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GA/T 1919-2021 English PDF

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GA/T 1919-2021: Forensic sciences - Examination methods for succinycholine and succinymonocholine - LC-MS and IR
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GA/T 1919-2021English439 Add to Cart 4 days [Need to translate] Forensic sciences - Examination methods for succinycholine and succinymonocholine - LC-MS and IR Valid GA/T 1919-2021

PDF similar to GA/T 1919-2021


Standard similar to GA/T 1919-2021

GA/T 1788.2   GA/T 1711   GA/T 424   GA/T 1912   GA/T 1913   GA/T 1909   

Basic data

Standard ID GA/T 1919-2021 (GA/T1919-2021)
Description (Translated English) Forensic sciences - Examination methods for succinycholine and succinymonocholine - LC-MS and IR
Sector / Industry Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard A92
Word Count Estimation 19,191
Issuing agency(ies) Ministry of Public Security

GA/T 1919-2021: Forensic sciences - Examination methods for succinycholine and succinymonocholine - LC-MS and IR


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences - Examination methods for succinycholine and succinymonocholine - LC-MS and IR ICS 13.310 CCSA92 People's Republic of China Public Safety Industry Standards Forensic Science Succinylcholine and Succinylcholine Test Liquid Chromatography-Mass Spectrometry and Infrared Spectroscopy Published on 2021-10-14 2022-05-01 Implementation Published by the Ministry of Public Security of the People's Republic of China

foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents" Drafting. Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents. This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1). focal point. This document is drafted by. Jiangsu Provincial Public Security Department Physical Evidence Identification Center, Guangxi Zhuang Autonomous Region Public Security Department Criminal Investigation Corps, Fujian Provincial Public Security Bureau Department of Criminal Technology Corps, Hunan Provincial Public Security Department Physical Evidence Identification Center, Jiangxi Provincial Public Security Department Criminal Police Corps, Guangdong Provincial Public Security Department Criminal Technology Center, Criminal Technology Institute of Guangzhou Public Security Bureau. The main drafters of this document. Wang Xuehu, Zhang Qianshang, Liu Xiaofeng, Lin Jia, Yan Xiaojun, Liu Yongzi, Pei Maoqing, Sun Limin. Forensic Science Succinylcholine and Succinylcholine Test Liquid Chromatography-Mass Spectrometry and Infrared Spectroscopy

1 Scope

This document specifies the liquid chromatography-mass spectrometry (LC-mass spectrometry) of succinylcholine and succinylcholine in forensic biological samples (blood, muscle tissue). MS) and Infrared Spectroscopy (IR) Test Methods for Succinylcholine Chloride and Succinyl Monocholine Chloride in In Vitro Solid Samples. This document applies to the qualitative and quantitative analysis of succinylcholine and succinylcholine in forensic biological samples (blood, muscle tissue) and solid samples Qualitative analysis of succinylcholine chloride and succinylcholine chloride in the product. Other non-biological test materials can be referred to and applied.

2 Normative references

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to this document. GB/T 6682 Analysis Laboratory Water Specifications and Test Methods GA/T 122 Toxic Analysis Terminology

3 Terms and Definitions

Terms and definitions defined in GA/T 122 apply to this document. 4 Liquid chromatography-mass spectrometry 4.1 Principle The blank sample and the added sample were used as controls, and the biological samples were extracted and concentrated according to the requirements of parallel operation. Double quadrupole tandem mass spectrometry or liquid chromatography-high resolution mass spectrometry was used for detection, and external standard method was used for quantification. 4.2 Reagents and materials 4.2.1 Reagents The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis were of chromatographic grade, including Include the following reagents. a) Acetonitrile. b) Methanol. c) 20.0 mmol/L ammonium acetate solution containing 0.2% (volume fraction) formic acid. weigh 1540.0 mg ammonium acetate, add 100 mL Dissolve in water, add 2.0mL formic acid, and dilute to 1000mL. d) Initial mobile phase. take 10 mL of 20.0 mmol/L ammonium acetate solution containing 0.2% (volume fraction) formic acid and 90 mL of acetonitrile Mix well. e) Standard solution.

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