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Forensic sciences - Examination methods for 7 phenylethylamines including 4-ethyl-2, 5-dimethoxyphenethylamine in suspected drugs - LC and LC-MS
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GA/T 1927-2021
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Basic data Standard ID | GA/T 1927-2021 (GA/T1927-2021) | Description (Translated English) | Forensic sciences - Examination methods for 7 phenylethylamines including 4-ethyl-2, 5-dimethoxyphenethylamine in suspected drugs - LC and LC-MS | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | Classification of Chinese Standard | A92 | Word Count Estimation | 23,249 | Issuing agency(ies) | Ministry of Public Security |
GA/T 1927-2021: Forensic sciences - Examination methods for 7 phenylethylamines including 4-ethyl-2, 5-dimethoxyphenethylamine in suspected drugs - LC and LC-MS ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13.310
CCSA92
People's Republic of China Public Safety Industry Standards
Forensic Science 2,5-Dimethoxy-4- in Suspected Drugs
7 kinds of phenethylamine drugs such as ethyl phenethylamine test
Liquid chromatography and liquid chromatography-mass spectrometry
LCandLC-MS
Published on 2021-10-14
2022-05-01 Implementation
Published by the Ministry of Public Security of the People's Republic of China
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
drafted.
Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by the National Criminal Technology Standardization Technical Committee Toxic Analysis Sub-Technical Committee (SAC/TC179/SC1).
focal point.
This document is drafted by. Ministry of Public Security Material Evidence Appraisal Center, Hainan Provincial Public Security Department, Jiangsu Provincial Public Security Bureau Material Evidence Appraisal Center, Ministry of Public Security Drug Control Situation
Report to the Technology Center and the Public Security Bureau of Bijie City, Guizhou Province.
The main drafters of this document. Zhao Yang, Zhai Wanfeng, Wen Wu, Zheng Hui, Zhang Chunshui, Liu Guangming, Qian Kaiwen, Zhang Tingting, Qian Zhenhua, Chang Ying, Li Peng,
Zhao Yanbiao, Yang Hongxian, Zheng Xiaoyu, Liu Kelin, Zhang Jing, Gu Yuebao, Wang Xuehu, Zhang Qianshang, Yang Zhi, Wei Jiao, Wen Biao, Du Song, Zeng Yuan, Long Qinglin,
Gao Lisheng.
Forensic Science 2,5-Dimethoxy-4- in Suspected Drugs
7 kinds of phenethylamine drugs such as ethyl phenethylamine test
Liquid chromatography and liquid chromatography-mass spectrometry
1 Scope
This document regulates 2,5-dimethoxy-4-ethylphenethylamine (2C-E), 2,5-dimethoxy-benzene
Ethylamine (2C-H), 2,5-dimethoxy-4-iodophenethylamine (2C-I), N-(2-methoxybenzyl)-2-(2,5-dimethylene) Oxy-4-bromophenyl)ethanamine
(2C-B-NBOMe), N-(2-methoxybenzyl)-2-(2,5-dimethoxy-4-chlorophenyl)ethanamine (2C-C-NBOMe), N- (2-Methoxybenzyl
yl)-2-(2,5-dimethoxy-4-methylphenyl)ethanamine (2C-D-NBOMe), N-(2-methoxybenzyl)-2-(2,5 -Dimethoxy-4-iodobenzene
Liquid chromatography-mass spectrometry (LC-MS) qualitative test method and liquid chromatography (LC) quantitative test method of ethyl) ethylamine (2C-I-NBOMe).
This document applies to 2C-E, 2C-H, 2C-I, 2C-B-NBOMe, 2C-C-NBOMe,
Qualitative and quantitative analysis of 2C-D-NBOMe and 2C-I-NBOMe.
2 Normative references
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations
documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to
this document.
GB/T 6682 Analysis Laboratory Water Specifications and Test Methods
GB/T 27418 Evaluation and representation of measurement uncertainty
GA/T 122 Toxic Analysis Terminology
3 Terms and Definitions
Terms and definitions defined in GA/T 122 apply to this document.
4 Principles
For 2C-E, 2C-H, 2C-I, 2C-B-NBOMe, 2C-C-NBOMe, 2C-D-NBOMe, 2C-I-NBOMe (Chemical
For compound information, see Appendix A) for extraction. Using liquid chromatography-mass spectrometry detection, retention time, mass spectral characteristic ion pair and ion pair abundance ratio
As the basis for qualitative judgment; liquid chromatography was used for detection, the chromatographic peak area was used as the quantitative basis, and the external standard single-point method or the external standard standard curve method was used.
Perform quantitative analysis.
5 Reagents and Materials
5.1 Reagents
The experimental water should meet the first-class water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis were of chromatographic grade,
Reagents include.
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