
X44
National Standards of People's Republic of China
Replacing GB 10351-1989
Food Additives cineole content of 80% eucalyptus oil
Posted 2008-12-03
2009-06-01 implementation
Administration of Quality Supervision, Inspection and Quarantine of People's Republic of China
Standardization Administration of China released
Foreword
Chapter 4 of this standard are mandatory, the rest are recommended.
This standard with the US Food Chemicals Codex FCC (Ⅳ).1996 "eucalyptus" in non-equivalent.
This standard replaces GB 10351-1989 "Food Additives cineole content of 80% eucalyptus oil."
This standard compared with GB 10351-1989, the main modifications are as follows.
--- Remove color like the color of the label;
--- Cineole levels ranging from 85.0% to 80.0% ~ ≥80.0%.
Appendix A of this standard is an informative annex.
The standard proposed by China National Light Industry Council.
This standard by the National Standardization Technical Committee on Food Additives.
The standard by the Shanghai Institute of spices, spice Sichuan Yibin Huarong Co., Ltd. Kunming Ai harmonic spice and Beijing Beida positive
Yuan Science and Technology Co., Ltd. is responsible for drafting.
The main drafters of this standard. Zhangxin Jun, Xu Yi, Jinqi Zhang, Wang Changrong, Xu, Lin Chengjie, Bob.
This standard replaces the standards previously issued as follows.
--- GB 10351-1989.
Food Additives cineole content of 80% eucalyptus oil
1 Scope
This standard specifies the food additive cineole content of 80% eucalyptus oil requirements, test methods, inspection rules, marking, packaging, transportation
Transport, storage and shelf life.
As raw materials, processed by distillation to obtain food additive cineole content of 80% by mass of eucalyptus oil analysis and evaluation.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
GB 190 packaging and marking of dangerous goods
GB/T 5009.74 limit test of heavy metals in food additives
Determination of GB/T 5009.76 arsenic in food additives
GB/T 11539-2008 spices Packed Column Gas Chromatography common method (ISO 7359. 1985, IDT)
GB/T 11540 Determination of relative density of spices (GB/T 11540-2008, ISO 279.1998, MOD)
GB/T 14454.2 spice aroma evaluation method
GB/T 14454.4 spices refractive index measurement (GB/T 14454.4-2008, ISO 280.1998, MOD)
GB/T 14454.5 Determination of spices optical rotation (GB/T 14454.5-2008, ISO 592.1998, MOD)
GB/T 14454.7 Determination of spices freezing point (GB/T 14454.7-2008, ISO 1041. 1973, MOD)
GB/T 14455.3 spices dissolved in ethanol (mixed) to assess the degree (GB/T 14455.3-2008, ISO 875.1999, MOD)
3 Terms and Definitions
The following terms and definitions apply to this standard.
3.1
Take essential oils after distillation process obtained cineole minimum content of 80% eucalyptus oil (hereinafter referred to as 80% eucalyptus oil).
4 Requirements
Technical requirements 80% eucalyptus oil should be in accordance with Table 1.
Table 1
project
Claim
Eucalyptus oil as raw material to other oil as raw material
Appearance colorless to pale yellow liquid
Characteristic aroma aroma of 1,8-cineole, camphor-like flavor with a slightly spicy and cool taste
The relative density (20 ℃/20 ℃) 0.909 ~ 0.919 0.904 ~ 0.925
Table 1 (continued)
project
Claim
Eucalyptus oil as raw material to other oil as raw material
Refractive index (20 ℃) 1.4580 ~ 1.4650 1.4580 ~ 1.4700
Optical rotation (20 ℃) 0 ° ~ + 5 ° -10 ° ~ + 10 °
Miscibility (20 ℃) 1 volume of the sample soluble in 5 volumes of 70% (volume fraction) ethanol as a clear solution
Cineole content /% ≥80.0
Safrole content (GC) /% Not detected < 0.002
Heavy metal content (Pb) ≤10mg/kg
Arsenic content ≤3mg/kg
5 Test methods
5.1 Verification of Appearance
The sample is placed in color than the inner tube, were visually observed.
5.2 Evaluation aroma
According to the provisions of GB/T 14454.2 of.
5.3 Determination of relative density
According to GB/T 11540 regulations.
5.4 Determination of refractive index
According to GB/T 14454.4 of the provisions.
5.5 Determination of the optical rotation
According to GB/T 14454.5 of the provisions.
5.6 Assessment of miscibility
According to the provisions of GB/T 14455.3 of.
Determination of 5.7 cineole content
According to GB/T 14454.7 of the provisions.
5.8 Determination of safrole content
5.8.1 Instruments
5.8.1.1 chromatograph, recorder and microprocessor
According to GB/T 11539-2008 provisions in Chapter 5.
