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Forensic sciences - Examination methods for 8 fentanyl derivatives in suspected drugs - GC and GC-MS
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Basic data Standard ID | GA/T 1922-2021 (GA/T1922-2021) | Description (Translated English) | Forensic sciences - Examination methods for 8 fentanyl derivatives in suspected drugs - GC and GC-MS | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | Classification of Chinese Standard | A92 | Word Count Estimation | 19,181 | Issuing agency(ies) | Ministry of Public Security |
GA/T 1922-2021: Forensic sciences - Examination methods for 8 fentanyl derivatives in suspected drugs - GC and GC-MS ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences - Examination methods for 8 fentanyl derivatives in suspected drugs - GC and GC-MS
ICS 13.310
CCSA92
People's Republic of China Public Safety Industry Standards
Forensic science suspects 8 fentanyl-like substances in drugs
Check gas chromatography and gas chromatography-mass spectrometry
Published on 2021-10-14
2022-05-01 Implementation
Published by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
drafted.
Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1).
focal point.
This document is drafted by. Criminal Technology Center of Guangdong Provincial Public Security Department, Physical Evidence Appraisal Center of Ministry of Public Security, Gansu Provincial Public Security Department, Ministry of Public Security Anti-drug Information
report to the Technology Center.
The main drafters of this document. Pei Maoqing, Zhang Liang, Hu Haolang, Wang Bin, Shi Wenbing, Xu Ruolun, Zheng Hui, Teng Hanfei, Feng Chao.
Forensic science suspects 8 fentanyl-like substances in drugs
Check gas chromatography and gas chromatography-mass spectrometry
1 Scope
This document regulates fentanyl, acetylfentanyl, acryloylfentanyl, isobutyrylfentanyl in suspected drug solid samples in the field of forensic science
Gas chromatography-mass spectrometry (GC-MS) qualitative test method and gas chromatography
Gas chromatography (GC) quantitative test method.
This document applies to fentanyl, acetylfentanyl, acryloyl fentanyl, isobutyryl fentanyl in suspected drug solid samples in the field of forensic science
Qualitative and quantitative analysis of fentanyl, valeryl fentanyl, 4-fluorobutyryl fentanyl, furan fentanyl, and fentanyl. Other in vitro samples and fentanyl
Nisin derivatives can be used by reference.
2 Normative references
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations
documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to
this document.
GB/T 27418 Evaluation and representation of measurement uncertainty
GA/T 122 Toxic Analysis Terminology
3 Terms and Definitions
Terms and definitions defined in GA/T 122 apply to this document.
4 Principles
Eight fentanyl-like substances (see Appendix A for the basic information of the compounds) in the solid samples of suspected drugs were extracted. gas color
Spectral-mass spectrometry detection, with retention time, mass spectrometry characteristic ions and ion abundance ratio as qualitative judgment basis; gas chromatography detection, chromatographic detection
The peak area was used as the quantitative basis, and the quantitative analysis was carried out by the external standard single-point method, the external standard standard curve method, the internal standard single-point method and the internal standard standard curve method.
5 Reagents and Materials
5.1 Reagents
Unless otherwise stated, the reagents used in the analysis are of analytical grade, including.
a) methanol;
b) Internal standard. propyl spasmolysis (SKF525A);
c) Standard solution.
1) Standard material stock solutions. fentanyl, acetylfentanyl, acryloylfentanyl, isobutyrylfentanyl, valerylfentanyl, 4-fluorobutane
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