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GA/T 1932-2021 English PDF

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GA/T 1932-2021: Forensic sciences - Examination methods for BZP, mCPP and TFMPP in suspected drugs - GC and GC-MS
Status: Valid
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GA/T 1932-2021English349 Add to Cart 3 days [Need to translate] Forensic sciences - Examination methods for BZP, mCPP and TFMPP in suspected drugs - GC and GC-MS Valid GA/T 1932-2021

PDF similar to GA/T 1932-2021


Standard similar to GA/T 1932-2021

GA/T 1788.2   GA/T 1711   GA/T 424   GA/T 1923   GA/T 1924   GA/T 1922   

Basic data

Standard ID GA/T 1932-2021 (GA/T1932-2021)
Description (Translated English) Forensic sciences - Examination methods for BZP, mCPP and TFMPP in suspected drugs - GC and GC-MS
Sector / Industry Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard A92
Word Count Estimation 15,174
Issuing agency(ies) Ministry of Public Security

GA/T 1932-2021: Forensic sciences - Examination methods for BZP, mCPP and TFMPP in suspected drugs - GC and GC-MS


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences - Examination methods for BZP, mCPP and TFMPP in suspected drugs - GC and GC-MS ICS 13.310 CCSA92 People's Republic of China Public Safety Industry Standards Forensic Science Benzylpiperazine, 1-(3-Chloro Phenyl)piperazine and 1-(3-trifluoromethylphenyl)piperazine test Gas chromatography and gas chromatography-mass spectrometry Published on 2021-10-14 2022-05-01 Implementation Published by the Ministry of Public Security of the People's Republic of China

foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents" drafted. Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents. This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1). focal point. This document is drafted by. Dalian Municipal Public Security Bureau Criminal Science and Technology Research Institute, Ministry of Public Security Material Evidence Identification Center, Ministry of Public Security Anti-drug Intelligence Technology Center, Liaoning Police College. The main drafters of this document. Wang Zhengqiao, Wang Bin, Zhang Junjie, Liu Yuanyuan, Xie Wenhui, Luo Feng, Qin Chen, Zhang Ling, Zhou Xing, Zhu Haiyan, Zheng Hui, Hua Zhendong, Li Guoping, Xu Xiuming. Forensic Science Benzylpiperazine, 1-(3-Chloro Phenyl)piperazine and 1-(3-trifluoromethylphenyl)piperazine test Gas chromatography and gas chromatography-mass spectrometry

1 Scope

This document regulates benzylpiperazine (BZP), 1-(3-chlorophenyl)piperazine (mCPP) and 1- Gas chromatography-mass spectrometry (GC-MS) qualitative test method and gas chromatography (GC) quantitative test of (3-trifluoromethylphenyl)piperazine (TFMPP) method. This document is applicable to the qualitative and quantitative analysis of BZP, mCPP, and TFMPP in solid samples of suspected narcotics in the field of forensic science.

2 Normative references

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to this document. GB/T 27418 Evaluation and representation of measurement uncertainty GA/T 122 Toxic Analysis Terminology

3 Terms and Definitions

Terms and definitions defined in GA/T 122 apply to this document.

4 Principles

Extraction of BZP, mCPP and TFMPP in the suspected drug solid samples (for compound information, see Appendix A). gas color Spectral-mass spectrometry detection, with retention time, characteristic ion fragments and ion abundance ratio as qualitative judgment basis; gas chromatography-hydrogen flame ionization The chromatographic peak area was used as the quantitative basis, and the external standard single-point method or the external standard standard curve method was used for quantitative analysis.

5 Reagents and Materials

5.1 Reagents All reagents used are of analytical grade, including. a) methanol; b) Standard solution. 1) Standard material stock solution. BZP, mCPP and TFMPP standard material stock solution; 2) Standard working solutions are divided into the following four categories according to experimental requirements. ---Qualitative standard working solution. Pipette appropriate amount of BZP, mCPP and TFMPP standard stock solution, dilute with methanol 0.1mg/mL standard working solution of BZP, mCPP and TFMPP, refrigerated at 0℃~4℃

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