5.8.1.2 Column
Packed column. length 2m ~ 3m, inner diameter of 3mm.
Stationary phase. SE30,5% applied to the ChromosorbWAWDMCS80 mesh to 100 mesh.
5.8.1.3 Detector
Hydrogen flame ionization detector.
5.8.2 Reagents and standard solutions
5.8.2.1 Reagents
Benzene. analytical, chromatographic purity was determined under the test conditions of at least 99%.
Safrole. chromatographic purity was determined under the test conditions of at least 99%.
5.8.2.2 safrole content of 0.002% formulated standard solution
Accurately weigh 1.0000g ± 0.0002g of safrole in 500mL flask, diluted with benzene to the mark. Imbibe the
Solution 1.0mL in 100mL flask, diluted with benzene to the mark, shake spare.
5.8.3 Operating Conditions
5.8.3.1 Temperature
Chromatography oven. 135 ℃.
Inlet.200 ℃.
Detector.200 ℃.
5.8.3.2 carrier gas flow rate
Nitrogen. 15mL/min.
Determination 5.8.3.3 column efficiency
Chemically inert test. according to GB/T 11539-2008 test method specified in 8.1, shall comply with the requirements.
Column efficiency. measured according to GB/T 11539-2008 8.2 specification method should meet the requirements.
5.8.3.4 Determination
Area normalization method. Determination of safrole content according to GB/T 11539-2008 10.4 specified method. The standard solution (5.8.2.2)
And samples were measured injection volume must be the same. Compare two chromatograms on the size of the safrole peak area.
5.8.4 repeatability and results are shown
According to GB/T 11539-2008 provisions in 11.4, shall comply with the requirements.
80% of eucalyptus oil and safrole typical gas chromatogram of the standard solution (area normalization method) See Appendix A.
5.9 Determination of heavy metal content (P Chou basis)
According to GB/T 5009.74 of the provisions.
Determination of Arsenic 5.10
According to GB/T 5009.76 of the provisions.
6 Inspection rules
6.1 to 80% by eucalyptus plant quality inspection department inspection, the manufacturer shall ensure that products conform to the requirements of this standard, each
Batch manufactured products should be accompanied by quality certificate. Appearance, aroma, relative density, refractive index, optical rotation, miscibility, eucalyptol, safrole
Content factory inspection items, and arsenic content, heavy metal content (Pb) for the type of test items, test once every six months.
6.2 Acceptance shall be entitled in accordance with the provisions of this standard of product quality inspection received meets the requirements of this standard, for each batch
Once acceptance, acceptance of different batches respectively.
6.3 Sampling Method. each batch of packaging units 1 to 2, total pumping; 3 ~ 100 extract 2; 100 more than the increase taking further part
3%. Sampler with a sample drawn from a uniform 50mL ~ 100mL per package unit, all the extracted sample is placed within MIXER
Mix well, respectively, into two clean, dry, inert sealed containers, protected from light. Container attach a label stating. manufacturer name, product
Name, date of production, batch number, number and date of sampling, with a bottle for examination, another bottle retained for future reference.
6.4 As a result there is an indicator of acceptance does not meet the requirements of this standard, it can be doubled again in conjunction with the production plant to extract a sample reinspection. As retest knot
If there are indicators of failure, then the product can not be accepted.
6.5 When both supply and demand on product quality objection occurs, resolve by mutual agreement or arbitration by the statutory inspection bodies.
7 signs, packaging, transportation, storage and shelf life
7.1 marks
Packing of products should be marked. "food additive" word, product name, manufacturer name and address, trademark, batch number, net weight, date of manufacture
And shelf life, license number, and the standard number GB 190 flammable materials specified in flags. For special customer requirements, and other custom manufacturers
protocol.
7.2 Packaging
80% eucalyptus oil should be installed in clean and free of miscellaneous taste of galvanized iron or food-grade plastic bucket, or according to customer requirement.
7.3 Transport
During transport should be light light disposal to prevent the sun and rain, can not be mixed with toxic and hazardous substances, mixed operation, and shall conform to the relevant departments
Provisions.
7.4 Storage
Products should be stored in a cool, dry, ventilated warehouse, avoid mixed air pollution, away from fire.
7.5 Shelf Life
Subject to the conditions of storage, packaging integrity, without the unsealing, the product shelf life of one year. Late re-examine whether the operator
Combined requirements of this standard, qualified can still be used.
Appendix A
(Informative)
80% of eucalyptus oil and safrole typical gas chromatogram of the standard solution
(Area normalization method)
80% of eucalyptus oil and safrole typical GC standard solution is shown in Figure A. 1.
Figure A. 1
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