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SN/T 0645-2014: Determination of diuron residues in meat and meat products for export. Liquid chromatography method
Status: Valid SN/T 0645: Evolution and historical versions
| Standard ID | Contents [version] | USD | STEP2 | [PDF] delivered in | Standard Title (Description) | Status | PDF |
| SN/T 0645-2014 | English | 389 |
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Determination of diuron residues in meat and meat products for export. Liquid chromatography method
| Valid |
SN/T 0645-2014
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| SN 0645-1997 | English | 519 |
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4 days [Need to translate]
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Method for the determination of diuron residues in meats and meat products for export
| Obsolete |
SN 0645-1997
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PDF similar to SN/T 0645-2014
Basic data | Standard ID | SN/T 0645-2014 (SN/T0645-2014) | | Description (Translated English) | Determination of diuron residues in meat and meat products for export. Liquid chromatography method | | Sector / Industry | Commodity Inspection Standard (Recommended) | | Classification of Chinese Standard | X22 | | Classification of International Standard | 67.120.10 | | Word Count Estimation | 15,158 | | Older Standard (superseded by this standard) | SN 0645-1997 | | Quoted Standard | GB/T 6682 | | Regulation (derived from) | AQSIQ notification issued in 2014 on the first batch of 230 industry-standard entry-exit inspection and quarantine | | Issuing agency(ies) | General Administration of Customs | | Summary | This Standard specifies the method of liquid chromatography export meat and meat products diuron residues. This Standard applies to beef, canned luncheon meat, chicken meatballs, lamb, donkey in the determination of diuron Long residues. | SN/T 0645-2014: Determination of diuron residues in meat and meat products for export. Liquid chromatography method
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Determination of diuron residues in meat and meat products for export.Liquid chromatography method
People's Republic of China Entry-Exit Inspection and Quarantine Standards
Replacing SN 0645-1997
Exports of meat and meat products Determination of diuron Long Residue
Liquid chromatography
Issued on. 2014-01-13
2014-08-01 implementation
People's Republic of China
The State Administration of Quality Supervision, Inspection and Quarantine released
Foreword
This standard was drafted in accordance with GB/T 1.1-2009 given rules.
This standard replaces SN 0645-1997 "export of meat and meat products diuron residues in."
Compared with SN 0645-1997, the main technical changes are as follows.
--- The original standard name "export meat and meat products diuron residues in" to "export meat and meat products diuron
Determination of the residual liquid chromatography ";
--- Cancel the original standard sampling and sample preparation section;
--- The original scope of application of the revised standard is. beef, canned luncheon meat, chicken meatballs, lamb, donkey;
--- Sample pretreatment conditions were revised;
--- Of liquid chromatography conditions were revised.
This standard is proposed and managed by the National Certification and Accreditation Administration Committee.
This standard was drafted. People's Republic of China Shandong CIQ.
The main drafters of this standard. Li Junmin, Bai Xinghua, He Tongxin, into yellow, Gengjin Pei Yan Qiucheng.
This standard replaces the standards previously issued as follows.
--- SN 0645-1997.
Exports of meat and meat products Determination of diuron Long Residue
Liquid chromatography
1 Scope
This standard specifies the method for liquid chromatography export meat and meat products diuron residues.
This standard applies to beef, canned luncheon meat, chicken meatballs, lamb, donkey in the determination of diuron Long residues.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein
Member. For undated references, the latest edition (including any amendments) applies to this document.
Laboratory use specifications and test methods GB/T 6682 Analysis
3 Method summary
Sample remaining diuron methanol - acetonitrile (11, volume ratio) extraction by liquid-liquid partition and neutral alumina column purified,
Determined by high performance liquid chromatography with UV detection, external standard.
4 Reagents and materials
Unless otherwise specified, the reagents were of analytical grade water as a water GB/T 6682 regulations.
4.1 Methanol. HPLC grade.
4.2 acetonitrile. HPLC grade.
4.3 chloroform. The all-glass apparatus redistilled.
4.4 petroleum ether. boiling range 60 ℃ ~ 90 ℃, after all-glass apparatus redistilled.
4.5 anhydrous sodium sulfate. After burning 650 ℃ 4h, storage desiccator.
4.6 sodium chloride.
4.7 methanol - acetonitrile (11 volume). amount of an equal volume of methanol and acetonitrile, mixed well and reserve.
4.8 methanol - acetonitrile - water (70525, volume ratio). by volume of methanol, acetonitrile and water, mixed thoroughly take 70.5.25 volume ratio, and
Degassed, filtered and set aside.
4.9 with saturated sodium chloride solution. adding an excess of sodium chloride in water, heated and boiled for 10min, until no more sodium chloride dissolved, cooled
To room temperature. The cooled solution was filtered with filter paper, that is, saturated sodium chloride solution.
4.10 diuron (diuron) standard purity greater than or equal to 98.0%.
4.11 Standard stock solution (100mg/L). Weigh 10.0mg diuron standards, was dissolved in methanol - acetonitrile (4.7), and transferred
100mL flask with methanol - acetonitrile (4.7) to volume, mix, 0 ℃ ~ 4 ℃ preservation.
4.12 standard working solution. If necessary, draw a certain amount of standard stock solution (4.11), with methanol - into a series of diluted aqueous solution (4.8) - acetonitrile
Standard working solution.
4.13 neutral alumina column. 6mL, 1000mg, or equivalent person. Before use 5mL methanol - acetonitrile - water (4.8) Pre-rinse.
4.14 over anhydrous sodium Column. 3g over anhydrous sodium sulfate and placed in a glass column tube.
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