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SN/T 1851-2006: Determination of retardant in textiles. GC-MS method
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| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 1851-2006 | English | 259 |
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Determination of retardant in textiles. GC-MS method
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SN/T 1851-2006
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Basic data | Standard ID | SN/T 1851-2006 (SN/T1851-2006) | | Description (Translated English) | Determination of retardant in textiles. GC-MS method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | W04 | | Classification of International Standard | 59-010 | | Word Count Estimation | 8,886 | | Date of Issue | 2006-11-10 | | Date of Implementation | 2007-05-16 | | Regulation (derived from) | Chinese industry standards for record 2007 of 3 (total of 87) | | Issuing agency(ies) | General Administration of Customs | | Summary | This standard specifies the textile flame retardant tris (2, 3 dibromo- propyl) phosphate, polybrominated biphenyls, polybrominated diphenyl ethers and eight five PBDE detection method. This standard applies to textile flame retardant tris (2, 3 dibromo- propyl) phosphate, polybrominated biphenyls, polybrominated diphenyl ethers five and eight Determination of polybrominated diphenyl ethers. | SN/T 1851-2006: Determination of retardant in textiles. GC-MS method---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of retardant in textiles.GC-MS method
Book of the People's Republic of China Entry and Exit Inspection and Quarantine
Method for detecting flame retardant finishing agent in textiles
Gas chromatography-mass spectrometry
Released on.2006-11-10
2007-05-16 implementation
People's Republic
The General Administration of Quality Supervision, Inspection and Quarantine issued
Foreword
Appendix A of this standard is an informative annex.
This standard is proposed and managed by the National Certification and Accreditation Administration.
This standard was drafted by the Shenzhen Entry-Exit Inspection and Quarantine Bureau of the People's Republic of China.
The main drafters of this standard. Li Lixia, Zhang Weiya, Liu Caiming, Wang Chengyun, Fan Xiurong, Tang Lichun, Yan Naiqing.
This standard is the first industry standard for entry-exit inspection and quarantine.
Method for detecting flame retardant finishing agent in textiles
Gas chromatography-mass spectrometry
1 Scope
This standard specifies three (2,3-dibromopropyl)phosphate, polybrominated biphenyl, pentabromodiphenyl ether and octabromodiphenyl ether in textiles.
Detection method.
This standard applies to the flame retardant finishing agent tris(2,3-dibromopropyl)phosphate, polybrominated biphenyl, pentabromodiphenyl ether and octabromodiphenyl ether in textiles.
Determination.
2 Terms and definitions
The following terms and definitions apply to this standard.
Add substances that prevent flame burning in textiles. Such as. Tris (2,3-dibromopropyl) phosphate (Tris (2,3-dibromopropyl)
Phosphate), polybrominated biphenyls (PBBs), pentabrominated diphenyl
Ether) and octabrominated diphenylether.
3 Principle
The sample was extracted by Soxhlet using toluene as the extraction solvent, and the extract was concentrated and chromatographed by gas chromatography-mass spectrometry.
analysis.
4 reagents and standards
Unless otherwise specified, the reagents used should be of analytical grade.
4.1 Toluene. chromatographically pure.
4.2 Tris(2,3-dibromopropyl)phosphate standard. purity ≥ 96.9%.
4.3 Polybrominated biphenyl standards. purity ≥ 98.2%.
4.4 Tris(2,3-dibromopropyl)phosphate standard stock solution. Accurately weigh 10.0mg of tris(2,3-dibromopropyl)phosphate standard
(4.2), placed in a 100 mL volumetric flask, diluted to the mark with toluene (4.1), and mixed. The concentration of this solution was 100 mg/L.
4.5 Polybromobiphenyl standard stock solution. Accurately weigh 10.0mg of polybrominated biphenyl standard (4.3), placed in a 100mL volumetric flask,
Dilute to the mark with toluene (4.1) and mix. The concentration of this solution was 100 mg/L.
4.6 Pentabromodiphenyl ether standard solution. 50mg/L isooctane solution.
4.7 OctaBDE standard solution. 50mg/L isooctane solution.
4.8 Internal standard. Decachlorobiphenyl, purity 100% ± 4%.
4.9 Standard stock solution of internal standard. accurately weigh the appropriate amount of decachlorobiphenyl standard (4.8), and prepare the concentration with toluene (4.1).
Standard stock solution of 100 mg/mL.
4.10 Mixed standard working solution. Take appropriate amount of internal standard standard stock solution (4.9), tris(2,3-dibromopropyl)phosphate standard stock solution
(4.4), PBB standard stock solution (4.5), pentabromodiphenyl ether (4.6) and octabromodiphenyl ether (4.7) standard solution at a concentration of 50 mg/L, root
Dissolve to a suitable concentration of the mixed standard working solution with toluene (4.1) as needed.
4.11 Internal standard solution. Take appropriate amount of internal standard stock solution (4.9), and dilute to a suitable concentration of solution with toluene (4.1) as needed.
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