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Methods for chemical analysis of cadmium zinc telluride - Determination of zinc and cadmium contents - Inductively coupled plasma atomic emission spectrometry
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Basic data
| Standard ID | GB/T 41769-2022 (GB/T41769-2022) |
| Description (Translated English) | Methods for chemical analysis of cadmium zinc telluride - Determination of zinc and cadmium contents - Inductively coupled plasma atomic emission spectrometry |
| Sector / Industry | National Standard (Recommended) |
| Classification of Chinese Standard | H13 |
| Word Count Estimation | 14,199 |
| Issuing agency(ies) | State Administration for Market Regulation, China National Standardization Administration |
GB/T 41769-2022: Methods for chemical analysis of cadmium zinc telluride - Determination of zinc and cadmium contents - Inductively coupled plasma atomic emission spectrometry
---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Methods for chemical analysis of cadmium zinc telluride - Determination of zinc and cadmium contents - Inductively coupled plasma atomic emission spectrometry
ICS 77.120.99
CCSH13
National Standards of People's Republic of China
Method for chemical analysis of cadmium zinc telluride - Determination of zinc and cadmium content
Inductively Coupled Plasma Atomic Emission Spectroscopy
Published on 2022-10-12
2023-02-01 Implementation
State Administration for Market Regulation
Released by the National Standardization Administration
foreword
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1.Structure and Drafting Rules of Standardization Documents"
drafted.
Please note that some content of this document may be patented. The issuing agency of this document assumes no responsibility for identifying patents.
This document is proposed by China Nonferrous Metals Industry Association.
This document is under the jurisdiction of the National Nonferrous Metals Standardization Technical Committee (SAC/TC243).
This document is drafted by. Guangdong Pilot Rare Materials Co., Ltd., Beikuang Testing Technology Co., Ltd., Chengdu CNBM Photoelectric Materials Co., Ltd.
Company, Shenzhen Zhongjin Lingnan Nonferrous Metals Co., Ltd., Zijin Copper Co., Ltd., Zhuzhou Smelting Group Co., Ltd., China Inspection and Quarantine
Inspection and Certification Group Guangxi Co., Ltd., National Standard (Beijing) Inspection and Certification Co., Ltd., Industrial Analysis and Testing Center of Guangdong Academy of Sciences, Guohe General
(Qingdao) Testing and Evaluation Co., Ltd., China Nonferrous Metals Guilin Mineral Geology Research Institute Co., Ltd., Shaoguan City, Guangdong Province, Quality Metrology Supervision and Inspection
testing institute.
The main drafters of this document. Zhu Zanfang, Wei Shenglin, Luo Haixia, Zheng Lin, Zuo Hongyi, Zhong level, Ning Yumei, Qin Jianyou, Li Tian, Zhang Yucheng,
Gu Xusheng, Zhang Zhenglian, Yuan Qi, Su Chunfeng, Sun Yanrong, Tan Xiuli, Zhang Yuping, Yang Yue, Wei Yajuan, Zhang Lijiu, Ruan Guise, Wu Xueying.
Method for chemical analysis of cadmium zinc telluride - Determination of zinc and cadmium content
Inductively Coupled Plasma Atomic Emission Spectroscopy
Caution - Persons using this document should have practical experience in formal laboratory work. This document does not address all possible security issues
question. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the conditions stipulated by relevant national regulations.
1 Scope
This document specifies the method for the determination of zinc and cadmium content in cadmium zinc telluride.
This document is applicable to the determination of zinc and cadmium content in cadmium zinc telluride.
The amount is 18.00%~46.00%.
2 Normative references
The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations
documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to
this document.
GB/T 6682 Analysis Laboratory Water Specifications and Test Methods
3 Terms and Definitions
There are no terms and definitions that need to be defined in this document.
4 Principles
After the sample was dissolved in nitric acid and hydrochloric acid, the solution was fixed to volume and then weighed (accurate to 0.0001g), using yttrium as the internal standard element, using inductively coupled plasma
The daughter atomic emission spectrometer was used to measure the intensity of the characteristic spectral line of the element to be tested in the solution, and the content of zinc, cadmium and cadmium in the sample were calculated through the standard curve.
content.
5 Reagents or materials
Unless otherwise specified, only reagents confirmed as analytical grade and laboratory secondary water in accordance with GB/T 6682 are used in the analysis.
5.1 Hydrochloric acid (ρ=1.19g/mL).
5.2 Nitric acid (ρ=1.42g/mL).
5.3 Hydrochloric acid (1 10).
5.4 Zinc standard solution. Weigh 0.10g of metallic zinc (wZn≥99.99%) (accurate to 0.0001g) into a 250mL beaker, add 15mL
Hydrochloric acid (5.1), 5 mL of nitric acid (5.2), cover with a watch glass, heat at low temperature until completely dissolved, remove, cool to room temperature, rinse the surface with a small amount of water
Transfer the test solution to a pre-dried and weighed 250mL volumetric flask (m0), dilute it with water to the mark, and weigh the mass (m1) (accurate to
0.001g), mix well, 1g of this solution contains about 400μg zinc.
5.5 Cadmium standard solution. Weigh 0.10g metal cadmium (wCd≥99.99%) (accurate to 0.0001g) into a 250mL beaker, add 15mL
...
