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Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - LC and LC-MS
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GA/T 1929-2021
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Basic data Standard ID | GA/T 1929-2021 (GA/T1929-2021) | Description (Translated English) | Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - LC and LC-MS | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | Classification of Chinese Standard | A92 | Word Count Estimation | 19,120 | Issuing agency(ies) | Ministry of Public Security |
GA/T 1929-2021: Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - LC and LC-MS ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - LC and LC-MS
ICS 13.310
CCSA92
People's Republic of China Public Safety Industry Standards
Forensic Science Suspected Drugs in AB-CHMINACA,
AB-FUBINACA and AB-PINACA inspection
Liquid chromatography and liquid chromatography-mass spectrometry
Published on 2021-10-14
2022-05-01 Implementation
Published by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
drafted.
Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1).
focal point.
This document is drafted by. Ministry of Public Security Physical Evidence Appraisal Center, Fujian Provincial Public Security Department Criminal Technology Corps, Jiangsu Provincial Public Security Department Physical Evidence Appraisal Center,
Anti-drug Information Technology Center of the Ministry of Public Security.
The main drafters of this document. Chang Ying, Zhao Yang, Yang Hongxian, Zheng Hui, Zhang Chunshui, Li Hangqi, Qian Kaiwen, Qian Zhenhua, Li Peng, Zhao Yanbiao,
Zheng Xiaoyu, Wen Wu, Zhai Wanfeng, Liu Kelin, Gu Yuebao, Wang Xuehu, Qiao Hongwei, Zhang Qianshang, Lin Jia, Gao Lisheng.
Forensic Science Suspected Drugs in AB-CHMINACA,
AB-FUBINACA and AB-PINACA inspection
Liquid chromatography and liquid chromatography-mass spectrometry
1 Scope
This document specifies that AB-CHMINACA[N-(1-carbamoyl-2-methylpropyl)-1-(cyclohexyl)
Hexylmethyl)indazole-3-carboxamide], AB-FUBINACA[N-(1-carbamoyl-2-methylpropyl)-1-(4-fluorobenzyl)indazole-3-carboxyl
Amine], AB-PINACA [N-(1-carbamoyl-2-methylpropyl)-1-pentylindazole-3-carboxamide] liquid chromatography-mass spectrometry (LC-MS) qualitative
Test method and liquid chromatography (LC) quantitative test method.
This document applies to the identification of AB-CHMINACA, AB-FUBINACA, AB-PINACA in suspected drug samples in the field of forensic science
Qualitative and quantitative analysis.
2 Normative references
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations
documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to
this document.
GB/T 6682 Analysis Laboratory Water Specifications and Test Methods
GB/T 27418 Evaluation and representation of measurement uncertainty
GA/T 122 Toxic Analysis Terminology
3 Terms and Definitions
Terms and definitions defined in GA/T 122 apply to this document.
4 Principles
AB-CHMINACA, AB-FUBINACA, AB-PINACA in suspected drug samples (see Appendix A for compound information)
row extraction. Liquid chromatography-mass spectrometry was used for detection, and the retention time, mass spectral characteristic ion pair and ion pair abundance ratio were used as the basis for qualitative judgment;
Detected by liquid chromatography, the chromatographic peak area was used as the quantitative basis, and the quantitative analysis was carried out by external standard single-point method or external standard standard curve method.
5 Reagents and Materials
5.1 Reagents
The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis were of chromatographic grade,
Reagents include.
a) acetonitrile;
b) methanol;
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