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Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - GC and GC-MS
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GA/T 1928-2021
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Basic data Standard ID | GA/T 1928-2021 (GA/T1928-2021) | Description (Translated English) | Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - GC and GC-MS | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | Classification of Chinese Standard | A92 | Word Count Estimation | 15,192 | Issuing agency(ies) | Ministry of Public Security |
GA/T 1928-2021: Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - GC and GC-MS ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Forensic sciences - Examination methods for AB-CHMINACA, AB-FUBINACA and AB-PINACA in suspected drugs - GC and GC-MS
ICS 13.310
CCSA92
People's Republic of China Public Safety Industry Standards
Forensic Science Suspected Drugs in AB-CHMINACA,
AB-FUBINACA and AB-PINACA inspection
Gas chromatography and gas chromatography-mass spectrometry
Published on 2021-10-14
2022-05-01 Implementation
Published by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
drafted.
Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1).
focal point.
This document is drafted by. Ministry of Public Security Material Evidence Identification Center, Fujian Provincial Public Security Department Criminal Technology Corps, Zhejiang Provincial Public Security Department, Ministry of Public Security Anti-drug Information
Report Technology Center, Ningbo City Public Security Bureau, Zhejiang Province, Zhejiang Province Shaoxing City Public Security Bureau.
The main drafters of this document. Yang Hongxian, Zheng Xiaoyu, Wen Wu, Zheng Hui, Zhang Chunshui, Li Hangqi, Fu Defeng, Zhao Yang, Qian Zhenhua, Chang Ying, Li Peng,
Jia Wei, Zhuang Shun, Sun Jiancong, Wu Kaifeng, Liu Jiming, Zhao Yanbiao, Zhai Wanfeng, Liu Kelin, Gao Lisheng.
Forensic Science Suspected Drugs in AB-CHMINACA,
AB-FUBINACA and AB-PINACA inspection
Gas chromatography and gas chromatography-mass spectrometry
1 Scope
This document regulates N-(1-carbamoyl-2-methylpropyl)-1-(cyclohexylmethyl)indium in solid samples of suspected narcotics in the field of forensic science
azole-3-carboxamide (AB-CHMINACA), N-(1-carbamoyl-2-methylpropyl)-1-(4-fluorobenzyl)indazole-3-carboxamide (AB-FUBI-
NACA), N-(1-carbamoyl-2-methylpropyl)-1-pentylindazole-3-carboxamide (AB-PINACA) gas chromatography-mass spectrometry (GC-MS)
Qualitative test method and gas chromatography (GC) quantitative test method.
This document applies to AB-CHMINACA, AB-FUBINACA, AB-CHMINACA, AB-FUBINACA, AB-
Qualitative and quantitative analysis of PINACA.
2 Normative references
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations
documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to
this document.
GB/T 27418 Evaluation and representation of measurement uncertainty
GA/T 122 Toxic Analysis Terminology
3 Terms and Definitions
Terms and definitions defined in GA/T 122 apply to this document.
4 Principles
AB-CHMINACA, AB-FUBINACA, AB-PINACA (for compound information, see Appendix A) in suspected drug solid samples were tested.
row extraction. Gas chromatography-mass spectrometry was used for detection, and retention time, characteristic ions and ion abundance ratios were used as the basis for qualitative judgment;
The chromatographic peak area was used as the quantitative basis, and the external standard single-point method or the external standard standard curve method was used for quantitative analysis.
5 Reagents and Materials
5.1 Reagents
Unless otherwise stated, the reagents used in the analysis are of analytical grade, including.
a) methanol;
b) Standard solution.
1) Standard material stock solution. 1.0mg/mLAB-CHMINACA, AB-FUBINACA, AB-PINACA standard material
Stock solution, refrigerated at 0℃~4℃, valid for 12 months;
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